A mixture containing 1,3,5-trimethoxybenzene (A), phenol (B), aniline (C) and 1-naphthoic acid (D) was dissolved in...
A mixture containing 1,3,5-trimethoxybenzene (A), phenol (B), aniline (C) and 1-naphthoic acid (D) was dissolved in dichloromethane. Next two extractions wereperformed first using HCl then with NaOH. Which of the compounds could not beseparated in this procedure. Explain and show the pertinent reaction equation/s.
Homework Answers
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A mixture containing 1,3,5-trimethoxybenzene (A), phenol (B),
aniline (C) and 1-naphthoic acid (D) was dissolved in...
A mixture containing 1, 3, 5-trimcthoxybcnzcnc (A), phenol (B), aniline (C) and 1-naphthoic acid (D) was...
A mixture containing 1, 3, 5-trimcthoxybcnzcnc (A), phenol (B), aniline (C) and 1-naphthoic acid (D) was dissolved in dichloromethane. Next two extractions were performed first using HC1 then with NaOH. Which of the compounds could not be separated in this procedure. Explain and show the pertinent reaction equation/s. student wanted to separate a mixture of benzoic acid and aniline that were dissolved in ethanol. Could the student separate the two compounds using a base extraction (NaOH)? Explain
An unknown mixture (dissolved in diethyl ether) contains only 2 of the following : benzoic acid,...
An unknown mixture (dissolved in diethyl ether) contains only 2 of the following : benzoic acid, phenol, aniline and napthalene. You use the acid-base extraction method and want to identify the 2 compounds in your original mixture. 1) To separate the organic acid you add NaOH and to separate the organic base you add HCl.In both cases these extractions are followed by extractions with water. Why do we add water? Why is this step important? (A clear explanation please). 2)When...
A mixture of compounds containing dimethylamine, phenol, ammonia, and acetic acid is separated using liquid-liquid extraction...
A mixture of compounds containing dimethylamine, phenol, ammonia, and acetic acid is separated using liquid-liquid extraction as follows: Step 1: Concentrated HCl is added followed by draining the aqueous layer. Step 2: Dilute NaOH is added to the organic layer followed by draining the aqueous layer. Step 3: Concentrated NaOH is added to the organic layer followed by draining the aqueous layer. Which compound would you expect to be extracted into the aqueous layer after the addition of dilute NaOH,...
Three compounds below were dissolved in a solution of diethyl ether [Answer choices are aniline, benzoic...
Three compounds below were dissolved in a solution of diethyl
ether
[Answer choices are aniline, benzoic acid, and benzil]
____ can be extracted into the aqueous layer using 3 M HCL
____ can be extracted into the aqueous layer using 3M NaOH
Draw the compounds left in solution
The three compounds below were disolved in a solution of diethyl ether. Mapd OH NH2 aniline benzoic acid benzil Select answercan be extracted into the aqueous layer using 3M HCI. Select answercan...
4. A mixture of dodecano ic acid and dodecan - 1 -ol is dissolved in diethyl ether. Suggest a procedure for separat...
4. A mixture of dodecano ic acid and dodecan - 1 -ol is dissolved in diethyl ether. Suggest a procedure for separating the two compounds. (1 point)
Exercise 2 Separation of a Mixture Based on Acid-Base Properties One purpose of this exercise is...
Exercise 2 Separation of a Mixture Based on Acid-Base Properties One purpose of this exercise is to learn how to use a separatory funnel to extract a single component away from other compounds in solution. To do so, we will apply the principles of solubility and acid-base behavior you’re seeing in class. One of the compounds is neutral in the acid-base sense. It has no ability to either donate or accept a proton from an aqueous solution, and will remain...
Use of Extraction to Isolate a Neutral Compound from a Mixture Containing an Acid or Base...
Use
of Extraction to Isolate a Neutral Compound from a Mixture
Containing an Acid or Base Impurity.
Part 4D
Hi guys I had a question about this lab. I am not sure how to
create a flow chart for it as well as what chemical equations it
needs. please let me know if you need more information.
layer. In the Optional Exercise, the sample contains a neutrum base impurity; however, a detailed procedure is not given. If you are assigned...
Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in diethyl...
Okay, so we had solid benzoic acid, ethyl 4- aminobenzoate, and 9-fluorenone all dissolved in diethyl ether (4ml). We separated the basic component by adding 3M HCl, we separated the acidic component by adding 3M NaOH. I don't understand what happens here. To isolate the acidic solution, we added 6 M NaOH and used the vacuum to recover the solid. To isolate the basic solution we added 6M HCl. Here are the questions I am having trouble with... • Why...
3. 0.7253 g sample containing an unknown weak acid HA was dissolved in 50 mL water...
3. 0.7253 g sample containing an unknown weak acid HA was dissolved in 50 mL water and titrated against 0.1555 M NaOH, requiring 48.11 mL to of NaOH to reach the end-point. During the titration reaction, the pH of the solution is 3.77 when half of the HA is neutralized and the equivalence-point pH is 8.33. (a) State two ways to standardize the NaOH used in the titration. (b) Suggest and explain an indicator that can be used in the...
using the procedures, we used dichloromethane as the unknown mixture and i was able to extract...
using the procedures, we used dichloromethane as the unknown
mixture and i was able to extract benzoic acid for an acid,
5-chloro-2-methoxyanaline for a base compound and biphenyl for
neutral compound.
i don't know if that answers the missing part but if it didn't
could you be specific please? thank you!
2. Construct a flow chart of the acid-base extraction you carried out. Use the specific structure of the compounds isolated. Don't use the molecular formula. (15 pts) We used...
A mixture containing 1, 3, 5-trimcthoxybcnzcnc (A), phenol (B), aniline (C) and 1-naphthoic acid (D) was dissolved in dichloromethane. Next two extractions were performed first using HC1 then with NaOH. Which of the compounds could not be separated in this procedure. Explain and show the pertinent reaction equation/s. student wanted to separate a mixture of benzoic acid and aniline that were dissolved in ethanol. Could the student separate the two compounds using a base extraction (NaOH)? Explain
A mixture of compounds containing dimethylamine, phenol, ammonia, and acetic acid is separated using liquid-liquid extraction as follows: Step 1: Concentrated HCl is added followed by draining the aqueous layer. Step 2: Dilute NaOH is added to the organic layer followed by draining the aqueous layer. Step 3: Concentrated NaOH is added to the organic layer followed by draining the aqueous layer. Which compound would you expect to be extracted into the aqueous layer after the addition of dilute NaOH,...
Three compounds below were dissolved in a solution of diethyl
ether
[Answer choices are aniline, benzoic acid, and benzil]
____ can be extracted into the aqueous layer using 3 M HCL
____ can be extracted into the aqueous layer using 3M NaOH
Draw the compounds left in solution
The three compounds below were disolved in a solution of diethyl ether. Mapd OH NH2 aniline benzoic acid benzil Select answercan be extracted into the aqueous layer using 3M HCI. Select answercan...
4. A mixture of dodecano ic acid and dodecan - 1 -ol is dissolved in diethyl ether. Suggest a procedure for separating the two compounds. (1 point)
Use
of Extraction to Isolate a Neutral Compound from a Mixture
Containing an Acid or Base Impurity.
Part 4D
Hi guys I had a question about this lab. I am not sure how to
create a flow chart for it as well as what chemical equations it
needs. please let me know if you need more information.
layer. In the Optional Exercise, the sample contains a neutrum base impurity; however, a detailed procedure is not given. If you are assigned...
using the procedures, we used dichloromethane as the unknown
mixture and i was able to extract benzoic acid for an acid,
5-chloro-2-methoxyanaline for a base compound and biphenyl for
neutral compound.
i don't know if that answers the missing part but if it didn't
could you be specific please? thank you!
2. Construct a flow chart of the acid-base extraction you carried out. Use the specific structure of the compounds isolated. Don't use the molecular formula. (15 pts) We used...
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