For the last picture: The values for the NMR are 7.59, 7.58, 7.57, 7.57, 7.55, 7.55, 7.55, 7.53, 7.25 (cdcl3), 7.01, 7.01, 7.00, 6.99, 6.98, 6.98, 6.97, 6.97, 6.96, 6.95. (from left to right). Also the values found for the IR and NMR are listed in the first picture. I need help figuring out their functional groups and why (preferably an explanation if you don't mind). Also I need help analyzing the TLC and find it's value.
I added the values from the last picture just in case if it's hard to see. But the first picture has all the signals already found from both IR and NMR Spectra I just need to know what functional group they belong to and why. I also need help analyzing the TLC.
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For the last picture: The values for the NMR are 7.59, 7.58, 7.57, 7.57, 7.55, 7.55,...
What functional groups are present? What does TLC indicate? Analysis IR spectrum and 1H NMR OTH Absorbance (au) 01 4000 1600 1000 200 Frequency wavenumbers) Figure 3. IR spectrum of the second intermediate, bis(2,4,5-trifluorophenyl)methanone (6). 1.3 Cleaning up Used sodium sulfate goes into solid waste. The aqueous layer from extraction goes into aqueous wute. TLC plates go into silica waste. TLC capillaries go into glass wute. 2 Supporting information 2.1 Bis(2,4,5-trifluorophenyl)methanone 6. IR (ATR, cm): 3142, 303, 3070, 1661, 1627,...
Instructions listed below: I also need help analyzing the TLC. Also the last picture is just a handout that I also I need help on. I just noticed that the last page is very hard to understand so if you cannot analyze it it's fine. Bis(2,4,5-trifluorophenyl)methanol Scheme 1. Preparation of 5. Br Mg MgBr Oxolane F 5 Scheme 2. Reaction of (2,4,5-trifluorophenyl)magnesium bromide (5) with ethyl formate (3) to form the product of the first step, bis(2,4,5-trifluorophenyl)methanol (4). OH MgBr...
can someone please tell me all the peaks bends etc in the first IR as well as the functional groups. also interpret the nmr please 07- 04- Absorbanco (au) 0.1- 0+ 3000 3000 15 1000 500 2000 Frequency (wavenumbers) Figure 3. IR spectrum of the second intermediate, bis(2,4,5-trifluorophenyl)methanone (6). 753 701 10.5 10.0 9.5 9.0 8.5 8.0 7520 6.5 6.0 5.5 4.5 4.0 3.5 Com 50 3.0 2.5 2.0 1.5 1.0 0.5 indicator. Melting point analysis was performed using a...