Based on the Wittig Reaction exp. below, please answer a) and
b). In b) you can disregard the part about the IR, just please
interpret and assign protons, shift values, which protons are for
which groups, etc on the HNMR. The % yield was 34%, and MP was
lower than expected (to assist with answering part a). This should
be all the information you need to answer the question.
HNMR
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Based on the Wittig Reaction exp. below, please answer a) and
b). In b) you can...
This is the Wittig reaction. Below I have the reaction performed. So first we have the...
This is the Wittig reaction. Below I have the reaction
performed. So first we have the IR of starting material and then
the product, all the peaks for all IR. Please identify the peaks in
all the IR. Please also explain the difference observed thank you!.
For this reaction an NMR is also performed, have to label the H NMR
based on the product formed also based on the values given have to
determine if the product was cis -9-2(...
1151 VCL 11-8: Claisen Condensation -1 For this assignment, the target compound that you should s...
1151 VCL 11-8: Claisen Condensation -1 For this assignment, the target compound that you should synthesize is methyl acetoacetate. This is another carbonyl addition variation. Examine the product and determine which ester is the nucleophile and which is the electrophile. Keep in mind the mechanism and that you need to acidify the intermediate in order to isolate a neutral product. Synthesis Procedures 1. Start Virtual ChemLab and select Claisen Condensation-I from the list of assignments in the electronic workbook. After...
can someone please tell me all the peaks bends etc in the first IR as well...
can someone please tell me all the peaks bends etc in the
first IR as well as the functional groups. also interpret the nmr
please
07- 04- Absorbanco (au) 0.1- 0+ 3000 3000 15 1000 500 2000 Frequency (wavenumbers) Figure 3. IR spectrum of the second intermediate, bis(2,4,5-trifluorophenyl)methanone (6). 753 701 10.5 10.0 9.5 9.0 8.5 8.0 7520 6.5 6.0 5.5 4.5 4.0 3.5 Com 50 3.0 2.5 2.0 1.5 1.0 0.5 indicator. Melting point analysis was performed using a...
EXPERIMENT 2A DIELS-ALDER REACTION OF ANTHRACENE REFERENCES Pavia et al (4/e): Tech. 6.1/6.2, 7.2-7.4 Klein (1/e)...
EXPERIMENT 2A DIELS-ALDER REACTION OF ANTHRACENE REFERENCES Pavia et al (4/e): Tech. 6.1/6.2, 7.2-7.4 Klein (1/e) pp. 784-792 EQUATION heat Diels-Alder Adduct 9,30-dihydroanthracene-9,10- endo-o B-seccinic anhydride mp 262264 PROCEDURE Place 0.200 grams of anthracene and an equal molar amount of maleic anhydride in 5 mL of xylenes in a 10-mL round-bottom flask with a magnetic stir bar. Attach a water-cooled condenser and reflux for 60 minutes. Allow the solution to cool to room temperature and then place the flask in...
What is the reaction product(s) of oleic acid & sodium methoxide? Show the structure(s). Part A:...
What is the reaction product(s) of oleic acid & sodium methoxide? Show the structure(s). Part A: Acid Catalyzed Fischer Esterification of Free Fatty Acids Add 20 mL of canola oil and a magnetic stir bar to a 125-mL Erlenmeyer flask, and place the flask on a magnetic stirring plate. Add 2–3 mL of methanol and up to three drops of concentrated sulfuric acid Perform this step with caution, as this is a strong acid! Immerse a thermometer into the reaction...
what would be the percent yield if the final weight of my product is 0.1357g this...
what would be the percent yield if the final weight of my product
is 0.1357g this is a green chemistry wittig reaction to produce
1,4-diphenyl-1,3-butadiene from benzyltriphenylphosphonium chloride
and trans- cinnamaledyde using sodium hydroxide as the base
You will be using a Green Chemistry Wittig reaction (NOT Wittig-Horner Emmons reaction) to produce 1,4-diphenyl-1,3-butadiene starting with benzyltriphenylphosphonium chloride and trans- cinnamaledyde using sodium hydroxide as the base. This reaction is considered a "green" reaction, because an aqueous solution will be used...
Only need help with 5,6,7 and mechanism FTIR and NMR Spectra After completing a reaction and...
Only need help with 5,6,7
and mechanism
FTIR and NMR Spectra After completing a reaction and working up the products, it is still necessary to confirm that the correct product was formed. The most common tools used for this analysis are Fourier Transform Infrared (FTIR) and Nuclear Magnetic Resonance (NMR) spectroscopy. In the virtual laboratory, 'H and C NMR spectra are available. Details on interpreting FTIR and NMR spectra are found in your textbook. Your instructor may or may not...
tthe weight of my product is 0.87 g and they gave me the density! how can...
tthe weight of my product is 0.87 g and they gave me the
density! how can i calculte the percent yield?
- Page < 8 > of 14 | 0 Data and Observations Weight of product: Melting range of product: Attach any spectra to your laboratory report Calculations and Graphs Calculate the percent yield. Keep in mind that the reagents may not be 100% pure; refer to labels on the containers. The density of 50% aqueous sodium hydroxide is 1.5...
Hi! Can you please answer questions a and b for my organic lab report :) The...
Hi! Can you please answer questions a and b for my organic lab
report :) The pictures below the questions is my lab procedure.
Thank you
6. Analysis Questions: a) This lab utilized a new technique called reflux, and the use of a condenser tube while heating the reaction. What is the purpose of the condenser? Why not just heat the reaction in a closed vessel instead? b) A student misread the instructions and first refluxed the sodium methoxide in...
i need help with #3 please! SAFETY NOTES: Bromobenene and acetophenone are irritants. Wear gloves and...
i need help with #3 please!
SAFETY NOTES: Bromobenene and acetophenone are irritants. Wear gloves and avoid contact with skin, eyes, and clothing • MHC) is dritating to the skin avoid contact with the skin, eyes, and clothing Diethyl ether, usually referred to simply as "ether", is volatile and flammable. Keep a safe distance from hot electrical devices WASTE DISPOSAL *** A itrate is the liquid that passed through the Hirsch funnel, ending up in the bottom of the sidearm...
This is the Wittig reaction. Below I have the reaction
performed. So first we have the IR of starting material and then
the product, all the peaks for all IR. Please identify the peaks in
all the IR. Please also explain the difference observed thank you!.
For this reaction an NMR is also performed, have to label the H NMR
based on the product formed also based on the values given have to
determine if the product was cis -9-2(...
1151 VCL 11-8: Claisen Condensation -1 For this assignment, the target compound that you should synthesize is methyl acetoacetate. This is another carbonyl addition variation. Examine the product and determine which ester is the nucleophile and which is the electrophile. Keep in mind the mechanism and that you need to acidify the intermediate in order to isolate a neutral product. Synthesis Procedures 1. Start Virtual ChemLab and select Claisen Condensation-I from the list of assignments in the electronic workbook. After...
can someone please tell me all the peaks bends etc in the
first IR as well as the functional groups. also interpret the nmr
please
07- 04- Absorbanco (au) 0.1- 0+ 3000 3000 15 1000 500 2000 Frequency (wavenumbers) Figure 3. IR spectrum of the second intermediate, bis(2,4,5-trifluorophenyl)methanone (6). 753 701 10.5 10.0 9.5 9.0 8.5 8.0 7520 6.5 6.0 5.5 4.5 4.0 3.5 Com 50 3.0 2.5 2.0 1.5 1.0 0.5 indicator. Melting point analysis was performed using a...
EXPERIMENT 2A DIELS-ALDER REACTION OF ANTHRACENE REFERENCES Pavia et al (4/e): Tech. 6.1/6.2, 7.2-7.4 Klein (1/e) pp. 784-792 EQUATION heat Diels-Alder Adduct 9,30-dihydroanthracene-9,10- endo-o B-seccinic anhydride mp 262264 PROCEDURE Place 0.200 grams of anthracene and an equal molar amount of maleic anhydride in 5 mL of xylenes in a 10-mL round-bottom flask with a magnetic stir bar. Attach a water-cooled condenser and reflux for 60 minutes. Allow the solution to cool to room temperature and then place the flask in...
what would be the percent yield if the final weight of my product
is 0.1357g this is a green chemistry wittig reaction to produce
1,4-diphenyl-1,3-butadiene from benzyltriphenylphosphonium chloride
and trans- cinnamaledyde using sodium hydroxide as the base
You will be using a Green Chemistry Wittig reaction (NOT Wittig-Horner Emmons reaction) to produce 1,4-diphenyl-1,3-butadiene starting with benzyltriphenylphosphonium chloride and trans- cinnamaledyde using sodium hydroxide as the base. This reaction is considered a "green" reaction, because an aqueous solution will be used...
Only need help with 5,6,7
and mechanism
FTIR and NMR Spectra After completing a reaction and working up the products, it is still necessary to confirm that the correct product was formed. The most common tools used for this analysis are Fourier Transform Infrared (FTIR) and Nuclear Magnetic Resonance (NMR) spectroscopy. In the virtual laboratory, 'H and C NMR spectra are available. Details on interpreting FTIR and NMR spectra are found in your textbook. Your instructor may or may not...
tthe weight of my product is 0.87 g and they gave me the
density! how can i calculte the percent yield?
- Page < 8 > of 14 | 0 Data and Observations Weight of product: Melting range of product: Attach any spectra to your laboratory report Calculations and Graphs Calculate the percent yield. Keep in mind that the reagents may not be 100% pure; refer to labels on the containers. The density of 50% aqueous sodium hydroxide is 1.5...
Hi! Can you please answer questions a and b for my organic lab
report :) The pictures below the questions is my lab procedure.
Thank you
6. Analysis Questions: a) This lab utilized a new technique called reflux, and the use of a condenser tube while heating the reaction. What is the purpose of the condenser? Why not just heat the reaction in a closed vessel instead? b) A student misread the instructions and first refluxed the sodium methoxide in...
i need help with #3 please!
SAFETY NOTES: Bromobenene and acetophenone are irritants. Wear gloves and avoid contact with skin, eyes, and clothing • MHC) is dritating to the skin avoid contact with the skin, eyes, and clothing Diethyl ether, usually referred to simply as "ether", is volatile and flammable. Keep a safe distance from hot electrical devices WASTE DISPOSAL *** A itrate is the liquid that passed through the Hirsch funnel, ending up in the bottom of the sidearm...
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