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help please An extraction was performed using mixture of the compounds below. First the organic mixture...
An extraction was performed using mixture of the compounds below. First the organic mixture was dissolved...
An extraction was performed using mixture of the compounds below. First the organic mixture was dissolved in dichloromethane, treated with acid, and separated. The organic layer was then treated with base and separated. Sort the compounds based which layer it was in at the end of the extraction Acidic Aqueous Layer Basic Aqueous Layer Organic Layer Only
A mixture containing 1, 3, 5-trimcthoxybcnzcnc (A), phenol (B), aniline (C) and 1-naphthoic acid (D) was...
A mixture containing 1, 3, 5-trimcthoxybcnzcnc (A), phenol (B), aniline (C) and 1-naphthoic acid (D) was dissolved in dichloromethane. Next two extractions were performed first using HC1 then with NaOH. Which of the compounds could not be separated in this procedure. Explain and show the pertinent reaction equation/s. student wanted to separate a mixture of benzoic acid and aniline that were dissolved in ethanol. Could the student separate the two compounds using a base extraction (NaOH)? Explain
A mixture of compounds containing dimethylamine, phenol, ammonia, and acetic acid is separated using liquid-liquid extraction...
A mixture of compounds containing dimethylamine, phenol, ammonia, and acetic acid is separated using liquid-liquid extraction as follows: Step 1: Concentrated HCl is added followed by draining the aqueous layer. Step 2: Dilute NaOH is added to the organic layer followed by draining the aqueous layer. Step 3: Concentrated NaOH is added to the organic layer followed by draining the aqueous layer. Which compound would you expect to be extracted into the aqueous layer after the addition of dilute NaOH,...
Acid/Base Extraction 1. Provide a flow chart detailing the acid/base extraction/separation of the compounds shown below....
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in diethyl ether. We separated the basic component by adding 3M HCl, we separated the acidic component by adding 3M NaOH. I don't understand what happens here. To isolate the acidic solution, we added 6 M NaOH and used the vacuum to recover the solid. To isolate the basic solution we added...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so...
The Separation of Three Organic Compounds by Acid, Base Reactions and Liquid, Liquid Extraction. Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in methyleene chloride. We separated the basic component by adding 3M HCl, we separated the acidic component by adding 3M NaOH. I don't understand what happens here. To isolate the acidic solution, we added 6 M NaOH and used the vacuum to recover the solid. To isolate the basic solution we added...
Propose an extraction scheme to separate the mixture of following compounds shown below: (5 pts) ...
question regarding separation using acid-base
extraction lab
Propose an extraction scheme to separate the mixture of following compounds shown below: (5 pts) COOH Br and
Propose an extraction scheme to separate the mixture of following compounds shown below: (5 pts) COOH Br and
A liquid-liquid extraction is performed according to the schematic below. Which compound(s) should we expect to...
A liquid-liquid extraction is performed according to the schematic below. Which compound(s) should we expect to find in layer B? You can assume 100% of each compound is separated into its respective layer. benzoic acid diethyl ether biphenyl 5% NaOH (aq) Aqueous Organic Layer A 6 M HCl(aq) Aqueous Organic Layers C & D secondom i Vacuum Filtration Benzoic Acid
Liquid-Liquid Extraction P14. Your instructor gives you 1g of a 50:50 mixture of the following solids...
Liquid-Liquid Extraction P14. Your instructor gives you 1g of a 50:50 mixture of the following solids and asks you to separate them from one another. First you dissolve the mixture in ether: methyl trains-cinnamate OH trans-cinnamic acid OMe mp 34-38°c mp 133°C Using what you learned in P11-P12, complete the extraction plan below (aqueous acid or base should be added?): Aqueous solution of added Top layer: circle one (aqueous or organic?) Bottom layer: circle one (aqueous or organic?) Beaker compounds...
An extraction was performed using mixture of the compounds below. First the organic mixture was dissolved in dichloromethane, treated with acid, and separated. The organic layer was then treated with base and separated. Sort the compounds based which layer it was in at the end of the extraction Acidic Aqueous Layer Basic Aqueous Layer Organic Layer Only
A mixture containing 1, 3, 5-trimcthoxybcnzcnc (A), phenol (B), aniline (C) and 1-naphthoic acid (D) was dissolved in dichloromethane. Next two extractions were performed first using HC1 then with NaOH. Which of the compounds could not be separated in this procedure. Explain and show the pertinent reaction equation/s. student wanted to separate a mixture of benzoic acid and aniline that were dissolved in ethanol. Could the student separate the two compounds using a base extraction (NaOH)? Explain
A mixture of compounds containing dimethylamine, phenol, ammonia, and acetic acid is separated using liquid-liquid extraction as follows: Step 1: Concentrated HCl is added followed by draining the aqueous layer. Step 2: Dilute NaOH is added to the organic layer followed by draining the aqueous layer. Step 3: Concentrated NaOH is added to the organic layer followed by draining the aqueous layer. Which compound would you expect to be extracted into the aqueous layer after the addition of dilute NaOH,...
Acid/Base Extraction
1. Provide a flow chart detailing the acid/base
extraction/separation of the compounds shown below. Your answer
must employ the following reagents: methylene chloride,
hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M),
10% sodium bicarbonate (aq). Clearly indicate the product(s) and
layers formed following each step of your separation scheme.
IMPORTANT: p-cresol is soluble in sodium hydroxide solution but
insoluble in neutral water or sodium bicarbonate solution. 2-
ethylbenzoic acid is soluble in both sodium hydroxide and...
Provide a flow chart detailing the acid/base extraction/separation of the compounds show below. Your answer must employ the following reagents: methylene chloride, hydrochloric acid (1M & 6M), sodium hydroxide (1M & 6M), 10% sodium bicarbonate (aq). Clearly indicate the product(s) and layers formed following each step of your separation scheme. IMPORTANT: p-cresol is soluble in sodium hydroxide solution but insoluble in neutral water or sodium bicarbonate solution. 2-ethylbenzoic acid is soluble in both sodium hydroxide and sodium bicarbonate solutions. Use...
question regarding separation using acid-base
extraction lab
Propose an extraction scheme to separate the mixture of following compounds shown below: (5 pts) COOH Br and
Propose an extraction scheme to separate the mixture of following compounds shown below: (5 pts) COOH Br and
A liquid-liquid extraction is performed according to the schematic below. Which compound(s) should we expect to find in layer B? You can assume 100% of each compound is separated into its respective layer. benzoic acid diethyl ether biphenyl 5% NaOH (aq) Aqueous Organic Layer A 6 M HCl(aq) Aqueous Organic Layers C & D secondom i Vacuum Filtration Benzoic Acid
Liquid-Liquid Extraction P14. Your instructor gives you 1g of a 50:50 mixture of the following solids and asks you to separate them from one another. First you dissolve the mixture in ether: methyl trains-cinnamate OH trans-cinnamic acid OMe mp 34-38°c mp 133°C Using what you learned in P11-P12, complete the extraction plan below (aqueous acid or base should be added?): Aqueous solution of added Top layer: circle one (aqueous or organic?) Bottom layer: circle one (aqueous or organic?) Beaker compounds...
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