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18. 1. Provide degrees of unsaturation 2. Identify the IR peaks of interest. 3. Analyze, appropriately...
MF C12H1404 MW 222 *C 64.8 %H 6.4 TRETTANCE cer 144.72 11? 18426 Mass Spec. Data...
MF C12H1404 MW 222 *C 64.8 %H 6.4 TRETTANCE cer 144.72 11? 18426 Mass Spec. Data relative m/z abund. 50 8 65 12 76 14 93 10 104 9 105 11 149 100 150 176 10 177 21 744.62 1967.70 1 3 2500 AVENUMBERS 1000 Copyright © 1994 3H IN Copyright © 1994 3H 2H 1H 1H M 1207077772 Proton NMR 2.0 1.5 PPW 170 166 160 155 136 130 PPM PPW Carbon 13 NMA 18. 1. Provide degrees of...
(15 + 11 + 4 pts, 30 pts total) 18-20. Spectroscopy: Analyze the spectroscopic data provided....
(15 + 11 + 4 pts, 30 pts total) 18-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (15 pts) 18. 1. Provide degrees of unsaturation 2. Identify the IR peaks of interest. 3. Analyze, appropriately and sufficiently, the NMR peaks of interest. 4. Provide the structure. 5. Appropriately, identify the carbon-13 peaks, as alkyl, alkenyl, alkynyl, aromatic, carbonyl, etc. MF 24° MW m2 SC 64.8 SH64 Mass Spec. Data relative abund 14. 65 76 12...
(15 + 11 pts, 26 pts total) 19-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may...
(15 + 11 pts, 26 pts total) 19-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (15 pts) 19. 1. Provide degrees of unsaturation. 2. Identify the IR peaks of interest. 3. Analyze, appropriately and sufficiently, the NMR peaks of interest. 4. Provide the structure. 5. Appropriately, identify the carbon-13 peaks, as alkyl, alkenyl, alkynyl, aromatic, carbonyl, etc. MFC12004 MW 222 SC 6.8 SH6.4 Mass Spes. Data relatie le und 104 15 11 H9 100 Copyright...
18-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 19....
18-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 19. 1. Provide degrees of unsaturation. 2. Identify the IR peaks of interest. 3. For the NMR peaks of interest, ONLY indicate the "tells," but do so appropriately and sufficiently. 4. Provide the structure. MF CHINO MW 137 *C 70.0 SH 8.1 N 10.2 AR 47.40 . Mass Spee. Data relative abund. 19 SI 16 33 24 65 11 SI 10 100 109 3H Copyright...
19-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 20....
19-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 20. 1. Provide degrees of unsaturation. 2. Identify the IR peaks of interest. 3. For the NMR peaks of interest, ONLY indicate the "tells," but do so appropriately and sufficiently. 4. Provide the structure ME COMO MW 137 SC 70.0 SN 102 Mam Spec. Data 27 19 si 3110 10964 34 Copyright 1994 2H2H Proton IWA 120 100 20 PPM Carbon 13 NMR
Label each peak on your carbon- and proton-NMR; and label only the principle peaks found in...
Label each peak on your carbon- and proton-NMR; and label only
the principle peaks found in the compound. All peaks are presented
in the 4000-1000 wavenumber range.
Copyright 1994 Proton NMR 60 140 Carbon 13 NMA 120 100 2H 80 MF 8H11 MW 137 %C70.0 EH 8.1 N 10.2 2 PPM 20 PPM
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MFC,1,0, Identify the structure...
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MFC,1,0, Identify the structure of the unknown compound MP pls MW 114 *C 73.6 WW 124 Mass Spee, D relativ mix bund, 27 71 74 LESTE WVELDEN Copyright © 1994 래 TTTT 2.0 3.0 Proton NMR 1.5 1.0 PPM MITTIT 200 TTI TITTI 80 60 40 20 PPM 0 180 160 Y 120 140 100 Carbon 13 NMA 8. Consider the IR, 'H-NMR and 13C-NMR spectra of the...
assign the major absorptions in the IR spectra, assign chemical shifts in both NMR, designate the...
assign the major absorptions in the IR spectra, assign chemical
shifts in both NMR, designate the parent peak in the mass spectra
data and assign the major fragments to their corresponding peaks,
and finally provide the structure for the formula.
MF C9H100 MW 134 SC 10.6 SH 7.5 Mass Spec. Data relative mit abund 5123 77 27 91 100 12 103 105 134 1357 Copyright © 1994 2H2H 2.8 2.PPK Proton NMR 215010 205 206 195 196 PPM Carbon 13...
assign the major absorptions in the IR spectra, assign chemical shifts in both NMR, designate the...
assign the major absorptions in the IR spectra, assign chemical
shifts in both NMR, designate the parent peak in the mass spectra
data and assign the major fragments to their corresponding peaks,
and finally provide the structure for the formula.
MF CHE MW 68 %C88.2 *H 11.8 Mass Spec. Data relative m/ abund. 21 3H .. Copyright © 1994 Note 'long-range' coupling. T TTTTTTTTTTTTTTTTT 2.4 2.2 2.0 Proton NMR 1.8 1.6 1.4 1.0 0.8 PPM Carbon 13 NMR
Label the significant peaks in the IR and NMR spectra. When analyzing the signals in the 'HNMR, b...
Label the significant peaks in the IR and NMR spectra. When analyzing the signals in the 'HNMR, be sure to include all appropriate information. For example: 3H, singlet, 0 neighbors, and c (the letter referring to the corresponding unique type of hydrogens that were labeled in the structure). It is recommended to provide more analysis for each signal than what is described above, when necessary, such as labeling any coupling constants if any are provided For NMR label each peak...
MF C12H1404 MW 222 *C 64.8 %H 6.4 TRETTANCE cer 144.72 11? 18426 Mass Spec. Data relative m/z abund. 50 8 65 12 76 14 93 10 104 9 105 11 149 100 150 176 10 177 21 744.62 1967.70 1 3 2500 AVENUMBERS 1000 Copyright © 1994 3H IN Copyright © 1994 3H 2H 1H 1H M 1207077772 Proton NMR 2.0 1.5 PPW 170 166 160 155 136 130 PPM PPW Carbon 13 NMA 18. 1. Provide degrees of...
(15 + 11 + 4 pts, 30 pts total) 18-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (15 pts) 18. 1. Provide degrees of unsaturation 2. Identify the IR peaks of interest. 3. Analyze, appropriately and sufficiently, the NMR peaks of interest. 4. Provide the structure. 5. Appropriately, identify the carbon-13 peaks, as alkyl, alkenyl, alkynyl, aromatic, carbonyl, etc. MF 24° MW m2 SC 64.8 SH64 Mass Spec. Data relative abund 14. 65 76 12...
(15 + 11 pts, 26 pts total) 19-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (15 pts) 19. 1. Provide degrees of unsaturation. 2. Identify the IR peaks of interest. 3. Analyze, appropriately and sufficiently, the NMR peaks of interest. 4. Provide the structure. 5. Appropriately, identify the carbon-13 peaks, as alkyl, alkenyl, alkynyl, aromatic, carbonyl, etc. MFC12004 MW 222 SC 6.8 SH6.4 Mass Spes. Data relatie le und 104 15 11 H9 100 Copyright...
18-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 19. 1. Provide degrees of unsaturation. 2. Identify the IR peaks of interest. 3. For the NMR peaks of interest, ONLY indicate the "tells," but do so appropriately and sufficiently. 4. Provide the structure. MF CHINO MW 137 *C 70.0 SH 8.1 N 10.2 AR 47.40 . Mass Spee. Data relative abund. 19 SI 16 33 24 65 11 SI 10 100 109 3H Copyright...
19-20. Spectroscopy: Analyze the spectroscopic data provided. (Student may ignore the MS data.) (11 pts) 20. 1. Provide degrees of unsaturation. 2. Identify the IR peaks of interest. 3. For the NMR peaks of interest, ONLY indicate the "tells," but do so appropriately and sufficiently. 4. Provide the structure ME COMO MW 137 SC 70.0 SN 102 Mam Spec. Data 27 19 si 3110 10964 34 Copyright 1994 2H2H Proton IWA 120 100 20 PPM Carbon 13 NMR
Label each peak on your carbon- and proton-NMR; and label only
the principle peaks found in the compound. All peaks are presented
in the 4000-1000 wavenumber range.
Copyright 1994 Proton NMR 60 140 Carbon 13 NMA 120 100 2H 80 MF 8H11 MW 137 %C70.0 EH 8.1 N 10.2 2 PPM 20 PPM
7. Consider the IR, 'H-NMR and C-NMR spectra of the compound with MFC,1,0, Identify the structure of the unknown compound MP pls MW 114 *C 73.6 WW 124 Mass Spee, D relativ mix bund, 27 71 74 LESTE WVELDEN Copyright © 1994 래 TTTT 2.0 3.0 Proton NMR 1.5 1.0 PPM MITTIT 200 TTI TITTI 80 60 40 20 PPM 0 180 160 Y 120 140 100 Carbon 13 NMA 8. Consider the IR, 'H-NMR and 13C-NMR spectra of the...
assign the major absorptions in the IR spectra, assign chemical
shifts in both NMR, designate the parent peak in the mass spectra
data and assign the major fragments to their corresponding peaks,
and finally provide the structure for the formula.
MF C9H100 MW 134 SC 10.6 SH 7.5 Mass Spec. Data relative mit abund 5123 77 27 91 100 12 103 105 134 1357 Copyright © 1994 2H2H 2.8 2.PPK Proton NMR 215010 205 206 195 196 PPM Carbon 13...
assign the major absorptions in the IR spectra, assign chemical
shifts in both NMR, designate the parent peak in the mass spectra
data and assign the major fragments to their corresponding peaks,
and finally provide the structure for the formula.
MF CHE MW 68 %C88.2 *H 11.8 Mass Spec. Data relative m/ abund. 21 3H .. Copyright © 1994 Note 'long-range' coupling. T TTTTTTTTTTTTTTTTT 2.4 2.2 2.0 Proton NMR 1.8 1.6 1.4 1.0 0.8 PPM Carbon 13 NMR
Label the significant peaks in the IR and NMR spectra. When analyzing the signals in the 'HNMR, be sure to include all appropriate information. For example: 3H, singlet, 0 neighbors, and c (the letter referring to the corresponding unique type of hydrogens that were labeled in the structure). It is recommended to provide more analysis for each signal than what is described above, when necessary, such as labeling any coupling constants if any are provided For NMR label each peak...
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