2. Benzoic acid and diphenyl ketone are both insoluble in water. Suggest a method for separating...
why isnt the benzoic acid answer?꙼̈ melting points of Benzoic acid and Phenyl succinate are both 121 celsius in the chart. can you please explain?꙼̈ 1. An unknown compound X is one of the four compounds listed in the following table. A mixture of X with benzoic acid melts at 89°C, a mixture of X with phenylsuccinate melts at 20°C, and a mixture of X with m-aminophenol melts at 102°C. What is the identity of X? Explain Chemnical mp. ("C)...
An unknown mixture (dissolved in diethyl ether) contains only 2 of the following : benzoic acid, phenol, aniline and napthalene. You use the acid-base extraction method and want to identify the 2 compounds in your original mixture. 1) To separate the organic acid you add NaOH and to separate the organic base you add HCl.In both cases these extractions are followed by extractions with water. Why do we add water? Why is this step important? (A clear explanation please). 2)When...
4. Propose an experimental method to separate benzoic acid from biphenyl an unwanted by- product of the reaction). Keep in mind that benzoic acid and biphenyl are not soluble in water. COOH Biphenyl Benzoic acid (Hint: Think about the reactivity of the above two compounds towards bases and acids)
4. A mixture of dodecano ic acid and dodecan - 1 -ol is dissolved in diethyl ether. Suggest a procedure for separating the two compounds. (1 point)
Which of these compounds are soluble in water? Benzoic Acid 4-t-butylphenol 2-chlorobenzoic acid 1-napthol o-toluic acid
Suggest a flow chart for the separation of a mixture of benzyl alcohol and benzoic acid using extraction procedure. (4 marks) Hydrolysis of compound A2 (CH 403) gave A3 and A4, A3 can be obtained from a reaction of 1-bromobutane with NaCN followed by acid hydrolysis. A reaction of A4 with thionyl chloride (SOCl2) afforded A5. Treatment of A5 with 2-propanol yielded A6. Deduce the structures of A2 to A6. (5 marks)
You have 100 mL of a solution of benzoic acid in water; the amount of benzoic acid in the solution is estimated to be about 0.30 g. The distribution coefficient of benzoic acid in diethyl ether and water is approximately 10. Calculate the amount of acid that would be left in the water solution after four 20-mL extractions with ether. Do the same calculation, using one 80-mL extraction with ether, to determine which method is more efficient.
2. Synthesize the following ketone from benzoic acid. 3. Complete the following reaction scheme. 1. DIBALH 2. H30* TMSCI pyridine CrO3 H30* SOCI2 (Et) Culi
A student carried out the experiment and recovered 0.345g of benzoic acid and 0.157 g of isoamyl alcohol. Calculate the % yield recovery of both compounds. show work. The mixture that you used in class has a total composition of 12g of Benzoic acid dissolved in 60.0ml of isoamyl alcohol and 60.0ml of of MTBE.
5. Compound C is insoluble in water and is soluble in 5M HCl solution. Identify the structure of C from the following options. i) Aniline ii) Benzoic acid iii) Phenol iv) Toluene 6. Compound D is insoluble in water/ 5M HCI / 5M NaOH / 5MNaHCO3 solutions. It forms a silver mirror when treated with Ammonical silver nitrate solution (Tollen's reagent). Identify the functional group in D. i) An alkyne ii) Phenol iii) An alkene iv) An aldehyde 7. Compound...