If
you like the answer please give a thumbs up ?.
As indicated early, the next step of our synthesis will be a Chlorination reaction. Just like...
We will also need a catalytic amount of AlCl3. For this we will use 0.1 equivalents of AlCl3. Question #26: How many mmoles of AlCl3 will be needed for our reaction? Round to the tenths place. mmol
After purification, this reaction yielded 5.6 g of product Question #20: Using the mmoles of benzene calculated earlier (55.8) and the molecular weight of the product (123 g/mol) predict the theoretical 100 % yield of the product in grams. Round to the tenths place. 6.9 Question #21: Using this number predict the experimental yield (reminder, the reaction produced 5.6 g of product.) Round to the nearest whole number.
Solution Stoichiometry: The next step in the lab is to carefully measure out 25.00 mL of the 0.250 M Na2CO3 solution, and 30.00 mL of the 0.200 M CaCl2 solution, and mix them together. Use Reaction Stoichiometry to predict the limiting reactant in the reaction, and the amount in grams of calcium carbonate that we expect to precipitate (theoretical yield). Remember: M= mols solute / L solution Use the following table to help organize your information. 0.250 M Na2CO3 00.200M...
Synthesis of crude product.
1. Combine reagents (following either step A or B, depending on the
benzaldehyde assigned to
you). It is best not to use a brand-new conical vial right out
of the package, as the surface is not rough enough to help induce
precipitation.
A. In a 5-mL conical vial, combine 0.15 g of 3-nitrobenzaldehyde
(151.121 g/mol), 0.12 mL
of acetophenone (120.151 g/mol; d = 1.03 g/mL), and 0.80 mL of
95% ethanol.
OR
B. Pipette 0.13 mL...
Just Answer Question 5
Synthesis of 2-chloro-2-methylbutane (literature version) Concentrated aqueous hydrochloric acid (HCI, 3.3 equivalents) was slowly added to 2-methyl-2-butanol (1.0 equivalents) in a 100 mL round bottom flask with stirring. The reaction was stirred for 15 minutes at room temperature. Upon completion, the reaction mixture was transferred to a 60 mL separatory funnel and the aqueous layer was removed. The organic layer (i.e. the product) was successively washed with: (1) saturated aqueous NaCl (brine), (2) saturated aqueous NaHCO,...
Question- The second step is a name reaction. a) What is its name: b) Is it OK that we left the reaction in our drawer over the week? What would have happened if we didn’t have a good seal on the stopper? Draw a possible reaction scheme. Background The field of medicinal chemistry combines the specialties of synthetic organic chemistry and biology, and biochemistry. Compounds are generated and biological activity is screened using target specific assays. . These assays are...
What is the objective of this experiment?
The reaction solvent for this experiment is xylene. What
property of this solvent makes it a better choice than toluene or
benzene?
Draw the orbitals involved in the 4+2 electrocyclization for
this reaction. Draw the structures of the reactants as best you
can. It may be appropriate to abbreviate the structure of
anthracene.
IR is not provided for this reaction product. Why is IR not
useful for monitoring the reaction or characterizing the...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
need help with the boxed bullet point. writing the chemical
reaction scheme for the experiment.
Synthesis of an Alkyl Halide: A Nucleophilic Substitution Reaction, Part I Pre-lab Assignment for Synthesis of an Alkyl Halide: A Nucleophilic Substitution Reaction, Part 1 1. From The Organic Chem Lab Survival Manual ( edition) by Zubrick • Review pages 201-204: Standard Reflux. • Review pages 127-140: Extraction • Review pages 164-189: Distillation, Simple Distillation. The Distillation Example, and The Distillation Mistake. 2. Read this...
Give a detailed mechanism for this reaction and give a separation
scheme
NUCLEOPHILIC ACYL SUBSTITUTION: Synthesis of an Ester Isoamyl acetate (Banana Oil) Purpose This experiment demonstrat and alcohol. The technique of refluxing the reaction mixture is introduced. es the procedure for the synthesis of an ester from a carboxylic acid Esters are an important functional group in organic chemistry, and esters are found widely distributed in nature. Many lower molecular weight esters are associated with natural fuit flavors and...