O. 218.188 10 [rel] Environment Chemical Shift Multiplicity Integration Hydrogen (ppm) нь Hc Hd He
Draw a H NMR spectrum for each compound. Pay attention to the chemical shift (ppm) multiplicity, and integration of each peak. The boxes indicate where the peaks should go (which ppm range) as well as the relative height of each peak OH PPM O 3 PPM -2. H 10 8 PPM
Нь He Ha -CEC Hd a) Given that the 'H NMR spectrum was acquired at 300 MHz, convert the ppm values for the alkenyl region to Hz and provide the cis proton coupling constant to 1 decimal place. b) Please provide the chemical shift values for Он i) Both alkyne carbons ii) The aromatic carbon bearing the substituent ili)H vi) H v) He iv) H H NMR spectrum 7.50 745 740 7.35 6.0 58 S.6 n (ppm) S4 52 75...
What is the 'H NMR chemical shift value (in ppm) of the indicated hydrogen? 0 O 4.2 5.2 none of these 6.2
NMR, please help.
16) Chemical Formula: C,H,O, IR: strong peak 1720cm-1 PPM mple A4 thouis Yoo 05 quadret 1:2:2:1 Triplet 1:3:1 244 PPM USER: -- DATE: 04/12/10 08:27 PTS1d: 4096 Nuts - A4 OF1: 372.1 010 AlglobalVZGH.ppg SWI: 1000 PW: 19.6 us PD: 3.0 sec NA LB: 0.0 (ethylacetate) H3C CH₂ - CH3 C4H8O₂ 2. PROTON MAGNETIC RESONANCE SPECTRAL DATA Complete the table below by listing the chemical shiits of all of the signal patterns in the nmr spectrum of...
Evaluate and investigate the
following IR Spectrum and 1H
NMR Spectrum. Identify the most important
peaks and correlate the results as much
as you can from the obtained product in the multi-step
synthesis of ethyl acetoacetate. This is Product
C from this multi-step synthesis where Product
B was identified as in the figure below and as such,
identify what product can be obtained after the synthesis
from the spectra provided. Use the template below in analysing the
spectra.
Figure 1...
Please help identify conpound
Sample A8 PPM DATE: 04/12/10 (09:15) AB FIR 60.010 SWI: 1000 PW: 19.6 OF 1: 368.7 USER: PTSid: 8192 EX: HIV.ppg PD: 3.0 sec INAS Nutstemp 1605 3064 486 %Transmittance 2874 556 2895 746 3028 2932 1453 1496 269 772 3500 3000 1500 1000 500 2500 2000 Wavenumbers (cm-1) Date: Fri Oct 29 11:30:24 2010 (GMT-07:00) AB KBr Scans: 16 Resolution: 2.000 Name Organic Chemistry 2242 Spectroscopy Unknown A (S-05) During this lab period, you are...
please need help with all the questions and ASAP, thank you
11. Please predict the principle organic product of the following reactions, show stereochemistry where appropriate. Note that some reactions involve isotope-labeled compounds, in those cases the correct isotope must be used. (66') 1. LIAID 2. H,O (1) 18 1) THF (2). CH3Li + 2) HaO NaBH4 (3) CH3OD H2(excess)/Pt (4) d herd (5). - Mg Br D2O diethyl ether Br +Li (6) diethyl ether LICu(CH2CHs)2 Br (7). 1. diethyl...
Evaluate and investigate the
following IR Spectrum, 13C NMR Spectrum
and 1H NMR Spectrum. Identify
the most important peaks and correlate the
results as much as you can from the obtained product in
the multi-step synthesis of ethyl acetoacetate.
This is Product E from this multi-step synthesis
where Product C was identified as in the figure
below and as such, identify what product can be obtained
after the synthesis from the spectra provided. Use the template
below in analysing the...
Can someone help with the analysis of this NMR spectrum for the
synthesis of benzyl methyl ether. (Benzyl chloride, diethyl ether
and then added sodium methoxide to produce benzyl methyl
ether)?
What I have so far is:
4 different protons:
3 x 1H on the benzene ring, doublet
2 x 1H on benzene ring, either side of O, doublet
2H on Carbon beside O, quartet
3H on end of alkene with O, triplet
I don't understand where they match up...
Please complete for Tuesday, we will go through the questions and mark them in class. pg 156 - 4.23, 4.24, 4.26 pg 170 - 4.29, 4.31, pg 171-4.36 pg 175 - 4.59 pg 176- 4.74, 4.75, 4.80 pg 177-4.81, 4.82 pg 188- 5.1, 5.4, 5.5, 5.6, 5.11 - Using Table 5.1 pg 198-5.22, 5.25 pg 203 - 5.29 pg 206 - 5.37 pg 209 - 5.39 pg 2.14 5.61 pg 235-6.11, 6.14, 6.16 156 CHAPTER 4 Introduction to Organic Compounds...