50:50 mixture of Naphthalene and 4-Chloroaniline prepared, the extraction occurred using an ether solution. The mixture was prepared by a professional and is both accurate and precise. All glassware was cleaned with acetone. The SDS reports the following MPs: naphthalene = 80-82C and 4-chloroaniline = 67-70C • Mass of mixture: 1.992 g • Recovered Mass of naphthalene: 0.982 g • Mass of 4-chloroaniline: 1.032 • Naphthalene MP: 79.5 - 83.9°C • 4-Chloroaniline MP: 63.5 - 71.9°C Calculate the percent yield for each compound. Write a brief analysis on both the yield recovery and the MP determination. Be sure to include the following in your answer: Based on the results, did this separation go well overall? Were the yields good and what you would expect? Were the melting points good and what you would expect? Which compound had more issues when being separated? What are 2 common errors that could account for these results? Remember cause and effect, so explain everything to the best of your ability.
We need at least 10 more requests to produce the answer.
0 / 10 have requested this problem solution
The more requests, the faster the answer.
50:50 mixture of Naphthalene and 4-Chloroaniline prepared, the extraction occurred using an ether solution. The mixture...
6. 50:50 mixture of Naphthalene and 4-Chloroaniline prepared, the extraction occurred using an ether solution. The mixture was prepared by a professional and is both accurate and precise. All glassware was cleaned with acetone. The SDS reports the following MPs: naphthalene = 80-82C and 4-chloroaniline = 67-700 • Mass of mixture: 1.992 g • Recovered Mass of naphthalene: 0.982 g • Mass of 4-chloroaniline: 1.032 Naphthalene MP: 79.5 - 83.9°C • 4-Chloroaniline MP: 63.5 - 71.9°C Calculate the percent yield...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...