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What two methods could be used to purify the dimethyl fumarate? Based on the 12 Principles...

What two methods could be used to purify the dimethyl fumarate?

Based on the 12 Principles of Green Chemistry posted in the Green Chemistry Module, list 3 principles that are used in this experiment. The experiment: Isomers and Isomerization
B: Isomerization of Dimethyl Maleate

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Answer #1

ANS:- purification of Dimethyl fumrate

1. it can be washed with ethanol ,ethanol dissolve all its impurities and purified product will filter out..

method :-

  • take 100 gm Dimethyl Fumrate in 500 ml beaker .
  • add 200 ml ethanol and stirrer with glass rod
  • and filter
  • add 200 ml ethanol more in filtered dimethyle fumrate
  • stirrer,filter and evaporate methanol to dry.
  • pure product collect.

2.it can be purified by flash chromatography.

method:-

  • mobile phase - methanol water ratio 70 : 30
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