The chemical shift values in these spectra are approximate values not experimental values.
For each compound: 1. Determine the number of equivalent hydrogens - number of different signals 2....
-COOH 811-812 O x - - .o. -C For each compound: 1. Determine the number of equivalent hydrogens - number of different signals 2. Determine the splitting pattern of each signal 3. Sketch a possible spectrum 4. Then try to match the compound to the correct NMR spectrum ļ wt ♡ na 1CECH PPM
NMR worksheet: H-1 (proton) NMR -COOH کد 11 وه اسط .)= X For each compound: 4. Then try to match the compound to the correct NMR spectrum ! بر ♡ na = = = | ۲۲ OMIT this peak added in error) small broad peak (OH) $ PPM We were unable to transcribe this image
NMR worksheet: C-13 NMR - || - | |-- alkanes Ester C=0 approx. 170 - 180 ppm For each compound: 1. Determine the number of equivalent carbons 2. Predict and sketch the location of the peaks 3. Then try to match the compound to the correct NMR spectrum بز به م . . We were unable to transcribe this image
2. Predict the # of signals (nonequivalent types of hydrogens, those with different chemical shifts), their approximate chemical shift, and their splitting pattern in the NMR spectrum for each of the following compounds. HHO
2. Predict the number of signals and the splitting pattern (s,d,t, etc) for each of the hydrogens in the 'H NMR spectrum of the compound below. (14 points) CH3 -CH2-O-CH3 2. Design and draw the X and R charts using the following data based on a sample size of seven items. Five samples were taken and inspected. The means of those samples were 21.6, 20.5, 19.9, 20.8, and 22.1, and the sample ranges were 5.6, 5.0, 3.8, 2.2, and 4.5.
CHE 212 NMR Problem Set 1. Calculate DU from the molecular formula given on each spectrum 2. Draw structure of the organic compound on each NMR spectrum 3 Assign all peaks on both 1HNMR and 13CNMR spectra 4 Indicate spin-spin splitting (example: singlet, doublet, triplet etc.) on 1HNMR spectr Cattoo 22 10. P OR integral We were unable to transcribe this imageC4 HN IH 3H SH 3.5 Protoa NMR .br integral values tv C, H40 эн
Practice Problems Provide the number of hydrogens in each compound and pected in the 'H NMR of the following compounds. Draw equivalent sets H stce the examples shown above. He carbon are typically equivalent you w different carbons may be equivalent if they each compound and the number of signals that are compounds. Draw in all missing H's and label chemically ples shown above. Remember that H's attached to the same en lyou will learn about exceptions in CHEM 233)....
NMR worksheet: C-13 NMR somatic cuct c-a.c-- - --- LLLLLLLLLLLLLLLLLLLLLLL Ester C=O approx. 170-180 ppm For each compound: 1. Determine the number of equivalent carbons 2. Predict and sketch the location of the peaks 3. Then try to match the compound to the correct NMR spectrum 3. & Lond. 6. B O DO do 1howo 10 120109
login on time Question 8 4 pts In 4,4-dimethyl-2.pentanone, give the number of sets of equivalent protons in 1H NMR spectrum and show the splitting pattern of each set. Also, label the protons in the most downfield region and the upheld region.
Part 1: For each of the following structures, indicate the integration expected for the signal associated with the indicated hydrogen(s). a) i) ii) iii) iv) b) i) ii) iii) c) i) ii) iii) d) i) ii) iii) iv) v) vi) e) i) ii) iii) iv) f) i) ii) iii) iv) v) vi) Part 2: For each of the following structures, indicate the coupling (a.k.a, splitting) pattern expected for the signal associated with the indicated hydrogen(s) by placing the appropriate letter(s)...