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Starting at the x-axis at the 15 cycl / 85 tol point, draw a line straight up to the liquid curve (the bottom curve). Draw a straight horizontal line over to the vapor curve (the top curve) and back down to the liquid curve.
This is where your second fraction starts. Now draw a line from there over to the vapor curve, and back down to the liquid curve.
For your third fraction, draw another line across from the liquid to the vapor curve, then down to the x-axis.
Now check - are you at the 90 cycl / 10 tol point? If not, draw do a fourth fraction.
Therefore, 3 plates for the fractional. However, your simple distillation number will be the same as your theoretical plates. Each step on your fractional is equal to a simple distillation.
Refer to one of the BP-Composition curves for Cyclohexane - Toluene above. Starting with a mixture...
o-chem lab help 6. a. A mixture of 60 mol % n-propy!cyclohexane and 40 mol % n-propylbenzene is distilled through a simple distillation apparatus; assume that no fractionation occurs during the distillation. The boiling temperature is found to be 157。C (760 torr) as the first small amount of distillate is collected. The standard vapor pressures of n-propylcyclohexane and n-propylbenzene are known to be 769 torr and 725 torr, respectively, at 1573 °C Calculate the percentage of cach of the two...
a. Is distillation a purification or a characterization technique? Explain. b. Where the thermometer bulb should be placed in order to measure the temperature of the hot vapor accurately during distillation? c. What is the purpose of the “packing” in a fractional distillation column? d. Why should a distillation flask never be more than ¾ full before starting a distillation? e. You are fractionally distilling 100 mL of a 1:1 solution of cyclohexane and toluene. After 2 mL has distilled...
#9. if you were trying to separate two compounds with very close boiling points how could you increase the efficiency of a fractional distillation in order to separate those compounds? thank you!! b. Which component should still off ist? How does the boiling point of that liquid compare to comperare mesurements at the beginning of both simple and fractional distillation? d What does this comparison tell you about the composition of the station from both simple and tractional distillation? e....
#8- could simple distillation be used to isolate a pure sample? if so, in what type if situation would this be possible? thank you!! b. Which component should distill off first? c How does the boiling point of that liquid compare to temperature measurements at the beginning of both simple and fractional distilation? d. What does this comparison tell you about the composition of the intial distlation from both simple and fractional diestilation? e Using vour tractional distilation plot, estimate...
Need assistance with graph and pre-lab questjons 1. Refer to the vapor-liquid composition curve for a benzene/toluene solution below. a) Are benzene and toluene miscible or immiscible? b) What is the boiling point of a benzene-toluene mixture that is 20% benzene? c) What percent benzene is a benzene-toluene mixture that boils at 85°C? 110 100 95 0F-- 85 A" 80 75 0 10 20 30 40 50 60 7o 80 90 100 Molo porcont benzene 2. Refer to the Boiling...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
Working on the questions at the end of this lab report (see above). I need help answering questions 2, 3, and 4 completely and thoroughly. Thank you! s, until the I hexano 1 clean disti CYCLOHEXENE from CYCLOHEXANOL be dehydrated with solfuric acid to yield cyclohexene and waterf Add a 0°C (record ct and cal H,SO + H20 ainer. s in purification of any crude product are (a) the preliminary separation of the product from the reaction mixture by distillation...
Synthesis of 1-Bromobutane: An SN2 Reaction Pre-Laboratory Exercises PRE-LABORATORY EXERCISES NAME: Cynthesis of 1-Bromobutane: An SN 2 Reaction Butylbromide was prepared by refluxing in a 100-ml round bottomed flask a solution containing 13:35 Br 15 ml of water, 10 mL of n-butyl alcohol. 15 ml of concentrated H.SO. and a few boiling stories, 1. 2. R." d 1.275 laborales Nel CH3CH2CH2CH2OH + NaBr H2SO4 Superletalyst CHCH2CH2CHBr + NaHSO + HO (eq. 16) 1-butanol bp 118 C 1-bromobutane d 0.810 bp...
The following questions are from an experiment titled Friedel-Crafts Alkylation for Organic Chemistry II Lab. There are pictures attached of the lab manual. 2) Is this method a good route for the preparation of p-sec-butyltoulene? Give reasons for your answer. 3) Why do you use a large excess of toulene. What are its functions? 4) What is the purpose for adding the hydrochloric acid to the water in the separatory funnel in step 5? Hint: If no acid is added,...
i need help with the postlab questions please Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....