(1) If a 47.2 g sample of the
liquid 1-heptanethiol has a volume of
56.0 mL, what is the specific gravity of the
compound? Take the density of water to be 1.00 g/mL.
specific gravity =
(2) The liquid 1-heptanethiol is
insoluble in water. If approximately equal volumes of water and
1-heptanethiol were mixed in a separatory funnel,
would the water layer end up on the top or on the bottom?
_________water on the topwater on the bottom
(1) If a 47.2 g sample of the liquid 1-heptanethiol has a volume of 56.0 mL,...
The density of dichloromethane, an organic solvent, is 1.325 g/cm. If you mix 50 mL water and 50 mL dichloromethane together in a separatory funnel, which layer would be on top? The density of diethyl ether, an organic solvent, is 0.706 g/cm. If you mix 50 mL water and 50 mL diethyl ether together in a separatory funnel, which layer would be on top?
1) during liquid liquid extraction ( LLE) it is normal to use separatory funnel, and two non- miscible phases of solvents , for ex: water as polar phase and ethyl acetate is the organic phase. density of water is 1,0 g/ ml, while density of ethyl acetate is 0.90 g/ ml at 25.0 celsius degrees. which of the two solvents will end up at the buttom of the separatory funnel? 2) ) during liquid liquid extraction ( LLE) it is...
Check Answer Hint Resources Score: 41.8% of 25 > Organic Chemistry Roberts & Company Publishers Loudon presented by Macmillan Learning a) 50 mL of CH,CH, Br (bromoethane) and 50 mL of water are poured into a separatory funnel. Bromoethane is a water-insoluble compound with a density of 1.460 . The funnel is stoppered and the mixture is shaken vigorously. After standing, two layers separate. mL Which substance is in which layer? Explain. Bromoethane is more dense than water. The top...
Just Answer Question 5 Synthesis of 2-chloro-2-methylbutane (literature version) Concentrated aqueous hydrochloric acid (HCI, 3.3 equivalents) was slowly added to 2-methyl-2-butanol (1.0 equivalents) in a 100 mL round bottom flask with stirring. The reaction was stirred for 15 minutes at room temperature. Upon completion, the reaction mixture was transferred to a 60 mL separatory funnel and the aqueous layer was removed. The organic layer (i.e. the product) was successively washed with: (1) saturated aqueous NaCl (brine), (2) saturated aqueous NaHCO,...
a6f34c2c2eb8&attempt 1 Question 1 Volume Water 114.64 mL Initial Temperature of Water 60 °C Volume of Compound Y 100 mL 25 Initial Temperature of Compound Y °C 36.08 °C Final temperature of Compound Y + Water Question 2 Calculate the specific heat of Compound Y from your data. The specific heat of water is 4.184 J/gºC and its density is 1.00 g/mL. The density of compound Y is 2.78 g/mL. J/g°C
Name: Date: Separation of Acid/Base/Neutral compounds using liquid-liquid extraction OCH CHO HN Benzocaine Molecular Weight: 165.19 Melting Point: 88-90 °C 1,1-biphenyl Molecular Weight: 154.21 Melting Point: 68-70 °C trans-cinnamic acid Molecular Weight: 148.16 Melting Point: 132-135 °C Question 1: Identify the following compounds as Acid, Base or Neutral. (2 points) a. Benzocaine: b. Biphenyl: c. Trans-cinnamic acid: (2 points) _ (2 points) Question 2: Draw the structure in the box (5 points each): NaOH OCH,CH, HCM NaOHA HC form. Ples...
1. Indicate which of the following would be considered physical properties (P) and which would be considered chemical properties (C) of iron. ー-a. Iron reacts with oxygen to form iron oxides. b. Iron is a good conductor of heat and electricity. C. Iron melts at 1535°C. d. When iron is immersed in a solution of hydrochloric acid, hydrogen gas is produced. e. Iron becomes red-hot when heated. __ f. A500-cc volume of iron has a mass of 3930 g. Iron...
SYNTHESIS OF T-PENTYL CHLORIDE LAB Provide a stoichiometry table for the reaction being performed in this lab. PROCEDURE Preparation oft-Pentyl Chloride In a 125-mL separatory funnel, place 10.0 mL of tert-pentyl alcohol (2-methyl-2- butanol, MW = 88.2, d = 0.805 g/mL) and 25 mL of concentrated hydrochloric acid (d 1.18 g/mL). Do not stopper the funnel. Gently swirl the mixture in the separa- tory funnel for about 1 minute. After this period of swirling, stopper the separatory funnel and carefully...
Answer the following before coming to lab: 1.) Based on what you saw last week, which enantiomer of tartaric acid would you expect to co- crystallize with (SS)-1,2-diammoniumcyclohexane? 2.) If you had a neutral aqueous solution of triethylamine, would you add acid or base in order to extract it with an organic solvent? 3.) Now, consider a dichloromethane solution of triethylamine. Would you extract with acidic aqueous or basic aqueous solution in order to get the triethylamine out of the...
pre-laboratory Questions A 1 Explain why it is more efficient to make several extractions using small portions rather than one extraction using the same total volume. 2 Define the following terms: Drying agent intensity Drying agent capacity 3 Select the upper layer in each pair of mixed solvents (see Appendix C): Water and benzene Water and carbon tetrachloride Water and ether 4 Write an equation for the reaction of a benzoic acid with aqueous sodium bicarbonate. 5 Complete the following...