When determining the melting point of your pure benzophenone, some of the molten material had solidified...
Homework Answers
When the molecular weight of the unknown(mixture of pure substance and impurity) is determined, the melting point depends on amount of impurity present.
The freezing or melting point depression is directly proportional to the molality of the substance dissolved.
Or the molecular weight calculated using the melting point is directly proportional to mass of substance present.
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When determining the melting point of your pure benzophenone, some of the molten material had solidified...
How would your calculated value for the molecular weight of your unknown been affected (high, low,...
How would your calculated value for the molecular weight of your unknown been affected (high, low, no effect) if a small quantity of the unknown stuck to the metal stirring rod and failed to dissolve in the benzophenone?
A Freezing-Point Depression experiment is done using 2 different test tubes to find the molecular weight...
A Freezing-Point Depression experiment is done using 2 different test tubes to find the molecular weight of an unknown mixture. Tube 1 consists of pure Lauric acid, and Tube 2 consists of Lauric acid + an unknown solute mixture. From the calculations of this experiment, the molecular weight of the unknown acid can be found. A) How would the loss of some Lauric acid from Test Tube 1 have affected the calculation of a molecular weight? Would the calculated molecular...
Date Name Lab Section Partner(s) Determination of Molar Mass by Freezing Point Depression Data: Mass of...
Date Name Lab Section Partner(s) Determination of Molar Mass by Freezing Point Depression Data: Mass of empty test tube 2.2.6! Mass of test tube plus approximately 10.0 g of benzophenone 33.39 The difference is the mass of benzophenone (solvent) 8 kg Mass of unknown (-1.0 g) 1:09: 48.50°c 42.08. Freezing point of pure benzophenone Freezing point of benzophenone containing the unknown The difference is A fp CO Calculations: (Show set-up with cancellation of units) 1. molality of solution 2. moles...
Question 14 The melting point of a pure compound is known to be 110-111º. Describe the...
Question 14 The melting point of a pure compound is known to be 110-111º. Describe the melting behavior expected if this compound is contaminated with 5% of an impurity. 90-96 111-113 90-91 110-111 5 pts Question 15 You and your lab partner take melting points of the same sample. You observe a melting point of 101-107°C, while your partner observes a value of 110-112°C. Explain how you can get two different values with exactly the same sample. One of the...
Grignard Reaction 1. Draw your complete reaction, including the formation of the Grignard reagent and the...
Grignard Reaction 1. Draw your complete reaction, including the formation of the Grignard reagent and the reaction with your carbonyl compound. Below each reagent, write its molecular weight and density (if a liquid). Also write how much of each material you will use in ml (if liquid), grams, and moles. Also include the molecular weight and melting point of your final product. 2. How many moles of Grignard reagent are you synthesizing? What mass of water could fully react with...
Separating a Mixture, Recrystallization, pre-lab assignment could you also explain why you chose that substance for...
Separating a Mixture, Recrystallization, pre-lab
assignment
could you also explain why you chose that substance for the empty
spaces and question marks
EXPERIMENT 4 Pre-Lab Assignment Separating a Mixture, Recrystalliration Name Date 1. Complete the following flowchart which shows how to separate a mixture of sand, sodium chloride and acetanilide. Notice that after a separation process (a down arrow) the filtered solids are shown on the left and the filtrate (the liquid) is shown on the right. The terminal step...
What is the theoretical yield (in grams) and percent yield of your triphenylmethanol product in this...
What is the theoretical yield (in grams) and percent yield of your
triphenylmethanol product in this experiment? (Weight of
triphenylmethanol: 0.060g)
BACKGROUND AND THEORY The Grignard reaction was one of the first organometallic reactions discovered and is still one of the most useful synthetically. By reacting an organohalide (usually a bromide) with magnesium in ethereal solvent, carbon becomes a nucleophile. Grignard reagents are the starting points for the syntheses of many alkanes, primary, secondary, and tertiary alcohols, alkenes, and carboxylic...
Process A. Preparation of 4-t-butylcyclohexene Assembling the equipment Fill the almost complete sand bath, place it...
Process A. Preparation of 4-t-butylcyclohexene Assembling the equipment Fill the almost complete sand bath, place it on the base of the shelf, fix the thermometer with a clip and start heating until the temperature of the sand is - 110C. B. Mixing the reagents Using the plastic funnel, introduce 0.60-0.70 g of 4-t-butylcyclohexanol into a large, clean, dry test tube. Then add 10 drops of concentrated phosphoric acid, 3 drops of concentrated sulfuric acid and a pebble to moderate boiling....
CODE 102_8 Welding Many welding processes require the application of heat and/or pressure to produce a...
CODE 102_8 Welding Many welding processes require the application of heat and/or pressure to produce a suitable bond between the two parts being joined. There are a number of conventional and commercially practiced welding processes, which possess limitations in relation to material type and thickness, and in addition, the cost analysis may not allow for a process to be used on a specific application. The selection of suitable welding consumable (electrode or wire) is also an important factor in producing...
Pre-Laboratory Exercise: Plastics Identification I. List four properties that you will use in lab...
can
someone help me find this information?
Pre-Laboratory Exercise: Plastics Identification I. List four properties that you will use in lab to determine the identity of the polymer samples 2. Describe the density test. What observation will help you determine the density of each polymer? What precautions should be taken in placing the sample in the solutions? 3. Write the name and abbreviation for the six recyclable polymers 2 huetn deisity polyetayene.HDpz poulene: PP 4. Given the list of wavenumber...
Date Name Lab Section Partner(s) Determination of Molar Mass by Freezing Point Depression Data: Mass of empty test tube 2.2.6! Mass of test tube plus approximately 10.0 g of benzophenone 33.39 The difference is the mass of benzophenone (solvent) 8 kg Mass of unknown (-1.0 g) 1:09: 48.50°c 42.08. Freezing point of pure benzophenone Freezing point of benzophenone containing the unknown The difference is A fp CO Calculations: (Show set-up with cancellation of units) 1. molality of solution 2. moles...
Question 14 The melting point of a pure compound is known to be 110-111º. Describe the melting behavior expected if this compound is contaminated with 5% of an impurity. 90-96 111-113 90-91 110-111 5 pts Question 15 You and your lab partner take melting points of the same sample. You observe a melting point of 101-107°C, while your partner observes a value of 110-112°C. Explain how you can get two different values with exactly the same sample. One of the...
Grignard Reaction 1. Draw your complete reaction, including the formation of the Grignard reagent and the reaction with your carbonyl compound. Below each reagent, write its molecular weight and density (if a liquid). Also write how much of each material you will use in ml (if liquid), grams, and moles. Also include the molecular weight and melting point of your final product. 2. How many moles of Grignard reagent are you synthesizing? What mass of water could fully react with...
Separating a Mixture, Recrystallization, pre-lab
assignment
could you also explain why you chose that substance for the empty
spaces and question marks
EXPERIMENT 4 Pre-Lab Assignment Separating a Mixture, Recrystalliration Name Date 1. Complete the following flowchart which shows how to separate a mixture of sand, sodium chloride and acetanilide. Notice that after a separation process (a down arrow) the filtered solids are shown on the left and the filtrate (the liquid) is shown on the right. The terminal step...
What is the theoretical yield (in grams) and percent yield of your
triphenylmethanol product in this experiment? (Weight of
triphenylmethanol: 0.060g)
BACKGROUND AND THEORY The Grignard reaction was one of the first organometallic reactions discovered and is still one of the most useful synthetically. By reacting an organohalide (usually a bromide) with magnesium in ethereal solvent, carbon becomes a nucleophile. Grignard reagents are the starting points for the syntheses of many alkanes, primary, secondary, and tertiary alcohols, alkenes, and carboxylic...
Process A. Preparation of 4-t-butylcyclohexene Assembling the equipment Fill the almost complete sand bath, place it on the base of the shelf, fix the thermometer with a clip and start heating until the temperature of the sand is - 110C. B. Mixing the reagents Using the plastic funnel, introduce 0.60-0.70 g of 4-t-butylcyclohexanol into a large, clean, dry test tube. Then add 10 drops of concentrated phosphoric acid, 3 drops of concentrated sulfuric acid and a pebble to moderate boiling....
CODE 102_8 Welding Many welding processes require the application of heat and/or pressure to produce a suitable bond between the two parts being joined. There are a number of conventional and commercially practiced welding processes, which possess limitations in relation to material type and thickness, and in addition, the cost analysis may not allow for a process to be used on a specific application. The selection of suitable welding consumable (electrode or wire) is also an important factor in producing...
can
someone help me find this information?
Pre-Laboratory Exercise: Plastics Identification I. List four properties that you will use in lab to determine the identity of the polymer samples 2. Describe the density test. What observation will help you determine the density of each polymer? What precautions should be taken in placing the sample in the solutions? 3. Write the name and abbreviation for the six recyclable polymers 2 huetn deisity polyetayene.HDpz poulene: PP 4. Given the list of wavenumber...
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