in FRIEDEL-CRAFTS ACYLATION AND COLUMN CHROMATOGRAPHY lab
(2 pts) Amount of acetyl chloride used ____4______(drops) (each drop is 0.01 mL) _____2______(equivalents) Based on the amount of ferrocene you began the Friedel-Crafts reaction with, determine the percent yield of acetylferrocene, diacetylferrocene, and the percent recovery of unreacted ferrocene (show work)
react by 0.100 g of ferrocene at beginning
got 0 g of ferrocene, 0.012g of diacetylferrocene , 0.017g of acetylferrocene
calculate no of moles of each of them i.e ferrocene, acetylferrocene,diacetylferrocene. then divide the each of the mole value with moles of ferrocene taken and multiply by 100 we get %
for calculating no of moles u need molweight
mol weight of ferrocene=186.03
mol weight of acetyl ferrocene=228.07
mol weight of diacetyl ferrocene=270.10
amount of ferrocene taken for reaction=0.1g=0.1/186.03=5.37*10-4moles
amount of aceyl ferrocene formed= 0.017/228.07=7.45*10-5 moles
amount of diacetyl ferrocene formed= 4.44*10-5moles
% yield of diacetyl ferrocene= 8.27%
% yield of acetyl ferrocene= 13.87%
in FRIEDEL-CRAFTS ACYLATION AND COLUMN CHROMATOGRAPHY lab (2 pts) Amount of acetyl chloride used ____4______(drops) (each...
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