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Name: Hand this in for prelab assignment for the second week of this experiment (There is...
These questions are from an experiment where we had a mixture of Ferrocene, acetylferrocene and diacetyl...
These questions are from an experiment where we had a mixture of Ferrocene, acetylferrocene and diacetyl ferrocene and we separated each by using column chromatography. Before doing the column chromatography we did TLC analysis to ensure that we did, in fact, have a mixture of these 3 compounds. During the column chromatography we first eluted the ferrocene using pure hexane. Then we eluted the acetylferrocene using a 1:1 mixture of hexane and methylene chloride. Then we eluted the diacetylferrocene using...
Friedel-Crafts Acylation of Ferrocene "riedel-Crafts reactions are examples of electrophilic aromatic substitution reactions. The eaction involves...
Friedel-Crafts Acylation of Ferrocene "riedel-Crafts reactions are examples of electrophilic aromatic substitution reactions. The eaction involves the substitution of hydrogen on the aromatic ring system by an electrophilic arbon species forming a new carbon-carbon bond. Friedel-Crafts reactions may be used to ntroduce either an alkyl or acyl group. Ferrocene does not undergo addition reactions typical of cyclopentadiene, but undergoes Electrophilic aromatic substitution. The Friedel-Crafts acylation reaction of ferrocene involves he addition of the acylium cation to one of the carbon...
1. What is the purpose of column chromatography 2. What is the stationary phase? Mobile phase?...
1. What is the purpose of column chromatography 2. What is the stationary phase? Mobile phase? 3. What is the purpose of the cotton (glass wool) in column chromatography? 4. What is the purpose of the sand? 5. Why is it important to prevent the column from drying? 6. What can happen if you disrupt your even layer of silica gel? 7. Which compounds come off the column first, polar or nonpolar? 8. Keyon synthesized acetylferrocene (orange) in organic chemistry...
in FRIEDEL-CRAFTS ACYLATION AND COLUMN CHROMATOGRAPHY lab (2 pts) Amount of acetyl chloride used ____4______(drops) (each...
in FRIEDEL-CRAFTS ACYLATION AND COLUMN CHROMATOGRAPHY lab
(2 pts) Amount of acetyl chloride used ____4______(drops) (each
drop is 0.01 mL) _____2______(equivalents) Based on the amount of
ferrocene you began the Friedel-Crafts reaction with, determine the
percent yield of acetylferrocene, diacetylferrocene, and the
percent recovery of unreacted ferrocene (show work)
react by 0.100 g of ferrocene at beginning
got 0 g of ferrocene, 0.012g of diacetylferrocene , 0.017g of
acetylferrocene
REACTION PROCEDURE: To a 5 mL conical vial, add a spin...
Name:_ Post-Lab Questions You're the TA in an organic lab and the students are running a...
Name:_ Post-Lab Questions You're the TA in an organic lab and the students are running a column to separate the following compounds: methyl cinnamon trans-cinnamic acid HW 1. Student A calls you over and explains that after running his column and showing you the TLC of fractions 1-5 which only have one spot by UV. He combined these fractions, removed the solvent and took a melting point. He is worried something is wrong because he got 38°C and not 133°C....
Name:_ Post-Lab Questions You're the TA in an organic lab and the students are running a...
Name:_ Post-Lab Questions You're the TA in an organic lab and the students are running a column to separate the following compounds: methyl cinnamon trans-cinnamic acid HW 1. Student A calls you over and explains that after running his column and showing you the TLC of fractions 1-5 which only have one spot by UV. He combined these fractions, removed the solvent and took a melting point. He is worried something is wrong because he got 38°C and not 133°C....
Solutions Experiment 2 Prelab Assignment (Due before lab starts) Name Lab Day / Time 1. Indicate...
Solutions Experiment 2 Prelab Assignment (Due before lab starts) Name Lab Day / Time 1. Indicate which is the solvent and which is the solute in the following: Solvent Solute a. 50 mL H,O and 10 g sugar b. 150 ml H,0 and 50 mL isopropyl alcohol c. 150 mL H,0 and 250 mL isopropyl alcohol 2. Explain how stirring a solution would effect the rate of dissolving. 3. Explain how heating a solution would effect the rate of dissolving...
Hi can someone help me with my pre lab theory questions (1,2,3) on rate of elution...
Hi can someone help me with my pre lab theory questions (1,2,3)
on rate of elution or Rf? Here is some background below. Please
help explain as many as possible (1-3)! I dont really get the
relation ships in this lab, thank you!
1. What factors affect the rate of elution in organic compounds? 2. Explain what is the relationship between polarities of compounds (polar/non- polar compound) and rate of elution (Rf). 3. Explain what is the relationship between solvent...
In my organic chemistry lab we are performing a gas chromatography experiment and I need help...
In my organic chemistry lab we are performing a gas
chromatography experiment and I need help with our prelab
assignment, thanks!
Question 3 1 pts If compound A elutes (comes off) a GC column earlier than compound B in a temperature gradient GC run. What can be inferred about their respective boiling points? Compound A probably has a lower boiling point than that of compound B. Compound A and B have the same boiling point. Elution time does not correlate...
2. If two different compounds have the same Rr value, how might they be identified using paper chromatography?...
2. If two different compounds have the same Rr value, how might they be identified using paper chromatography? 3. Why is it important to keep the spots on the paper as small as possible? 4. If the solvent pool at the bottom of the beaker touched the spots on the 1.5cm line, what would happen to the spots? How would you address this error? 5. If you were teaching a student how to do paper chromatography, what three pieces of...
Friedel-Crafts Acylation of Ferrocene "riedel-Crafts reactions are examples of electrophilic aromatic substitution reactions. The eaction involves the substitution of hydrogen on the aromatic ring system by an electrophilic arbon species forming a new carbon-carbon bond. Friedel-Crafts reactions may be used to ntroduce either an alkyl or acyl group. Ferrocene does not undergo addition reactions typical of cyclopentadiene, but undergoes Electrophilic aromatic substitution. The Friedel-Crafts acylation reaction of ferrocene involves he addition of the acylium cation to one of the carbon...
1. What is the purpose of column chromatography 2. What is the stationary phase? Mobile phase? 3. What is the purpose of the cotton (glass wool) in column chromatography? 4. What is the purpose of the sand? 5. Why is it important to prevent the column from drying? 6. What can happen if you disrupt your even layer of silica gel? 7. Which compounds come off the column first, polar or nonpolar? 8. Keyon synthesized acetylferrocene (orange) in organic chemistry...
in FRIEDEL-CRAFTS ACYLATION AND COLUMN CHROMATOGRAPHY lab
(2 pts) Amount of acetyl chloride used ____4______(drops) (each
drop is 0.01 mL) _____2______(equivalents) Based on the amount of
ferrocene you began the Friedel-Crafts reaction with, determine the
percent yield of acetylferrocene, diacetylferrocene, and the
percent recovery of unreacted ferrocene (show work)
react by 0.100 g of ferrocene at beginning
got 0 g of ferrocene, 0.012g of diacetylferrocene , 0.017g of
acetylferrocene
REACTION PROCEDURE: To a 5 mL conical vial, add a spin...
Name:_ Post-Lab Questions You're the TA in an organic lab and the students are running a column to separate the following compounds: methyl cinnamon trans-cinnamic acid HW 1. Student A calls you over and explains that after running his column and showing you the TLC of fractions 1-5 which only have one spot by UV. He combined these fractions, removed the solvent and took a melting point. He is worried something is wrong because he got 38°C and not 133°C....
Name:_ Post-Lab Questions You're the TA in an organic lab and the students are running a column to separate the following compounds: methyl cinnamon trans-cinnamic acid HW 1. Student A calls you over and explains that after running his column and showing you the TLC of fractions 1-5 which only have one spot by UV. He combined these fractions, removed the solvent and took a melting point. He is worried something is wrong because he got 38°C and not 133°C....
Solutions Experiment 2 Prelab Assignment (Due before lab starts) Name Lab Day / Time 1. Indicate which is the solvent and which is the solute in the following: Solvent Solute a. 50 mL H,O and 10 g sugar b. 150 ml H,0 and 50 mL isopropyl alcohol c. 150 mL H,0 and 250 mL isopropyl alcohol 2. Explain how stirring a solution would effect the rate of dissolving. 3. Explain how heating a solution would effect the rate of dissolving...
Hi can someone help me with my pre lab theory questions (1,2,3)
on rate of elution or Rf? Here is some background below. Please
help explain as many as possible (1-3)! I dont really get the
relation ships in this lab, thank you!
1. What factors affect the rate of elution in organic compounds? 2. Explain what is the relationship between polarities of compounds (polar/non- polar compound) and rate of elution (Rf). 3. Explain what is the relationship between solvent...
In my organic chemistry lab we are performing a gas
chromatography experiment and I need help with our prelab
assignment, thanks!
Question 3 1 pts If compound A elutes (comes off) a GC column earlier than compound B in a temperature gradient GC run. What can be inferred about their respective boiling points? Compound A probably has a lower boiling point than that of compound B. Compound A and B have the same boiling point. Elution time does not correlate...
2. If two different compounds have the same Rr value, how might they be identified using paper chromatography? 3. Why is it important to keep the spots on the paper as small as possible? 4. If the solvent pool at the bottom of the beaker touched the spots on the 1.5cm line, what would happen to the spots? How would you address this error? 5. If you were teaching a student how to do paper chromatography, what three pieces of...
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