(a) Predict the 3IP NMR spectrum of |HPF5] (assuming a static structure) given that JpH = 939 Hz, ./PF(axiai) = 731 Hz and JPF(equatorial) 817 Hz.
(b) The [BiF7]2- and [SbFg]3- ions have pentagonal bipyramidal and octahedral structures, respectively. Are these observations consistent with the VSEPR model?
(c) Consider the following reaction scheme (K.O. Christe (1995) ./. Am. Chem. Soc., vol. 117, p. 6136):
Discuss the reaction scheme in terms of redox and Lewis acid-base chemistry. Comment on the structures of, and bonding in, the nitrogen- containing species in the scheme.
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