What is the mechanism for the gringard feaciton between: magnesium and bromoethane (with anhydrous ether—whats the...
Homework Answers
Add Answer to:
What is the mechanism for the gringard feaciton between: magnesium
and bromoethane (with anhydrous ether—whats the...
A Grignard reaction was performed using the following steps: Step 1: Addition of Grignard Reagent: Phenyl...
A Grignard reaction was performed using the following steps: Step 1: Addition of Grignard Reagent: Phenyl Magnesium Bromide a solution of phenyl magnesium bromide (2.7 mL of a 3.0 M solution in anhydrous diethyl ether) and 5 mL of anhydrous diethyl ether was dispensed into the round-bottom flask and stirred with a stir bar. Step 2: Addition Formation: Reaction with Benzophenone A solution of 0.72 g (mp = 48-49 degrees C) of benzophenone and 2.0 mL of anhydrous diethyl ether...
What is the purpose of extracting the aqueous layer two more times with ether in step...
What is the purpose of extracting the aqueous layer two more
times with ether in step 5?
What is the purpose of washing the combined organic layers with
NaOH in step 6?
Thank you
Reaction 1: Nitration HNO3 NO2 + H2SO4, H20 NO2 toluene NO2 ortho meta para Procedure for Reaction 1: 1) To a stirred solution of 3 ml (44.7 mmoles) 67 % HNO3 in 3.75 mL of water, H2SO4 (9 mL) was slowly added at 10-15 °C. 2)...
. Grignard Reagents and As (Addition, Nucleophil ic) Additions Magnesium metal spontaneously reduces organohalides via...
.
Grignard Reagents and As (Addition, Nucleophil ic) Additions Magnesium metal spontaneously reduces organohalides via a succession transfers. This results in the Grignard 'insertion reaction, as proposed in the 1920s single electron Procedure t was only Part A: Preparation of the Glassyware and Magnesium successful in ether solvents, and failed utterly n hydrocarbons such as benzene. 1. The Grignard reagent camot form in the presence of water, and any water that it comes Mg (solid) into contact with immed iately...
i need help with post questions, thanks Product Isolation After stirring the reaction for 5 minutes...
i need help with post questions, thanks
Product Isolation After stirring the reaction for 5 minutes and allowing the reaction mixture to cool (the reaction can be exothermic), remove the Claisen head from the conical vial. Slowly add 3 M HCl(aq) drop-wise. The solid may need to be broken up with a stirring rod or a pipet. Continue to add acid until the aqueous phase (bottom layer) tests positive with pH paper. Extractions can be done using the conical funnel...
Why did you wash the ether solution with sodium bicarbonate? Write chemical equations for the rea...
Why did you wash the ether solution with sodium bicarbonate? Write chemical equations for the reactions that took place. b. At which purification steps was the unreacted methanol removed in the reaction? Some of it may have been removed in more than one place. c. Three-Step Synthesis of Methyl Anisate (Step 3) 0 CHOH. Н.so, cat.) Wear gloves. Methanol is poisonous. Ether is an anesthetic, so don't breathe it. Sulfuric acid is a strong corrosive acid. Wash any you spill...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium...
Grignard Reaction with a Ketone: Triphenylmethanol Introduction: The purpose of this lab is to prepare phenylmagnesium bromide, a Grignard reagent, and react it with benzophenone to give triphenylmethanol. Grignard reagents are very reactive and must be synthesized in an environment free of water or any other source of potential proton donor. Once made, the Grignard reagent will do a nucleophilic attack on the carbonyl carbon of the ketone, benzophenone. The result is an alkoxide that is then protonated to give...
please answer the prelab excercise:) I tried doing it but I did not get very far Experiment 7: Grignard Reactio...
please answer the prelab excercise:) I tried doing it but I did not
get very far
Experiment 7: Grignard Reaction. Introduction Discovered by French chemist Victor Grignard, the reaction that now bears his name is an example of the preparation of an organometallic reagent. In this lab, phenylmagnesium bromide is the Grignard of interest, and it will be added to an aldehyde to produce an alcohol. Lab Objectives 1. To study organometallic reagents in general. benzophenone. 2. To prepare phenylmagnesium...
using pictures and a maximum of 10 words, explain why an oven-dried 5-ml conical vial and...
using pictures and a maximum of 10 words, explain why an oven-dried
5-ml conical vial and drying tube(step 1 and 2 of part 1) are used
in the reaction. do both please! also the notebook pages are the
procedure
(1) Using pictures and a maximum of 10 words, explain why an oven-dried 5-ml conical vial and drying tube (step 1 and 2 of Part 1) are used in the reaction. (2) After the addition of benzophenone to the mixture of...
What is the theoretical yield (in grams) and percent yield of your triphenylmethanol product in this...
What is the theoretical yield (in grams) and percent yield of your
triphenylmethanol product in this experiment? (Weight of
triphenylmethanol: 0.060g)
BACKGROUND AND THEORY The Grignard reaction was one of the first organometallic reactions discovered and is still one of the most useful synthetically. By reacting an organohalide (usually a bromide) with magnesium in ethereal solvent, carbon becomes a nucleophile. Grignard reagents are the starting points for the syntheses of many alkanes, primary, secondary, and tertiary alcohols, alkenes, and carboxylic...
please find the purpse, Discussion, conclusion un 27 Phoenix June 20 8:10 PM a 35AEXPERIMENT 35A...
please find the purpse, Discussion, conclusion
un 27 Phoenix June 20 8:10 PM a 35AEXPERIMENT 35A Triphenylmethanol PROCEDURE ether MgBr+ C-OH + MgBr(OH) OMgBr 0 Addct Addition of Benzophenone While the phenylmagnesium bromide solution is being heated and stirred under reflux, make a solution of 1.09 g benzophenone in 2 mL of anhrudrous ether in a 5-mL conical vial. Cap the vial until the reflux period is over. Once the Grignard reagent is cooled to room temperature, draw some of...
What is the purpose of extracting the aqueous layer two more
times with ether in step 5?
What is the purpose of washing the combined organic layers with
NaOH in step 6?
Thank you
Reaction 1: Nitration HNO3 NO2 + H2SO4, H20 NO2 toluene NO2 ortho meta para Procedure for Reaction 1: 1) To a stirred solution of 3 ml (44.7 mmoles) 67 % HNO3 in 3.75 mL of water, H2SO4 (9 mL) was slowly added at 10-15 °C. 2)...
.
Grignard Reagents and As (Addition, Nucleophil ic) Additions Magnesium metal spontaneously reduces organohalides via a succession transfers. This results in the Grignard 'insertion reaction, as proposed in the 1920s single electron Procedure t was only Part A: Preparation of the Glassyware and Magnesium successful in ether solvents, and failed utterly n hydrocarbons such as benzene. 1. The Grignard reagent camot form in the presence of water, and any water that it comes Mg (solid) into contact with immed iately...
i need help with post questions, thanks
Product Isolation After stirring the reaction for 5 minutes and allowing the reaction mixture to cool (the reaction can be exothermic), remove the Claisen head from the conical vial. Slowly add 3 M HCl(aq) drop-wise. The solid may need to be broken up with a stirring rod or a pipet. Continue to add acid until the aqueous phase (bottom layer) tests positive with pH paper. Extractions can be done using the conical funnel...
Why did you wash the ether solution with sodium bicarbonate? Write chemical equations for the reactions that took place. b. At which purification steps was the unreacted methanol removed in the reaction? Some of it may have been removed in more than one place. c. Three-Step Synthesis of Methyl Anisate (Step 3) 0 CHOH. Н.so, cat.) Wear gloves. Methanol is poisonous. Ether is an anesthetic, so don't breathe it. Sulfuric acid is a strong corrosive acid. Wash any you spill...
please answer the prelab excercise:) I tried doing it but I did not
get very far
Experiment 7: Grignard Reaction. Introduction Discovered by French chemist Victor Grignard, the reaction that now bears his name is an example of the preparation of an organometallic reagent. In this lab, phenylmagnesium bromide is the Grignard of interest, and it will be added to an aldehyde to produce an alcohol. Lab Objectives 1. To study organometallic reagents in general. benzophenone. 2. To prepare phenylmagnesium...
using pictures and a maximum of 10 words, explain why an oven-dried
5-ml conical vial and drying tube(step 1 and 2 of part 1) are used
in the reaction. do both please! also the notebook pages are the
procedure
(1) Using pictures and a maximum of 10 words, explain why an oven-dried 5-ml conical vial and drying tube (step 1 and 2 of Part 1) are used in the reaction. (2) After the addition of benzophenone to the mixture of...
What is the theoretical yield (in grams) and percent yield of your
triphenylmethanol product in this experiment? (Weight of
triphenylmethanol: 0.060g)
BACKGROUND AND THEORY The Grignard reaction was one of the first organometallic reactions discovered and is still one of the most useful synthetically. By reacting an organohalide (usually a bromide) with magnesium in ethereal solvent, carbon becomes a nucleophile. Grignard reagents are the starting points for the syntheses of many alkanes, primary, secondary, and tertiary alcohols, alkenes, and carboxylic...
please find the purpse, Discussion, conclusion
un 27 Phoenix June 20 8:10 PM a 35AEXPERIMENT 35A Triphenylmethanol PROCEDURE ether MgBr+ C-OH + MgBr(OH) OMgBr 0 Addct Addition of Benzophenone While the phenylmagnesium bromide solution is being heated and stirred under reflux, make a solution of 1.09 g benzophenone in 2 mL of anhrudrous ether in a 5-mL conical vial. Cap the vial until the reflux period is over. Once the Grignard reagent is cooled to room temperature, draw some of...
Most questions answered within 3 hours.
-
On May 1, First Bank perfected a security interest in Debtor’s
inventory. On June 1, Bob...
asked 33 minutes ago -
A new kind of typhoid shot is being developed by a medical
research team. The old...
asked 2 hours ago -
Write a chemical equation for these reactions. (Use
the lowest possible whole number coefficients.) Include
states-of-matter...
asked 4 hours ago -
For each of the Z-scores below, determine two probabilities
(show four three decimal places): (1) the...
asked 4 hours ago -
Oxidative phosphorylation is achieved through chemiosmotic
coupling, which turns chemical energy into osmotic potential energy
that...
asked 7 hours ago -
Hollywood Shoes would like to maintain their cash account at a
minimum level of $64,000, but...
asked 7 hours ago -
Proteins CtrA-P, DnaA, and GcrA behave similarly to what
molecule in the Eukaryotic Cell Cycle?
asked 7 hours ago -
TRUE OR FALSE
In case of a competitive tender procedure, in the request for
quotation, the...
asked 7 hours ago -
I am a little behind please provide some explanation, will
provide thumbs up.
This question considers...
asked 7 hours ago -
Let say the utility function as U(X,Y) = lnX + Y. Show that the
marginal rate...
asked 7 hours ago -
A current of I=8.0A is flowing in a typical extension cord of
length L=3.00m. The cord...
asked 7 hours ago -
1. When balancing the equation H2SO4 (aq) + NaOH (aq) →
Na2SO4(aq) + H2O(aq), would you...
asked 8 hours ago