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Determine the structure that is consistent with all the data. Provide the structure of the unknown as well as the structure of the base peak.
5) Provide a structure consistent with all of the data for the following compounds. Unless otherwise stated, the IR data is not all inclusive, i.e. you may propose a structure which would include peaks not specifically noted but your structure must account for the peaks which are listed or which are excluded. a) Compound Q (C6H100) decolorizes Br2/CC14. IR peaks at 3500 cm- and 1640 cm"! NO absorption between 1700 and 1800 cm? b) Compound K (C6H100) does not decolorize...
An unknown compound with molecular formula C8H8O2 is below. Provide a structure consistent and explain the reasoning.
a) Provide the structure that is consistent with the data below. C7H14O2 IR (cm-1): 2950, 1750 1H NMR (d): 2.3 (2H, q), 1.0 (3H, t), 0.9 (9H, s) b) Deduce the identity of the compound from the data provided. C10H14O: IR (cm-1): 3200-3500 (broad), 3050, 2950, 1610 1H NMR(δ): 1.0 (s, 6H), 2.0 (s, 3H), 2.8 (broad s, 1H), 7.3 (d, 2H), 7.6 (d, 2H) c) An unknown compound, C3H5Cl3, gave the following proton NMR...
The m/z of the M+ peak of an unknown is 146, and this peak is the base peak (i.e., the tallest peak). (See below mass spectrum of the unknown.) Combustion analysis data indicate 49.03% carbon and 2.74% hydrogen. The IR spectrum and 13C-NMR spectrum of this compound also were obtained and are shown below. Given this information, what is the name of this unknown molecule? MASS SPECTRUM 100 80 60 面 40 20 0.0 120 160 40 80 0.0 m/z...
Name (PRINT): Provide a structure consistent with the following molecular formula and spectroscopic data. You will al a correct structure or partial credit for answers given below. Formula: CH.0 IR: 1700 cm (very strong) DE 1630 medium) Provide Structure a) 5 4 3 2 1 ppm (2 pts partial credit) Use the molecular formula to calculate the total number of n-bonds plus rings. (DU) for the molecule. DU = (2 pts partial credit) Use the IR data to indicate what...
Provide the correct structure for your unknown based on the
spectroscopic data provided. Provide the correct name for your
compound. Either the IUPAC name, or a commonly accepted name (i.e.,
ethyl acetate in place of ethyl ethanoate) will be accepted.IR
spectrum: Assign as many peaks as possible. In particular, you
should assign peaks that were important in making your structural
interpretation (i.e. functional group peaks such as OH, C=O, N-H,
etc.).
1H-NMR spectrum: Assign all the peaks in the spectrum...
11. Identify and draw the structure of the unknown compound (C.H.O2) that is consistent with the spectra provided. Give your reasoning. الايل 10 9 8 7 6 PPM (8) INFRARED SPECTRUM TRANSMITTANCE 1000 2000 Wavenumber (cm-1) Relative intensity The molecular Low caleissa RSS Kits M T 0-rrrttit 10 20 TTTTTTTTTTTTTTTT 30 40 50 60 70 80
Please determine the IDENTITY of the unknown
compound and explain how each peak / data point from the following
instruments led to that identification. What does the gcms
indicate. Thank you very much! (The GCMS data is just a long set of
numbers which is why the question appears so long).
IR of unknown:
NMR unknown Proton Graphs (first is overall graph,
others that follow are zoomed in sections):
NMR unknown Carbon Graphs (first is overall graph,
others that follow...
5. Determine a structure that is consistent with the molecular formula and 13C-NMR data below. You may find it helpful to calculate your degrees of unsaturation first. a. C.H.NO: 13C-NMR 8 170.5, 37.9, 20.5 ppm CsH O2: 13C-NMR 8 207.1, 55.0, 39.2 ppm CsH&N2: 13C-NMR 8 110.1, 21.4, 16.3 ppm d. C1oHe: 13C-NMR 8 133.6, 128.0, 125.9 ppm
Determine the
structure of the unknown compounds by analyzing all major peaks in
the IF spectra and all peaks of the H-NMR spectra. Show all work
for this problem.
Predicted 1H NMR Spectrum Chemical Formula: CHNO 4 40 35 20 25 20 18 16 as do Padded 13C NMR spectrum - 119.62 21.08 5 10 15 20 110100 Fi ppm)