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Question 10 1 pts How can coloured impurities be removed from a solid compound by the...
(4 pts) (4 pts) (4 pts) (1 pts) 5. Calculations 6. Conclusions 7. Post lab Questions...
(4 pts) (4 pts) (4 pts) (1 pts) 5. Calculations 6. Conclusions 7. Post lab Questions 8. TA signature POST LAB QUESTIONS: 1. Why do we add methanol to the reaction if we see a purple ring? 2. What reaction is occurring with the methanol (show reaction)? Does this reactior affect your product? 3. Why do you get a precipitate when adding the HCl to make the solution acidic? Exp 8-5 Experiment 8: Preparation of Adipic Acid from Cyclohexene Oxidation...
QUESTION: Write a flow scheme for the work-up. THE WORK UP:
QUESTION:
Write a flow scheme for the work-up.
THE WORK UP:
C. Work-up (save all layers) and Isolation of Product MgBrCl Benzoic acid Transfer the mixture into a test tube. Rinse the beaker with about 3 mL of regular (not anhydrous) diethyl ether and pour the washings into the test tube. There should be two distinct layers in the test tube Remove the aqueous layer (to be discarded) and shake the ether layer with about 2 mL of 3 M...
What are the desirable characteristics of a solvent to be used in the recrystallisation of a...
What are the desirable characteristics of a solvent to be used
in the recrystallisation of a solid product? (Hint: what is the
underlying purpose of doing recrystallisation, aside from making
the product look attractive?)
EXPERIMENT5 PREPARATION OF BENZOIC ACID Oxidation of a Primary Alcohol In this experiment, a primary alcohol (benzyl alcohol) is oxidised to a carboxylic acid (benzoic acid) by a strong oxidising agent (potassium permanganate) Because the synthesis reaction is carried out in basic conditions, the carboxylic acid...
Separating a Mixture, Recrystallization, pre-lab assignment could you also explain why you chose that substance for...
Separating a Mixture, Recrystallization, pre-lab
assignment
could you also explain why you chose that substance for the empty
spaces and question marks
EXPERIMENT 4 Pre-Lab Assignment Separating a Mixture, Recrystalliration Name Date 1. Complete the following flowchart which shows how to separate a mixture of sand, sodium chloride and acetanilide. Notice that after a separation process (a down arrow) the filtered solids are shown on the left and the filtrate (the liquid) is shown on the right. The terminal step...
Part a please Question 3 (30 pts) Lead nitrate (Pb(NO3)2) is a toxic compound used in...
Part a please
Question 3 (30 pts) Lead nitrate (Pb(NO3)2) is a toxic compound used in lead paints in the past. It has far less use now, in specialized applications such as gold extraction. Unlike most lead salts, lead nitrate is soluble in water, as seen below in the solubility chart. After aqueous gold recovery, it is desired to recover the lead nitrate from the water via crystallization. A 70°C aqueous lead nitrate solution containing 50 wt% lead nitrate and...
PartA: Penny-→ Cu2+(aq) Make sure it is dated prior to 1982. Record mass to nearest 0.001 I. Weig...
PartA: Penny-→ Cu2+(aq) Make sure it is dated prior to 1982. Record mass to nearest 0.001 I. Weigh a copper penny. grams. 2. Place 450 mL of distilled water in a clean 600-mL beaker. Place the beaker on a hotplate and heat until the water boils. Do not wait for the water to boil now, but proceed with the rest of the experiment. You will need this water for rinsing in step C3. CAUTION. You will generate poison°แs nitrogen dioxide...
what is the theoretical yield of anisalacetophenone and dibenzalacetone formed? thank you. The Aldol Condensation Precautions:...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
CHROMIC ACID OXIDATION Pre Lab Questions the amounts of materials that will be used from the...
CHROMIC ACID OXIDATION Pre Lab Questions the amounts of materials that will be used from the experimental section above) H2SO4 + Na2Cr207 2H20- H2O, A Molecular Weight Theoretical yield amount moles on (if applicable) Equivalents 2. Look up the melting point for p-nitrobenzoic acid and record the reference. 3. What color change is expected to be observed in the reaction? Explain why. CHROMIC ACID OXIDATION Experimental Procedure: Part I: Synthesis of p-nitrobenzoic Acid 1. Under the hood, add 0.400 g...
Experiment 17A. A Solubility Product Constant Procedure Getting Started 1. Obtain a 10 ml pipet, ...
question#1
Experiment 17A. A Solubility Product Constant Procedure Getting Started 1. Obtain a 10 ml pipet, a 50 mL buret, and 2 pieces of 120 cm filter paper Preparing Saturated Solutions of M10J MIO), is an insoluble divalent iodate salt. The identity of the cation M-is unknown. 1 Prepare MIO,), by adding S0 ml of o.2 M KIO, to 20 mL of 1 Molar M(NO,J, in a 150 mt 2. Stir the mixture vigorously with a stirring rod. A white,...
Using your answer to question 10 part a, calculate the theoretical amount (in mg) that was...
Using your answer to question 10 part a, calculate the
theoretical amount (in mg) that was expected for the
p-methyl acetanilide product. Be sure to show your
work.
10a: 37.9 x 17.5 / 100 = 6.6325mmol
Reaction 2: Reduction NO2 NH4HCO2 NH2 + NO2 Pd/C NO2 NH2 NH2 m-methylaniline p-methylaniline 0-methylaniline ortho meta para Procedure for Reaction 2: 1) The mixture of ortho, meta, and para isomers obtained from reaction 1 (2.4 g, 17.5 mmoles) was added to a 50...
(4 pts) (4 pts) (4 pts) (1 pts) 5. Calculations 6. Conclusions 7. Post lab Questions 8. TA signature POST LAB QUESTIONS: 1. Why do we add methanol to the reaction if we see a purple ring? 2. What reaction is occurring with the methanol (show reaction)? Does this reactior affect your product? 3. Why do you get a precipitate when adding the HCl to make the solution acidic? Exp 8-5 Experiment 8: Preparation of Adipic Acid from Cyclohexene Oxidation...
QUESTION:
Write a flow scheme for the work-up.
THE WORK UP:
C. Work-up (save all layers) and Isolation of Product MgBrCl Benzoic acid Transfer the mixture into a test tube. Rinse the beaker with about 3 mL of regular (not anhydrous) diethyl ether and pour the washings into the test tube. There should be two distinct layers in the test tube Remove the aqueous layer (to be discarded) and shake the ether layer with about 2 mL of 3 M...
What are the desirable characteristics of a solvent to be used
in the recrystallisation of a solid product? (Hint: what is the
underlying purpose of doing recrystallisation, aside from making
the product look attractive?)
EXPERIMENT5 PREPARATION OF BENZOIC ACID Oxidation of a Primary Alcohol In this experiment, a primary alcohol (benzyl alcohol) is oxidised to a carboxylic acid (benzoic acid) by a strong oxidising agent (potassium permanganate) Because the synthesis reaction is carried out in basic conditions, the carboxylic acid...
Separating a Mixture, Recrystallization, pre-lab
assignment
could you also explain why you chose that substance for the empty
spaces and question marks
EXPERIMENT 4 Pre-Lab Assignment Separating a Mixture, Recrystalliration Name Date 1. Complete the following flowchart which shows how to separate a mixture of sand, sodium chloride and acetanilide. Notice that after a separation process (a down arrow) the filtered solids are shown on the left and the filtrate (the liquid) is shown on the right. The terminal step...
Part a please
Question 3 (30 pts) Lead nitrate (Pb(NO3)2) is a toxic compound used in lead paints in the past. It has far less use now, in specialized applications such as gold extraction. Unlike most lead salts, lead nitrate is soluble in water, as seen below in the solubility chart. After aqueous gold recovery, it is desired to recover the lead nitrate from the water via crystallization. A 70°C aqueous lead nitrate solution containing 50 wt% lead nitrate and...
PartA: Penny-→ Cu2+(aq) Make sure it is dated prior to 1982. Record mass to nearest 0.001 I. Weigh a copper penny. grams. 2. Place 450 mL of distilled water in a clean 600-mL beaker. Place the beaker on a hotplate and heat until the water boils. Do not wait for the water to boil now, but proceed with the rest of the experiment. You will need this water for rinsing in step C3. CAUTION. You will generate poison°แs nitrogen dioxide...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
CHROMIC ACID OXIDATION Pre Lab Questions the amounts of materials that will be used from the experimental section above) H2SO4 + Na2Cr207 2H20- H2O, A Molecular Weight Theoretical yield amount moles on (if applicable) Equivalents 2. Look up the melting point for p-nitrobenzoic acid and record the reference. 3. What color change is expected to be observed in the reaction? Explain why. CHROMIC ACID OXIDATION Experimental Procedure: Part I: Synthesis of p-nitrobenzoic Acid 1. Under the hood, add 0.400 g...
question#1
Experiment 17A. A Solubility Product Constant Procedure Getting Started 1. Obtain a 10 ml pipet, a 50 mL buret, and 2 pieces of 120 cm filter paper Preparing Saturated Solutions of M10J MIO), is an insoluble divalent iodate salt. The identity of the cation M-is unknown. 1 Prepare MIO,), by adding S0 ml of o.2 M KIO, to 20 mL of 1 Molar M(NO,J, in a 150 mt 2. Stir the mixture vigorously with a stirring rod. A white,...
Using your answer to question 10 part a, calculate the
theoretical amount (in mg) that was expected for the
p-methyl acetanilide product. Be sure to show your
work.
10a: 37.9 x 17.5 / 100 = 6.6325mmol
Reaction 2: Reduction NO2 NH4HCO2 NH2 + NO2 Pd/C NO2 NH2 NH2 m-methylaniline p-methylaniline 0-methylaniline ortho meta para Procedure for Reaction 2: 1) The mixture of ortho, meta, and para isomers obtained from reaction 1 (2.4 g, 17.5 mmoles) was added to a 50...
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