numbers 3-5 please Those are the three equations given to us and that is the reaction...
3) Critical analysis (3 points) (a) Why did you have to heat this reaction to such an extreme temperature? Use the mechanism you drew as a hint (b) Which is the slow step - the first, or second? In this experiment, you will react the product you made in last week's experiment (meso-stilbene dibromide) with strong base in an elimination experiment. This reaction with yield an alkyne, diphenylacetylene. The strong base you will use is potassium hydroxide. The second step...
Chemical Table (4 pts): 1) Fill in the reaction table below. Make sure you correctly calculate the molar amounts of your reactants. name formula mol.-eq. Mw mmol amount Meso-Stilbene Dibromide 1.00 300 mg Potassium Hydroxide 5.7 290 mg Triethylene glycol 2 mL product 2) Potassium hydroxide is hygroscopic. Will it be easy to weigh exactly 290 mg? Will the exact amount of potassium hydroxide be critical to this reaction and why?
1st picture is the questions and the next two pictures are the experiment the questions are based off of Prelab Questions 1) Based on the Material Safety Data Sheets (MSDS) for the compounds, which of the compounds in this experiment is the most hazardous, and why? 2) Fill in the reagent table below. Make sure you correctly calculate the molar amounts of your materials. Name Formula Mol.-eq. Mw mmol Density/Conc. Amount 10 400 mg Meso-Stilbene Dibromide Potassium Hydroxide 5.75 Triethylene...
Pre-Lab Assignment 1) Draw the reaction mechanism for the reaction. 2) Determine the limiting reagent. Procedure 1 Place approximately 1 g of stilbene dibromide prepared in last week's experiment in a 50 mL round bottom flask. Record the exact mass. Add 0.8 g of KOH and 4 mL of triethylene glycol from the syringe provided in the fume hood (rinse any crystals from the sides of the flask while adding triethylene glycol). 2 Heat the stirred reaction mixture to a...
number 5 please EXPERIMENT 8: BROMINATION OF TRANS-STILBENE glacial acetic acid Objective: Execute first step of two-step sequence to transform an alkene into an alkyne via a dihalide intermediate and use infrared spectroscopy to identify functional groups 5. Identify the limiting reagent for the reaction and explain why it is the limiting reagent. PLEASE NOTE: You will need to draw out a Table of Reagents in your notebook to ensure that you know how many moles of each reagent you...
number 5 please EXPERIMENT 8: BROMINATION OF TRANS-STILBENE Br3 Br glacial acetic acid Br Objective: Execute first step of two-step sequence to transform an alkene into an alkyne via a dihalide intermediate and use infrared spectros copy to identify functional groups 5. Identify the limiting reagent for the reaction and explain why it is the limiting reagent. PLEASE NOTE: You will need to draw out a Table of Reagents in your notebook to ensure that you know how many moles...
here is the procedure if needed EXPERIMENT 8: BROMINATION OF TRANS-STILBENE glacial acetic acid Objective: Execute first step of two-step sequence to transform an alkene into an alkyne via a dihalide intermediate and use infrared spectroscopy to identify functional groups PRELAB NOTEBOOK: In the laboratory notebook, write the overall experimental objective, chemical equation(s), reaction mechanism (consider all possible stereoisomers), draw a diagram or outline of the procedural steps, and complete the chemical safety table for all chemicals. 1. Why is...
CHEM 2001 Exp post lab Staple this to the post lab grade sheet... 5. Calculate the theoretical yield for this reaction using measurements from procedure. 6. If you obtained an actual yield of 0.57g. what is the yield? 7. What IR absorptions do you expect for the starting material (only in the functional group reg 4000cm to 1500cm)? 8. What IR absorptions do you expect for the product (only in the functional group region 4000cm 1500cm-')? to 9. If you...
Please answer the following questions/fill in the data tables based on the following experiment. EXPERIMENTAL PROCEDURE: Place sodium hydroxide (2.500 g) in a 100 mL Erlenmeyer flask and add water (25.0 mL) and ethanol (20.0 mL). Add a magnetic stirrer bar and stir until all the NaOH has dissolved. To a second reaction vessel, add benzaldehyde (2.650 g, 0.025 mol) and acetone (0.725 g, 0.0125 mol). Add approximately half of the aldehyde-ketone solution to the sodium hydroxide solution, and stir...
Determine the theoretical yield and limiting reagent Running the Reaction Add 0.100 g benzil and 0.30 mL 95% ethanol to a 3-mL conical vial. Place a spin vane in the vial and attach an air condenser. Heat the mixture with an aluminum block (90-100°C) while stirring until the benzil has dissolved (see inset in Tech- nique 6, Figure 6.1A). Using a 9-inch Pasteur pipette, add dropwise 0.25 mL of an aqueous potassium hydroxide solution' downward through the condenser into the...