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Determining the Purity of Aspirin using Iron (III) Chloride If the following compounds are tested using...
Please help me answer questions #1 through #12. Lab information and results are listed to the...
Please help me answer questions #1 through #12. Lab information
and results are listed to the right side. Thank you!
Paragraph . 1マーに 1 HTTL 2 | x' x, | so ea l E 1ヨ回ドもデ. | 2m 규亨ー过1K % Yield g aspirin obtained/ g aspirin calculated x 100 1. Mass of empty Erlenmeyer Flask,EF 2. Mass of EFsalicylic acid 3. Mass of EF+sslicylic acid + acetic anhydride 4. Mass of E 5. Calculate mass of salicylic acid used 8. Calculate...
allylic acid (aspirin) Preparation of DATE SECTION NAME GRADE PARTNER Experiment 33 PRE-LAB QUESTIONS Are the...
allylic acid (aspirin) Preparation of DATE SECTION NAME GRADE PARTNER Experiment 33 PRE-LAB QUESTIONS Are the medicinal properties of aspirin due to acetylsalicylic acid or salicyclic acid? 2. Draw the structure of aspirin. Should this compound test positive with 1% iron(III) chloride solution? Explain your answer. 3. Salicylic acid can irritate the stomach. Draw the structure of the molecule. Circle and name the functional group for groups) responsible for this effect Maonesium hydroxide, MgOH), and magnesium carbonate, MgCo., are often...
Experiment 11: Synthesis of Aspirin pre-lab (4 pts) 1) (2 pts) Refer to the introduction on...
Experiment 11: Synthesis of Aspirin pre-lab (4 pts) 1) (2 pts) Refer to the introduction on interpreting the ferric chloride test for phenols. Two students performed the aspirin synthesis experiment. Their melting point and ferric chloride test data are shown below. Based on the results, which student's aspirin has the higher purity? Justify your choice using the melting point data and ferric chloride test results. Melting point range for pure aspirin = 136-140 °C. Melting point range (°C) Ferric chloride...
Pre-lab Questions: Importance A one-step preparation of aspirin from its precursor, salicylic acid, via an ester...
Pre-lab Questions:
Importance A one-step preparation of aspirin from its precursor, salicylic acid, via an ester formation illustrates one of synthetic organic chemistry's most important uses, making the drugs that treat all types of illnesses. OH HOOH Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the ancient Greeks as a treatment for pain...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification Reactions Q: Calculate the expected mass of both methyl salicylate and aspirin assuming 100% yield. EXPERIMENT7 PREPARATION OF PHARMACEUTICALS...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification
Reactions
Q: Calculate the expected mass of both methyl salicylate and
aspirin assuming 100% yield.
EXPERIMENT7 PREPARATION OF PHARMACEUTICALS Fischer Esterification Reactions Almost 2500 years ago, physicians such as Hippocrates recommended that patients chew on the bark of the willow to alleviate pain. The active ingredient in willow bark was found to be salicin, a compound made of a molecule of salicyl alcohol bonded to a p-D-glucose molecule. In the stomach, the bond between...
1. Using Sigma-Aldrich website or Merck Index website or Google search find and draw structures for...
1. Using Sigma-Aldrich website or Merck Index website or Google search find and draw structures for the following compounds. (a) Atropine (b) Hydroxychloroquine (c) Saccharin (d) Cholesterol (e) Vitamin C (ascorbic acid) 2. Find the melting points for the following compounds by using Sigma-Aldrich or Google search (a) Biphenyl (b) 4-bromobenzoic acid (C) 3-nitrophenol 9. Chlorine, bromine and iodine all react with alkenes such as ethene in an addition reaction (a) Write the equation for the bromination of ethene, and...
Write chemical formulae of the following inorganic compounds: iron(III) oxide, hy- drocyanic acid (hint: hydrogen cyanide...
Write chemical formulae of the following inorganic compounds: iron(III) oxide, hy- drocyanic acid (hint: hydrogen cyanide has properties of an acid only when dissolved in water), phosphorus pentachloride, cobalt(II) acetate tetrahydrate, sodium tetraborate decahydrate (tetraborate stays for a B4O2-7 anion), barium hydroxide, dinitrogen, tin(IV) chloride (assume it is an ionic compound), tetraiodine nonaoxide, xenon hexafluoride, sodium peroxide, ammonium perchlorate, magnesium phosphide, chromium trioxide (this compound is more of a molecular than ionic type), aluminum hydrophosphate, sulfurous acid, argon, chromium(III) sulphate.
can you please help me with this !!! which ever you can is fine, please... thanks...
can you please help me with this !!!
which ever you can is fine, please... thanks !
Results/Data • Aspirin synthesis salicylic acid: 2.0 g Acetic anhydride: 2 mL d= 1.082g/ml sodium acetate: 0.4 g • Experimental yield of aspirin: 2.4 g REPORT DATE: NAME: LAB PARTNER: I PREPARATION OF METHYL SALICYLATE (OIL OF WINTERGREEN): Reaction Odor: Color after addition of FeCl solution: Control Odor: Color after addition of FeCl3 solution: Question Which functional group of salicylic acid forms a...
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual....
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual. Complete the Pre-lab Assignment. In this substitute lab exercise, you will watch a short video on preparing aspirin. The video is posted on the course Moodle page, and it provides the masses of the reactants and the product; you should be able to calculate the theoretical yield and the % yield from the data given by the video. Submit the completed assignment by March...
The weight of aspirin is 1.6 g and the reagents used to perform this synthesis was...
The weight of aspirin is 1.6 g and the reagents used to perform
this synthesis was 1.48 g salicylic acid, 3 mL ethanoic anhydride,
3 drops H2SO4, and acetylsalicylic acid
Synthesis of Aspirin Post-lab Questions February 2, 2018 Discussion of the aspirin product including, 1. The calculated percent yield of your aspirin product and comments on its purity based on the literature melting point and literature IR spectrum. Label all major peaks in the IR spectrum of your aspirin product....
Please help me answer questions #1 through #12. Lab information
and results are listed to the right side. Thank you!
Paragraph . 1マーに 1 HTTL 2 | x' x, | so ea l E 1ヨ回ドもデ. | 2m 규亨ー过1K % Yield g aspirin obtained/ g aspirin calculated x 100 1. Mass of empty Erlenmeyer Flask,EF 2. Mass of EFsalicylic acid 3. Mass of EF+sslicylic acid + acetic anhydride 4. Mass of E 5. Calculate mass of salicylic acid used 8. Calculate...
allylic acid (aspirin) Preparation of DATE SECTION NAME GRADE PARTNER Experiment 33 PRE-LAB QUESTIONS Are the medicinal properties of aspirin due to acetylsalicylic acid or salicyclic acid? 2. Draw the structure of aspirin. Should this compound test positive with 1% iron(III) chloride solution? Explain your answer. 3. Salicylic acid can irritate the stomach. Draw the structure of the molecule. Circle and name the functional group for groups) responsible for this effect Maonesium hydroxide, MgOH), and magnesium carbonate, MgCo., are often...
Experiment 11: Synthesis of Aspirin pre-lab (4 pts) 1) (2 pts) Refer to the introduction on interpreting the ferric chloride test for phenols. Two students performed the aspirin synthesis experiment. Their melting point and ferric chloride test data are shown below. Based on the results, which student's aspirin has the higher purity? Justify your choice using the melting point data and ferric chloride test results. Melting point range for pure aspirin = 136-140 °C. Melting point range (°C) Ferric chloride...
Pre-lab Questions:
Importance A one-step preparation of aspirin from its precursor, salicylic acid, via an ester formation illustrates one of synthetic organic chemistry's most important uses, making the drugs that treat all types of illnesses. OH HOOH Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the ancient Greeks as a treatment for pain...
PREPARATION OF PHARMACEUTICALS - Fischer Esterification
Reactions
Q: Calculate the expected mass of both methyl salicylate and
aspirin assuming 100% yield.
EXPERIMENT7 PREPARATION OF PHARMACEUTICALS Fischer Esterification Reactions Almost 2500 years ago, physicians such as Hippocrates recommended that patients chew on the bark of the willow to alleviate pain. The active ingredient in willow bark was found to be salicin, a compound made of a molecule of salicyl alcohol bonded to a p-D-glucose molecule. In the stomach, the bond between...
1. Using Sigma-Aldrich website or Merck Index website or Google search find and draw structures for the following compounds. (a) Atropine (b) Hydroxychloroquine (c) Saccharin (d) Cholesterol (e) Vitamin C (ascorbic acid) 2. Find the melting points for the following compounds by using Sigma-Aldrich or Google search (a) Biphenyl (b) 4-bromobenzoic acid (C) 3-nitrophenol 9. Chlorine, bromine and iodine all react with alkenes such as ethene in an addition reaction (a) Write the equation for the bromination of ethene, and...
can you please help me with this !!!
which ever you can is fine, please... thanks !
Results/Data • Aspirin synthesis salicylic acid: 2.0 g Acetic anhydride: 2 mL d= 1.082g/ml sodium acetate: 0.4 g • Experimental yield of aspirin: 2.4 g REPORT DATE: NAME: LAB PARTNER: I PREPARATION OF METHYL SALICYLATE (OIL OF WINTERGREEN): Reaction Odor: Color after addition of FeCl solution: Control Odor: Color after addition of FeCl3 solution: Question Which functional group of salicylic acid forms a...
Exercise 7: The % Yield of Aspirin Name Date Read Exercise 7 in your lab manual. Complete the Pre-lab Assignment. In this substitute lab exercise, you will watch a short video on preparing aspirin. The video is posted on the course Moodle page, and it provides the masses of the reactants and the product; you should be able to calculate the theoretical yield and the % yield from the data given by the video. Submit the completed assignment by March...
The weight of aspirin is 1.6 g and the reagents used to perform
this synthesis was 1.48 g salicylic acid, 3 mL ethanoic anhydride,
3 drops H2SO4, and acetylsalicylic acid
Synthesis of Aspirin Post-lab Questions February 2, 2018 Discussion of the aspirin product including, 1. The calculated percent yield of your aspirin product and comments on its purity based on the literature melting point and literature IR spectrum. Label all major peaks in the IR spectrum of your aspirin product....
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