Question 18 18 pts A) H2SO4 H20, heat R) NaBH2CN, CH2CH2OH B) NaOH, H2O, heat S)...
Question 20 15 pts OH A) HBO K) Cl2, hv B) NaOH, H2O L) SOCI2 C) CH3COONa, DMF M) LIAIHA, THE D) CH3CH2CH2CH2MgBr, ether N) NaBH4, CH3CH2OH E) CH3CH2MgBr, ether O) CH3CH2OH, H2SO4 F) CH3CH2Li, ether P) CH3CH2ON, CH3OH G) Croz, H2SO4, H20 Q) H3O+ H) PCC, CH2Cl2 R) PBr3 1) Brą, hv S) H2, Pd J) heat T) CH3CH2CH2CH2OH, heat U) H20, H2SO4 Look at the given synthesis and the provided reagents. Fill in the blanks with the single...
Question 20 15 pts OH A) HBr K) Cl2, hv B) NaOH, H2O L) SOCI2 C) CH3COONa, DMF M) LiAIH4, THE D) CH3CH2CH2CH2MgBr, ether N) NaBH4, CH3CH2OH E) CH3CH2MgBr, ether O) CH3CH2OH, H2SO4 F) CH3CH2Li, ether P) CH3CH2ONa, CH2OH G) CrO2, H2SO4, H2O Q) H30+ H) PCC, CH2Cl2 R) PBr3 1) Bre, hv S) H2, Pd J) heat T) CH2CH2CH2CH2OH, hea U) H20, H2SO4 Look at the given synthesis and the provided reagents. Fill in the blanks with the single...
Starting materials Eo ho la Eto V OEt H3C Et k. NaOH, H20 1.HCI, H2O, heat Reagents a. CH3Br f. Eto Na b. CH3CH2Br g. SOCI C. CH3CH2CH2Br h. NH3 d. (CH3)2CHBO i. CH3NH2 e. CH2CH2CH(Br)CH3 j. NH(CH3)2 Compound 1: 1fcfclgi Compound 2: 2fafbkl
CHROMIC ACID OXIDATION Pre Lab Questions the amounts of materials that will be used from the experimental section above) H2SO4 + Na2Cr207 2H20- H2O, A Molecular Weight Theoretical yield amount moles on (if applicable) Equivalents 2. Look up the melting point for p-nitrobenzoic acid and record the reference. 3. What color change is expected to be observed in the reaction? Explain why. CHROMIC ACID OXIDATION Experimental Procedure: Part I: Synthesis of p-nitrobenzoic Acid 1. Under the hood, add 0.400 g...
Exercise 2 Separation of a Mixture Based on Acid-Base Properties One purpose of this exercise is to learn how to use a separatory funnel to extract a single component away from other compounds in solution. To do so, we will apply the principles of solubility and acid-base behavior you’re seeing in class. One of the compounds is neutral in the acid-base sense. It has no ability to either donate or accept a proton from an aqueous solution, and will remain...
What is the theoretical yield (in grams) and percent yield of your
triphenylmethanol product in this experiment? (Weight of
triphenylmethanol: 0.060g)
BACKGROUND AND THEORY The Grignard reaction was one of the first organometallic reactions discovered and is still one of the most useful synthetically. By reacting an organohalide (usually a bromide) with magnesium in ethereal solvent, carbon becomes a nucleophile. Grignard reagents are the starting points for the syntheses of many alkanes, primary, secondary, and tertiary alcohols, alkenes, and carboxylic...