How many signals would you expect to see in the 13 C NMR spectra for:
a. 4 - (hydroxymethyl) - 2 - methoxyphenol
b. 4 - hydroxy - 3 - methoxybenzaldehyde
c. 4 - (hydroxymethyl) - 2 - methoxyphenyl acetate
How many signals would you expect to see in the 13 C NMR spectra for: a....
Not sure how to do #1 Teuutiny ayen. H3C NaBH, 95 % EtOH ? OCH vanillin acetate Figure 1. The reaction you will be investigating. possible products: Dr OH and/or on and/or ic Hzcy НО and/or HO OCH OCH OCH 4-hydroxy-3-methoxybenzaldehyde 4-hydroxymethyl) -2-methoxyphenol 4-hydroxymethyl) -2-methoxyphenyl acetate Figure 2. Possible reduction products. Pre-lab task: 1.) Assume that vanillin acetate is the limiting reagent, and calculate the theoretical yield of product if all of the vanillin acetate is converted to: a. 4-(hydroxymethyl)-2-methoxyphenol...
Question 13 5 pts How many signals would you expect to see in the 'C NMR spectrum of the following compound? осн, OCH, 3 4 Question 19 Predict the number of signals in the 13C NMR spectrum for the following structure. 5 8 7
1) How many signals would you expect to see molecule? would you expect to see in the 13C and 'H NMR spectra of the following a) 5 carbon signals; 2 proton signals b) 5 carbon signals; 3 proton signals d) 4 carbon signals; 2 proton signals c) 3 carbon signals; 3 proton signals 2) Select the major product of the following series of reactions. 1) BHTHE 2) H2O2, NaOH(aq) 3) H_Cr04 TOH
Assume that vanillin acetate is the limiting reagent, and calculate the theoretical yield of product if all of the vanillin acetate is converted to: a. 4 - (hydroxymethyl) - 2 - methoxyphenol b. 4 - hydroxy - 3 - methoxybenzaldehyde c. 4 - (hydroxymethyl) - 2 - methoxyphenyl acetat e
2.) How could you distinguish the which product has formed using IR spectroscopy? a. 4 - (hydroxymethyl) - 2 - methoxyphenol b. 4 - hydroxy - 3 - methoxybenzaldehyde c. 4 - (hydroxymethyl) - 2 - methoxyphenyl acetat e
32) How many signals would you expect to see in the 1H NMR spectrum of the following compound? CCH3 CH3 A) 6 B) 3 C) 5 D) 4 E) 2
19) How many signals would you expect to see in the 1H NMR spectrum of the following compound? ÖCH CH3 A) 5 B) 4 C) 3 D) 6 E) 2
How many signals would you expect to see in the 1H NMR spectrum in D20 of the following compound? CH3CHCH3 OH 3 o 7 2 8 4
How many signals would you expect to see in the 'H NMR spectrum of the following compound? CH2CH2CH2CH3 © 2 0 1 03 6 4
Part A How many signals would you expect to see in the 'H NMR spectrum of the following compound? CICH2CH2CI O A 05 O 3 2