Homework Answers
The above reaction is Wittig reaction. In which first step comprises of formation of phosphorous ylide. In second step this ylide reacts with 9-anthranaldehyde to form trans product.
Theoratical yield = (Mole. Wt. (Product)/Mole.Wt. (Reactant)) x Quantity of Reactant(g).
= (280.36/206.24) x 0.23 = 0.312g
Since your practical weight is too high, your product may contain impurities like excess reagent or triphenyl phosphonium salt. It will give quantitative yield.
Practical Yield = Wt. (Practical)/Wt.(Theoratical) x 100
= (0.87/0.312) x 100 = 278.8%
Add Answer to:
tthe weight of my product is 0.87 g and they gave me the
density! how can...
what would be the percent yield if the final weight of my product is 0.1357g this...
what would be the percent yield if the final weight of my product
is 0.1357g this is a green chemistry wittig reaction to produce
1,4-diphenyl-1,3-butadiene from benzyltriphenylphosphonium chloride
and trans- cinnamaledyde using sodium hydroxide as the base
You will be using a Green Chemistry Wittig reaction (NOT Wittig-Horner Emmons reaction) to produce 1,4-diphenyl-1,3-butadiene starting with benzyltriphenylphosphonium chloride and trans- cinnamaledyde using sodium hydroxide as the base. This reaction is considered a "green" reaction, because an aqueous solution will be used...
can someone explain to me what exactly is going on in this lab? like what does...
can
someone explain to me what exactly is going on in this lab? like
what does benzyltriphenylphosphonium chloride, trans-cinnamaldehyde
and water do ? why was NaOH used? we produced
1,4-diphenyl-1,3-butadiene
Procedure: Place 2.10 mmol benzyltriphenylphosphonium chloride (Calculate BEFORE you come to the lab and know how many grams you need!) and 2.00 mmol trans-cinnamaldehyde (Calculate BEFORE you come to the lab and know how many ml you need. Use the molecular weight and the density for your calculation.) in a...
1.) What side reactions occur during the following steps. 2.) How can the IR spectrum be...
1.)
What side reactions occur during the following steps.
2.) How can the IR spectrum be used to show that there is not
starting material left and the products are ketones?
3.) Describe the major differences and similarities between
the IR spectra of benzoin and benzil. Compare your IR spectrum with
those of benzoin and benzil.
Copper-Catalyzed Oxidation of Benzoin 1. Add a stir bar and 1.5 mL of glacial acetic acid, 0.250 g of NH4NO3 and 0.500 g of...
Please answer the following questions/fill in the data tables based on the following experiment. EXPERIMENTAL PROCEDURE:...
Please answer the following questions/fill in the data tables based on the following experiment. EXPERIMENTAL PROCEDURE: Place sodium hydroxide (2.500 g) in a 100 mL Erlenmeyer flask and add water (25.0 mL) and ethanol (20.0 mL). Add a magnetic stirrer bar and stir until all the NaOH has dissolved. To a second reaction vessel, add benzaldehyde (2.650 g, 0.025 mol) and acetone (0.725 g, 0.0125 mol). Add approximately half of the aldehyde-ketone solution to the sodium hydroxide solution, and stir...
What is the percent yield of the lab procedure below? my final weight of the product is 0.0519 g
what is the percent yield of the lab procedure below?
my final weight of the product is 0.0519 g
sure of the proper disposal methodl, properly Check with your laboratory insructor if you are PROCEDURE Be sure to dry the 5-mL reaction vial in the oven for at least twenty minutes. Water is experiment. this Preparation of the Ylide 1. Place 0.480 g of benzyltriphenylphosphonium chloride in a dry, 5-mlL reaction vial containing a magnetic spin vane Add 2 mL...
Please refer to the Aldol Condensation experiment in your lab manual (page 89) • Calculate the...
Please refer to the Aldol Condensation experiment in your lab manual (page 89) • Calculate the amounts of all chemicals needed in measurable amounts (i.e. grams or milliliters rather than moles.) • Determine the theoretical yield for the reaction. Mixture A: Prepare a solution of 5g of sodium hydroxide dissolved in Du and 40ml of ethanol at room temperature in a 250 ml Erlenmeyer flask. Mixture B: Mix 5.1 ml(5.31 g) of benzaldehyde (MW 106 g/mol; d = 1.04 g/ml)...
Can you explain how to find what is the theoretical yield, and the desired percent yield...
Can you explain how to find what is the theoretical yield, and
the desired percent yield of ethyl 4-nitrobenzoate?
1. Synthesis of ethyl 4-nitrobenzoate a) In a 50-ml round-bottom flask, weigh out 4-nitrobenzoic acid (0.85 g, 0.005 mol). Add to this 8 ml of absolute ethanol. Add boiling stones, and then bring this solution to the Lab Technologist. WATER OUT b) The Lab Technologist will deliver 1.2 ml of concentrated sulfuric acid to the mixture from the automatic pipette. [CAUTION,...
Based on the Wittig Reaction exp. below, please answer a) and b). In b) you can...
Based on the Wittig Reaction exp. below, please answer a) and
b). In b) you can disregard the part about the IR, just please
interpret and assign protons, shift values, which protons are for
which groups, etc on the HNMR. The % yield was 34%, and MP was
lower than expected (to assist with answering part a). This should
be all the information you need to answer the question.
HNMR
Discuss the percentage yield of the reaction. Explain and provide...
How do I find the theoretical masses of the elimination product and the addition product? The molecular weights are pro...
How do I find the theoretical masses of the elimination
product and the addition product? The molecular weights are
provided in table
Aldol Addition and Condensation Alm. You will perform two reactions, one of which is an aldol addition and one provides the aldol condensation product. Both procedures will be performed ALDOL ADDITION conditions ALDOL CONDENSATION MSDS - ME Reactants Table Reactant(s) 2-acetylpyridine 4-nitrobenzaldehyde methanol Sodium carbonate water MW Density BPMP D 11.12 12.04 USD ROISS 0.180 MW BP MP...
what is the theoretical yield and what is the percent yield? In a 125-mL Erlenmeyer flask...
what is the theoretical yield and what is the percent
yield?
In a 125-mL Erlenmeyer flask containing a magnetic stirring bar, mix 0.05 md benzaldehyde with the theoretical quantity of acetone, and add one-half the ture to a solution of 5 g of sodium hydroxide dissolved in 50 mL of water and 40 mL of ethanol at room temperature (<25°C). After 15 minutes of stirring ada remainder of the aldehyde-ketone mixture and rinse the container with a little ethanol to...
what would be the percent yield if the final weight of my product
is 0.1357g this is a green chemistry wittig reaction to produce
1,4-diphenyl-1,3-butadiene from benzyltriphenylphosphonium chloride
and trans- cinnamaledyde using sodium hydroxide as the base
You will be using a Green Chemistry Wittig reaction (NOT Wittig-Horner Emmons reaction) to produce 1,4-diphenyl-1,3-butadiene starting with benzyltriphenylphosphonium chloride and trans- cinnamaledyde using sodium hydroxide as the base. This reaction is considered a "green" reaction, because an aqueous solution will be used...
can
someone explain to me what exactly is going on in this lab? like
what does benzyltriphenylphosphonium chloride, trans-cinnamaldehyde
and water do ? why was NaOH used? we produced
1,4-diphenyl-1,3-butadiene
Procedure: Place 2.10 mmol benzyltriphenylphosphonium chloride (Calculate BEFORE you come to the lab and know how many grams you need!) and 2.00 mmol trans-cinnamaldehyde (Calculate BEFORE you come to the lab and know how many ml you need. Use the molecular weight and the density for your calculation.) in a...
1.)
What side reactions occur during the following steps.
2.) How can the IR spectrum be used to show that there is not
starting material left and the products are ketones?
3.) Describe the major differences and similarities between
the IR spectra of benzoin and benzil. Compare your IR spectrum with
those of benzoin and benzil.
Copper-Catalyzed Oxidation of Benzoin 1. Add a stir bar and 1.5 mL of glacial acetic acid, 0.250 g of NH4NO3 and 0.500 g of...
what is the percent yield of the lab procedure below?
my final weight of the product is 0.0519 g
sure of the proper disposal methodl, properly Check with your laboratory insructor if you are PROCEDURE Be sure to dry the 5-mL reaction vial in the oven for at least twenty minutes. Water is experiment. this Preparation of the Ylide 1. Place 0.480 g of benzyltriphenylphosphonium chloride in a dry, 5-mlL reaction vial containing a magnetic spin vane Add 2 mL...
Please refer to the Aldol Condensation experiment in your lab manual (page 89) • Calculate the amounts of all chemicals needed in measurable amounts (i.e. grams or milliliters rather than moles.) • Determine the theoretical yield for the reaction. Mixture A: Prepare a solution of 5g of sodium hydroxide dissolved in Du and 40ml of ethanol at room temperature in a 250 ml Erlenmeyer flask. Mixture B: Mix 5.1 ml(5.31 g) of benzaldehyde (MW 106 g/mol; d = 1.04 g/ml)...
Can you explain how to find what is the theoretical yield, and
the desired percent yield of ethyl 4-nitrobenzoate?
1. Synthesis of ethyl 4-nitrobenzoate a) In a 50-ml round-bottom flask, weigh out 4-nitrobenzoic acid (0.85 g, 0.005 mol). Add to this 8 ml of absolute ethanol. Add boiling stones, and then bring this solution to the Lab Technologist. WATER OUT b) The Lab Technologist will deliver 1.2 ml of concentrated sulfuric acid to the mixture from the automatic pipette. [CAUTION,...
Based on the Wittig Reaction exp. below, please answer a) and
b). In b) you can disregard the part about the IR, just please
interpret and assign protons, shift values, which protons are for
which groups, etc on the HNMR. The % yield was 34%, and MP was
lower than expected (to assist with answering part a). This should
be all the information you need to answer the question.
HNMR
Discuss the percentage yield of the reaction. Explain and provide...
How do I find the theoretical masses of the elimination
product and the addition product? The molecular weights are
provided in table
Aldol Addition and Condensation Alm. You will perform two reactions, one of which is an aldol addition and one provides the aldol condensation product. Both procedures will be performed ALDOL ADDITION conditions ALDOL CONDENSATION MSDS - ME Reactants Table Reactant(s) 2-acetylpyridine 4-nitrobenzaldehyde methanol Sodium carbonate water MW Density BPMP D 11.12 12.04 USD ROISS 0.180 MW BP MP...
what is the theoretical yield and what is the percent
yield?
In a 125-mL Erlenmeyer flask containing a magnetic stirring bar, mix 0.05 md benzaldehyde with the theoretical quantity of acetone, and add one-half the ture to a solution of 5 g of sodium hydroxide dissolved in 50 mL of water and 40 mL of ethanol at room temperature (<25°C). After 15 minutes of stirring ada remainder of the aldehyde-ketone mixture and rinse the container with a little ethanol to...
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