Fill the ice mold with tap water and put it in a freezer for 24 hours....
Fill the ice mold with tap water and put it in a freezer for 24 hours. Remove the mold from the freezer, loosen the ice but do not remove the ice and place the mold upside down in a thin paper plate and place the plate on a thick coffee table or dining table (see Figure 1). Wait for about 30 minutes, using the cell-phone or digital watch as a timer, and then measure the amount of water in the...
Fill the graduated cylinder with hot tap water and let stand for one minute. Pour water into the sink. Measure 70 mL of hot water. Pour the water into the foam cup. Measure the temperature of the water. Add an ice cube to the cup of water. Gently swirl the cup. Measure the temperature of the water as soon as the ice cube has completely melted. Pour the water into the graduated cylinder and measure the volume. The initial temperature...
Fill the graduated cylinder with hot tap water and let stand for one minute. Pour water into the sink. Measure 70 mL of hot water. Pour the water into the foam cup. Measure the temperature of the water. Add an ice cube to the cup of water. Gently swirl the cup. Measure the temperature of the water as soon as the ice cube has completely melted. Pour the water into the graduated cylinder and measure the volume. The initial temperature...
QUESTIONS TO ANSWER: Prepare a table of all chemicals used with the structure and purpose of each. Calculate the theoretical yield by finding limiting reactant of the experiment by converting reactants to product (remember to show all calculations used) Calculate the percent yield using the limiting reactant Calculate the Rf for triphenylmethanol. If there are two dots, determine which one is triphenylmethanol.. ( I did not provide data. Please let me know how I Would do this if I did)...
PROCEDURE CAUTION!!! Nitric acid and sulfuric acid are strong and corrosive acids. For that reason, avoid inhaling its vapors or causing any contact with the skin or clothing. Wear your protective glasses at all times. Use the extractors to work with these acids. A. Nitration of methyl benzoate 1. Preparation of the reactants. In the extractor you will find a burette with concentrated sulfuric acid, a second burette with concentrated nitric acid, clearly identified. Familiarize yourself with the scales of...
please find the purpse, Discussion, conclusion un 27 Phoenix June 20 8:10 PM a 35AEXPERIMENT 35A Triphenylmethanol PROCEDURE ether MgBr+ C-OH + MgBr(OH) OMgBr 0 Addct Addition of Benzophenone While the phenylmagnesium bromide solution is being heated and stirred under reflux, make a solution of 1.09 g benzophenone in 2 mL of anhrudrous ether in a 5-mL conical vial. Cap the vial until the reflux period is over. Once the Grignard reagent is cooled to room temperature, draw some of...
Pre-Lab Assignment 1) Draw the reaction mechanism for the reaction. 2) Determine the limiting reagent. Procedure 1 Place approximately 1 g of stilbene dibromide prepared in last week's experiment in a 50 mL round bottom flask. Record the exact mass. Add 0.8 g of KOH and 4 mL of triethylene glycol from the syringe provided in the fume hood (rinse any crystals from the sides of the flask while adding triethylene glycol). 2 Heat the stirred reaction mixture to a...
What are the desirable characteristics of a solvent to be used in the recrystallisation of a solid product? (Hint: what is the underlying purpose of doing recrystallisation, aside from making the product look attractive?) EXPERIMENT5 PREPARATION OF BENZOIC ACID Oxidation of a Primary Alcohol In this experiment, a primary alcohol (benzyl alcohol) is oxidised to a carboxylic acid (benzoic acid) by a strong oxidising agent (potassium permanganate) Because the synthesis reaction is carried out in basic conditions, the carboxylic acid...
for this experiment i got a yield of 0.02g. what is the theoretical and percentage yield? STUDENT HANDOUT Synthesis of poly(2-methoxy-542-ethylhexyloxy-1.4-phenyle Purpose of the Experiment ylhexyloxy-1.4-phenylenevinylene (MEH-PPV) The purpose of this experiment is 10 bis bromomethyl)-1-methoxy-4-2- experiment is to synthesize a polymer using a Gilch polymerization of 2,5 methyl)-1-methoxy-4-(2-ethylhexyloxybenzene, to investigate the polymer's photophysica properties, and to understand the mechanism of the polymerization reaction Introduction Polyphenylene vinylenes) or PPVs are highly luminescent polymers that are used for a variety of...