Label each peak on your carbon- and proton-NMR; and label only the principle peaks found in the compound. All peaks are presented in the 4000-1000 wavenumber range.
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Label each peak on your carbon- and proton-NMR; and label only
the principle peaks found in...
18-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 19....
18-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 19. 1. Provide degrees of unsaturation. 2. Identify the IR peaks of interest. 3. For the NMR peaks of interest, ONLY indicate the "tells," but do so appropriately and sufficiently. 4. Provide the structure. MF CHINO MW 137 *C 70.0 SH 8.1 N 10.2 AR 47.40 . Mass Spee. Data relative abund. 19 SI 16 33 24 65 11 SI 10 100 109 3H Copyright...
18. 1. Provide degrees of unsaturation 2. Identify the IR peaks of interest. 3. Analyze, appropriately...
18. 1. Provide degrees of unsaturation 2. Identify the IR peaks of interest. 3. Analyze, appropriately and sufficiently, the NMR peaks of interest. 4. Provide the structure. 5. Appropriately, identify the carbon-13 peaks, as alkyl, alkenyl, alkynyl, aromatic, carbonyl, etc. We were unable to transcribe this imageAVENUMBERS 3H Copyright © 1994 2H 2H 2H 2H 2 PPM Proton NMR 140 120 100 80 20 PPM Carbon 13 NMA
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MFC,1,0, Identify the structure...
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MFC,1,0, Identify the structure of the unknown compound MP pls MW 114 *C 73.6 WW 124 Mass Spee, D relativ mix bund, 27 71 74 LESTE WVELDEN Copyright © 1994 래 TTTT 2.0 3.0 Proton NMR 1.5 1.0 PPM MITTIT 200 TTI TITTI 80 60 40 20 PPM 0 180 160 Y 120 140 100 Carbon 13 NMA 8. Consider the IR, 'H-NMR and 13C-NMR spectra of the...
MP CHT.NO MW 137 SC 70.0 SH 8.1 EN 10.2 2H 2H Ti Proton MA 20...
MP CHT.NO MW 137 SC 70.0 SH 8.1 EN 10.2 2H 2H Ti Proton MA 20 100 20 PPM Carbon 13 NMA
assign the major absorptions in the IR spectra, assign chemical shifts in both NMR, designate the...
assign the major absorptions in the IR spectra, assign chemical
shifts in both NMR, designate the parent peak in the mass spectra
data and assign the major fragments to their corresponding peaks,
and finally provide the structure for the formula.
MF C9H100 MW 134 SC 10.6 SH 7.5 Mass Spec. Data relative mit abund 5123 77 27 91 100 12 103 105 134 1357 Copyright © 1994 2H2H 2.8 2.PPK Proton NMR 215010 205 206 195 196 PPM Carbon 13...
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MF:C,H, 0. 4 pts...
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MF:C,H, 0. 4 pts Identify the structure of the unknown compound. MF C7H140 MW 114 $C 73.6 SH 12.4 Mass Spec. D m/ sbund. 27 35 relativ 114 11 Popyright © 1994 1.0 PPM 3.0 Proton NMA TTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 200 180 160 140 Carbon 13 NMR T 120 TTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 100 80 60 40 20 PPM O en og and 8. Consider the IR, 'H-NMR and C-NMR spectra of the...
assign the major absorptions in the IR spectra, assign chemical shifts in both NMR, designate the...
assign the major absorptions in the IR spectra, assign chemical
shifts in both NMR, designate the parent peak in the mass spectra
data and assign the major fragments to their corresponding peaks,
and finally provide the structure for the formula.
MF CHE MW 68 %C88.2 *H 11.8 Mass Spec. Data relative m/ abund. 21 3H .. Copyright © 1994 Note 'long-range' coupling. T TTTTTTTTTTTTTTTTT 2.4 2.2 2.0 Proton NMR 1.8 1.6 1.4 1.0 0.8 PPM Carbon 13 NMR
MF C12H1404 MW 222 *C 64.8 %H 6.4 TRETTANCE cer 144.72 11? 18426 Mass Spec. Data...
MF C12H1404 MW 222 *C 64.8 %H 6.4 TRETTANCE cer 144.72 11? 18426 Mass Spec. Data relative m/z abund. 50 8 65 12 76 14 93 10 104 9 105 11 149 100 150 176 10 177 21 744.62 1967.70 1 3 2500 AVENUMBERS 1000 Copyright © 1994 3H IN Copyright © 1994 3H 2H 1H 1H M 1207077772 Proton NMR 2.0 1.5 PPW 170 166 160 155 136 130 PPM PPW Carbon 13 NMA 18. 1. Provide degrees of...
Identify the structure and draw it based on the formula and the spectroscopy. Justify your answer...
Identify the structure and draw it based on the formula and the
spectroscopy. Justify your answer
MF CH40 47 MW 114 C 73.6 SH 12.4 3H 6H Copyright 1994 0.5 2.0 1.0 PPM 3.0 Poton NMR 2.5 1.5 180 160 140 200 80 120 100 20 PPM 0 Carbon 13 NMA ww ab sa ELITSM м М 6е 28 1500 180e 2000 2500 HAVENUMBERS 6H ЗН Copyright 1994 ST'S0T 1289.32 aL L9ET 20 89T 6L 8TLT ALE62 HAVENUMBERS ЗН ©1994...
An alcohol 6. Consider the IR, 'H-NMR and 13C-NMR spectra of the compound with MF: C,H,...
An alcohol 6. Consider the IR, 'H-NMR and 13C-NMR spectra of the compound with MF: C,H, 0. Identify the structure of the unknown compound. 4 pts MF C7H160 MW 116 *C 72.3 %H 13.9 TS SSTT * TRANSMITTANCE Mass Spec. relati m/z abun 27 29 31 19 42 10 45 18 ze SCI 2870.23 Copyright © 1994 WAVENUMBERS WENUNTERS 124 9.612.5% Proton NMR 2.6 0.5 PPM 604020 PPM 1000 Carbon 13 NNA OH B. D. OH
18-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 19. 1. Provide degrees of unsaturation. 2. Identify the IR peaks of interest. 3. For the NMR peaks of interest, ONLY indicate the "tells," but do so appropriately and sufficiently. 4. Provide the structure. MF CHINO MW 137 *C 70.0 SH 8.1 N 10.2 AR 47.40 . Mass Spee. Data relative abund. 19 SI 16 33 24 65 11 SI 10 100 109 3H Copyright...
18. 1. Provide degrees of unsaturation 2. Identify the IR peaks of interest. 3. Analyze, appropriately and sufficiently, the NMR peaks of interest. 4. Provide the structure. 5. Appropriately, identify the carbon-13 peaks, as alkyl, alkenyl, alkynyl, aromatic, carbonyl, etc. We were unable to transcribe this imageAVENUMBERS 3H Copyright © 1994 2H 2H 2H 2H 2 PPM Proton NMR 140 120 100 80 20 PPM Carbon 13 NMA
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MFC,1,0, Identify the structure of the unknown compound MP pls MW 114 *C 73.6 WW 124 Mass Spee, D relativ mix bund, 27 71 74 LESTE WVELDEN Copyright © 1994 래 TTTT 2.0 3.0 Proton NMR 1.5 1.0 PPM MITTIT 200 TTI TITTI 80 60 40 20 PPM 0 180 160 Y 120 140 100 Carbon 13 NMA 8. Consider the IR, 'H-NMR and 13C-NMR spectra of the...
MP CHT.NO MW 137 SC 70.0 SH 8.1 EN 10.2 2H 2H Ti Proton MA 20 100 20 PPM Carbon 13 NMA
assign the major absorptions in the IR spectra, assign chemical
shifts in both NMR, designate the parent peak in the mass spectra
data and assign the major fragments to their corresponding peaks,
and finally provide the structure for the formula.
MF C9H100 MW 134 SC 10.6 SH 7.5 Mass Spec. Data relative mit abund 5123 77 27 91 100 12 103 105 134 1357 Copyright © 1994 2H2H 2.8 2.PPK Proton NMR 215010 205 206 195 196 PPM Carbon 13...
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MF:C,H, 0. 4 pts Identify the structure of the unknown compound. MF C7H140 MW 114 $C 73.6 SH 12.4 Mass Spec. D m/ sbund. 27 35 relativ 114 11 Popyright © 1994 1.0 PPM 3.0 Proton NMA TTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 200 180 160 140 Carbon 13 NMR T 120 TTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 100 80 60 40 20 PPM O en og and 8. Consider the IR, 'H-NMR and C-NMR spectra of the...
assign the major absorptions in the IR spectra, assign chemical
shifts in both NMR, designate the parent peak in the mass spectra
data and assign the major fragments to their corresponding peaks,
and finally provide the structure for the formula.
MF CHE MW 68 %C88.2 *H 11.8 Mass Spec. Data relative m/ abund. 21 3H .. Copyright © 1994 Note 'long-range' coupling. T TTTTTTTTTTTTTTTTT 2.4 2.2 2.0 Proton NMR 1.8 1.6 1.4 1.0 0.8 PPM Carbon 13 NMR
MF C12H1404 MW 222 *C 64.8 %H 6.4 TRETTANCE cer 144.72 11? 18426 Mass Spec. Data relative m/z abund. 50 8 65 12 76 14 93 10 104 9 105 11 149 100 150 176 10 177 21 744.62 1967.70 1 3 2500 AVENUMBERS 1000 Copyright © 1994 3H IN Copyright © 1994 3H 2H 1H 1H M 1207077772 Proton NMR 2.0 1.5 PPW 170 166 160 155 136 130 PPM PPW Carbon 13 NMA 18. 1. Provide degrees of...
Identify the structure and draw it based on the formula and the
spectroscopy. Justify your answer
MF CH40 47 MW 114 C 73.6 SH 12.4 3H 6H Copyright 1994 0.5 2.0 1.0 PPM 3.0 Poton NMR 2.5 1.5 180 160 140 200 80 120 100 20 PPM 0 Carbon 13 NMA ww ab sa ELITSM м М 6е 28 1500 180e 2000 2500 HAVENUMBERS 6H ЗН Copyright 1994 ST'S0T 1289.32 aL L9ET 20 89T 6L 8TLT ALE62 HAVENUMBERS ЗН ©1994...
An alcohol 6. Consider the IR, 'H-NMR and 13C-NMR spectra of the compound with MF: C,H, 0. Identify the structure of the unknown compound. 4 pts MF C7H160 MW 116 *C 72.3 %H 13.9 TS SSTT * TRANSMITTANCE Mass Spec. relati m/z abun 27 29 31 19 42 10 45 18 ze SCI 2870.23 Copyright © 1994 WAVENUMBERS WENUNTERS 124 9.612.5% Proton NMR 2.6 0.5 PPM 604020 PPM 1000 Carbon 13 NNA OH B. D. OH
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