HW4. A student ran a reaction and obtained the following data for an unknown by-product C that contains...
NMR and IR The 'H NMR for the unknown C: O 70 70 20 85 60 15 20 30 30 25 20 10 % pom Proton peak Integration Chemical Shift (ppm) Neighbors (n) Splitting pattern (n+1) report as singlet/doublet/tripletete 12 3.4 C must be an aliphatic alcohol. There is a strong O-H stretch in the IR and zero degrees of unsaturation. The remaining structure is determined by 'H NMR. (e) Predicted Structure C (label hydrogens with letter for assignment below):...
NMR & IR post lab question help! NMR and IR 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 ppm IH The 'H NMR for the unknown C: 20 7.5 7.0 6.5 6.0 6.5 5.0 4.5 4.0 3.5 3.0 25 20 519 05 Proton peak Integration Chemical Shift (ppm) Neighbors (m) Splitting pattern (+1) report as singlet/doublettripletlets. C must be an aliphatic alcohol. There is a strong O-H stretch in the IR and zero degrees of unsaturation. The remaining structure...
Liquid Extraction NMR and IR The 'H NMR for the unknown C: 8.0 7.5 7.0 6.5 6.0 5.5 5.0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 ppm Proton peak Integration Neighbors (n) Chemical Shift (ppm) Splitting pattern (n+1) (report as singlet/doublet/triplet/ete. 9 b. C must be an aliphatic alcohol. There is a strong O-H stretch in the IR and zero degrees of unsaturation. The remaining structure is determined by 'H NMR. (c) Predicted Structure C (label hydrogens with...
NMRR The 'H NMR for the unknown 0.0 7.5 7.0 6.5 6.0 5 5 .0 4.5 4.0 3.5 3.0 2.5 2.0 1.5 1.0 0.5 ppm Proton peak Integration Chemical Shift Neighbors (A) Splitting pattern (+1) (report as singlet/doublet/tripletlete. (היי C must be an aliphatic alcohol. There is a strong O-H stretch in the IR and zero degrees of unsaturation. The remaining structure is determined by 'H NMR. (6) Predicted Structure C (label hydrogens with letter for assignment below):
2. The H NMR spectrum of an unknown compound with the molecular formula CgH902 is provided below. The IR spectrum for this compound shows a large, broad peak at 3147 cm ? and a strong, sharp peak at 1645 cm-7. Provide a structure for this unknown. 2H 2H 10 98 HSP-06-318 ppm
I am trying to find the compound? If it is unknown what compound is it? i need to find the compound from the given spectrum Unknown #315-S20-2 Mol. Wt. = 181.0 g/mol C = 33.17% H=5.01% 0 = 17.68% Mass Spectrum IR S 100- HS-1W-2525 A M = 101 Relative Intensity TEMETTRE o proti temperaturniejowerpoi 25 50 75 100 125 m/ n 150 t 175 Based on the M.W., circle & label the molecular ion peak (M). Spec Regie From...
Unknown 315-S20-2 Can someone help me fill out the table on the right side please IR Spectrum: Unknown # 315-S20-2 Mol. Wt. = 181.0 g/mol C-33.17% H=5.01% 0 = 17.68% Molecular Formula Degree of Unsaturation = Mass Spectrum IR spectrum (liquid film) 100- Relative Intensity 150 175 25 50 75 100 125 m/z Based on the M.W., circle & label the molecular ion peak (M). Spectrum Region Frequency (cm ) Peak Shape (sharp, broad) MAVUTO Peak Intensity (strong, med., weak)...
Unknown H415 100 50 1000 1S00 2000 3000 BRVENUMBERI 4000 Unknown H415 ЗН 1 H-N 2H, q 1H, d 5H, m 1H, d 0 1 2 3 6 7 8 10 11 ppm HSP-00-049 Unknown H415 q 140 120 100 200 180 160 ppm CDS-00-726 20 -40 60 80 Relative Intensity 09 Unknown H415 100 MS-NJ-0442 80 20 thmpt 25 50 75 100 125 150 175 m/z Date: Name: Section/Group: Instructor: Report Sheet: Laboratory 14 MS,IR, 13C NMR, and 'H...
In this NMR handout, you will get practice interpreting NMR spectra. Refer to the NMR tutorial/theory for chemical shifts and descriptions of peak splitting. There are 4 NMR problems. For each problem, you have been given the chemical formula as well as the IR and NMR spectra. Draw the structure for each unknown compound and provide sufficient reasoning as to why you think it has that structure. To get full credit, determine the structure of the unknown compound, calculate the...
Choices: degrees of saturation: 0,1, 2, or, 3 Cardi B prepares compound D according the scheme below. Cardi B enjoys the odor of compound D, which recalls the refreshing sting of ammonia or other disinfectant. SOCI 2 equiv NH LIAIH Compound A CeH1202 Compound C CgH13NO Compound D Compound B H2O Though Cardi is unwilling to provide you with the identity of D, she has provided the molecular formula and IR data of compound A and the molecula formula and...