Solvent |
Boiling point (oC) |
Solubility in g/mL at room temperature |
Solubility in g/mL at bp |
A |
220 |
0.13 g |
43 g |
B |
80 |
4.8 g |
12 g |
C |
172 |
0.24 g |
36 g |
D |
168 |
2.4 g |
28 g |
a. The solvent B is recommended for carrying out the crystallization of p-toluic acid.
b. The reasons for recommending that solvent are as follows:
A student wanted to crystallize P-Toluic acid (structure and melting point shown below) and therefore obtained...
What is the literature (known) melting point for acetanilide? A student performed a recrystallization to purify a crude sample from a reaction. The amount of crude material collected from the reaction was 13.56 grams. After the purification, the student collected 8.97 grams of extremely pure material. a. What is the percent recovery of the desired material? b. Is it possible to determine how much of the desired material remained in solution after the filtration? The solubility of acetanilide in hot...
help with identifiying each unknown in extraction and washing experiment. the ir spectra are given below, along with data, and the lab sheet is attached. Neutral Solid Primary amine (Aniline) 3403cm - NE presence Transmittance 60 3258cm 1 streren NOUD Streich 50 Ctretcher strator NH2 aromatto 11 NO2 aring 2-nitroaniline K LILI 3600 3200 2800 2400 2000 1800 1600 Wavenumber cm-1 1400 1200 1000 800 600 Basic Solid primary amine Transmittance I NH2 Stretch p-acetvianiline 70 60 CS HG NO...
please identify the unknown and write a derivative Unknown compound 3 Clear liquid Physcial Properties Solubility Dissolve in ethyl ether Not dissolved in water Boiling point 77 IR spectrum Transmitance 3000 1000 2000 Wavenumber cm-1) Classification Positive test in Alkaline Iron (III) Hydroxamate test test CLASSIFICATION TESTS These tests must be done together with known AND FOLLOW PROCEDURE IN YOUR TEXT CARBOXYLIC ACIDS are detected by teating aqueous solutions with limus or pH paper. Also, disolve In NaHCO with bubbles...
Need help, numbers 3-6 please show work. and fill out table of chemicals for all chemical used. calculate mmol in the table as well show work please and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...