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allylic acid (aspirin) Preparation of DATE SECTION NAME GRADE PARTNER Experiment 33 PRE-LAB QUESTIONS Are the...
3. Salicylic acid can irritate the stomach. Draw the structure of the molecule. Circle and name the functional grou...
3. Salicylic acid can irritate the stomach. Draw the structure of the molecule. Circle and name the functional group (or groups) responsible for this effect. 4. Magnesium hydroxide. Mg(OH), and magnesium carbonate Mann are often neon
Name Lab Partner Lab Section Date Lab 9 DATA Part A: Synthesis of Aspirin Mass of...
Name Lab Partner Lab Section Date Lab 9 DATA Part A: Synthesis of Aspirin Mass of salicylic acid 1.047 g Mass of watch glass 37.3959 Mass of watch glass + dry product 38.1409 Calculated mass of dry product 0.7459 Melting range of product 136-140 Addition of FeCl, to salicylic acid Addition of FeCl, to product Theoretical yield of aspirin Show calculation: Percent yield of aspirin product Show calculation:
Preparation of Aspirin Name Class & Section PRE-LABORATORY ASSIGNMENT 1. What hazards should you be aware of wh...
Preparation of Aspirin Name Class & Section PRE-LABORATORY ASSIGNMENT 1. What hazards should you be aware of when working with the following chemicals? a. Acetic anhydride b. Concentrated sulfuric acid 2. Explain the following terms as they relate to this experiment. a. Catalyst b. Limiting reactant 3. Following the procedure described in this experiment, a student reacted 2.775 g of salicylic acid with 4.0 ml of acetic anhydride and recovered 2.986 g of aspirin. a. Calculate the number of moles...
Name Experiment 7 - PREPARATION OF ASPIRIN AND OTHER ESTERS Date Partner Station # - Pre-Lab...
Name Experiment 7 - PREPARATION OF ASPIRIN AND OTHER ESTERS Date Partner Station # - Pre-Lab Preparation Section Questions 1-3 refer to these structures: CH,CH-O-CH,CH, CH,CH,CH,CH.CH.CH-OH CH,-0-0-CH,CH.CH, O anch-o- & -on,ch, and on and ansch.com 1. a) List the letters for the structures that are esters. b) Circle the ester functional group in any esters. 2. a) Write the letters for the two compounds that could be used to make an ester by an esterification reaction. b) Write the reaction...
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1....
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1. The Synthesis of Aspirin Record the weight of your aspirin, and calculate the percentage yield. Base the yield on salicylic acid since we acetic anhydride was used. Show all calculations. Weight of aspirin d. 08035 Yield of aspirin 2. Contaminants in Aspirin What was the color of the salicylic acid-ferric chloride test solution? On the basis of color is either your aspirin or commercial...
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual....
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual. Complete the Pre-lab Assignment. In this substitute lab exercise, you will watch a short video on preparing aspirin. The video is posted on the course Moodle page, and it provides the masses of the reactants and the product; you should be able to calculate the theoretical yield and the % yield from the data given by the video. Submit the completed assignment by March...
help NAME SECTION DATE PARTNER GRADE Experiment 50 PRE-LAB QUESTIONS 1. What foods contain appreciable amounts...
help
NAME SECTION DATE PARTNER GRADE Experiment 50 PRE-LAB QUESTIONS 1. What foods contain appreciable amounts of vitamin C? 2. Vitamin C is ascorbic acid. Yet, in the structure given in the Background, one does not see a -COOH group. Instead, one sees a lactorne in the structure. Cirele the lactone. Explain from what functional groups it is formed, and how it is formed. 3. What is the minimum daily requirement of vitamin C to prevent scurvy in adults? 4....
Pre-lab Questions: Importance A one-step preparation of aspirin from its precursor, salicylic acid, via an ester...
Pre-lab Questions:
Importance A one-step preparation of aspirin from its precursor, salicylic acid, via an ester formation illustrates one of synthetic organic chemistry's most important uses, making the drugs that treat all types of illnesses. OH HOOH Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the ancient Greeks as a treatment for pain...
Preparation of Aspirin, Methyl Salicylate and Nylon Experiment #9 Pre-Lab Exercise Briefly describe the difference between...
Preparation of Aspirin, Methyl Salicylate and Nylon Experiment #9 Pre-Lab Exercise Briefly describe the difference between an acid and an ester. Give an example of each. 2. Show the chemical reaction for the hydrolysis of the ester, ethyl acetate, indicating the two products of this reaction. 3. Describe what is meant by an amide, showing the structure of at least one example of a compound that is an amide. Be sure to give the correct name of the compound you...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification Reactions Q: Calculate the expected mass of both methyl salicylate and aspirin assuming 100% yield. EXPERIMENT7 PREPARATION OF PHARMACEUTICALS...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification
Reactions
Q: Calculate the expected mass of both methyl salicylate and
aspirin assuming 100% yield.
EXPERIMENT7 PREPARATION OF PHARMACEUTICALS Fischer Esterification Reactions Almost 2500 years ago, physicians such as Hippocrates recommended that patients chew on the bark of the willow to alleviate pain. The active ingredient in willow bark was found to be salicin, a compound made of a molecule of salicyl alcohol bonded to a p-D-glucose molecule. In the stomach, the bond between...
3. Salicylic acid can irritate the stomach. Draw the structure of the molecule. Circle and name the functional group (or groups) responsible for this effect. 4. Magnesium hydroxide. Mg(OH), and magnesium carbonate Mann are often neon
Name Lab Partner Lab Section Date Lab 9 DATA Part A: Synthesis of Aspirin Mass of salicylic acid 1.047 g Mass of watch glass 37.3959 Mass of watch glass + dry product 38.1409 Calculated mass of dry product 0.7459 Melting range of product 136-140 Addition of FeCl, to salicylic acid Addition of FeCl, to product Theoretical yield of aspirin Show calculation: Percent yield of aspirin product Show calculation:
Preparation of Aspirin Name Class & Section PRE-LABORATORY ASSIGNMENT 1. What hazards should you be aware of when working with the following chemicals? a. Acetic anhydride b. Concentrated sulfuric acid 2. Explain the following terms as they relate to this experiment. a. Catalyst b. Limiting reactant 3. Following the procedure described in this experiment, a student reacted 2.775 g of salicylic acid with 4.0 ml of acetic anhydride and recovered 2.986 g of aspirin. a. Calculate the number of moles...
Name Experiment 7 - PREPARATION OF ASPIRIN AND OTHER ESTERS Date Partner Station # - Pre-Lab Preparation Section Questions 1-3 refer to these structures: CH,CH-O-CH,CH, CH,CH,CH,CH.CH.CH-OH CH,-0-0-CH,CH.CH, O anch-o- & -on,ch, and on and ansch.com 1. a) List the letters for the structures that are esters. b) Circle the ester functional group in any esters. 2. a) Write the letters for the two compounds that could be used to make an ester by an esterification reaction. b) Write the reaction...
Lab Section Nume Preparation and Examination of a Drug: Aspirin EXPERIMENT 25 OBSERVATIONS AND RESULTS 1. The Synthesis of Aspirin Record the weight of your aspirin, and calculate the percentage yield. Base the yield on salicylic acid since we acetic anhydride was used. Show all calculations. Weight of aspirin d. 08035 Yield of aspirin 2. Contaminants in Aspirin What was the color of the salicylic acid-ferric chloride test solution? On the basis of color is either your aspirin or commercial...
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual. Complete the Pre-lab Assignment. In this substitute lab exercise, you will watch a short video on preparing aspirin. The video is posted on the course Moodle page, and it provides the masses of the reactants and the product; you should be able to calculate the theoretical yield and the % yield from the data given by the video. Submit the completed assignment by March...
help
NAME SECTION DATE PARTNER GRADE Experiment 50 PRE-LAB QUESTIONS 1. What foods contain appreciable amounts of vitamin C? 2. Vitamin C is ascorbic acid. Yet, in the structure given in the Background, one does not see a -COOH group. Instead, one sees a lactorne in the structure. Cirele the lactone. Explain from what functional groups it is formed, and how it is formed. 3. What is the minimum daily requirement of vitamin C to prevent scurvy in adults? 4....
Pre-lab Questions:
Importance A one-step preparation of aspirin from its precursor, salicylic acid, via an ester formation illustrates one of synthetic organic chemistry's most important uses, making the drugs that treat all types of illnesses. OH HOOH Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the ancient Greeks as a treatment for pain...
Preparation of Aspirin, Methyl Salicylate and Nylon Experiment #9 Pre-Lab Exercise Briefly describe the difference between an acid and an ester. Give an example of each. 2. Show the chemical reaction for the hydrolysis of the ester, ethyl acetate, indicating the two products of this reaction. 3. Describe what is meant by an amide, showing the structure of at least one example of a compound that is an amide. Be sure to give the correct name of the compound you...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification
Reactions
Q: Calculate the expected mass of both methyl salicylate and
aspirin assuming 100% yield.
EXPERIMENT7 PREPARATION OF PHARMACEUTICALS Fischer Esterification Reactions Almost 2500 years ago, physicians such as Hippocrates recommended that patients chew on the bark of the willow to alleviate pain. The active ingredient in willow bark was found to be salicin, a compound made of a molecule of salicyl alcohol bonded to a p-D-glucose molecule. In the stomach, the bond between...
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