4-aminophenol (1.0 g) was dissolved in an inert organic solvent. Pyridine (1.50 mL) and acetyl ch...
4-aminophenol (1.0 g) was dissolved in an inert organic solvent. Pyridine (1.50 mL) and acetyl chloride (1.40 mL) were added, and the reaction was stirred until determined to be complete by TLC. Afteworkupup and purification, you isolated 1.40 g of a product. The experimental melting point was 155 oC, and mass spec analysis indicated that the molecular weight of this product is 193.20 g mol─1. What is the structure of the isolated product? Suggest a specific procedural modification that would allow you to synthesize acetaminophen using the same reagents as above.
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![久hCt Acerylcbide OH arinopRenol CRlonde cedure: Acefc.ocid Pora cetano] Scanned with CamScanner](http://img.homeworklib.com/images/f24f39bd-b40a-4ccf-9e71-b297fa9cc482.png?x-oss-process=image/resize,w_560)
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4-aminophenol (1.0 g) was dissolved in an inert organic solvent. Pyridine (1.50 mL) and acetyl ch...
The reaction was: 4-aminophenol + acetic anhydride + water (solvent) --> acetaminophen + acetic acid In...
The reaction was: 4-aminophenol + acetic anhydride + water
(solvent) --> acetaminophen + acetic acid
In this experiment, we characterize the products only by obtaining an experimental melting point. How could you use TLC to confirm that (i) your isolated product is pure, and (ii) your product is acetaminophen? [2 marks]
Need help, numbers 3-6 please show work. and fill out table of chemicals for all chemical...
Need help, numbers 3-6 please show work. and fill out table of
chemicals for all chemical used.
calculate mmol in the table as well show work please
and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
The reaction was: 4-aminophenol + acetic anhydride + water
(solvent) --> acetaminophen + acetic acid
In this experiment, we characterize the products only by obtaining an experimental melting point. How could you use TLC to confirm that (i) your isolated product is pure, and (ii) your product is acetaminophen? [2 marks]
Need help, numbers 3-6 please show work. and fill out table of
chemicals for all chemical used.
calculate mmol in the table as well show work please
and each of these must be listed in its own row. There are 10 column headings: IUPAC name OR common name, structure, CAS number (Chemical Abstract Service number) molecular mass, melting point (if applicable), boiling point (if applicable), solubility (in water, if applicable), density, amounts to be used in the experiment, and the...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
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