Solution :
A) The compound is camphor because it started melting at 182 °C and finished at 187 °C. The range of melting point is broad (from 182 to 187), which resembles with the camphor. The higher melting point of the compound might be due to incomplete reactions.
B) The synthesized compound is acetaminophen. The low melting point is due to presence of impurity while high melting point can be due to incomplete reaction. The increase in melting point is due to higher melting point of the starting reactants.
- A student is trying to identify an unknown solid based on its melting point. She...
determine unknown compound Melting point range 126-130 celcius Soluble in ether and water Has nitrogen No halogens No sulfur Possibly contains acid, alcohol, aldehyde, amine, anhydride, ester,ketone nitrile, phenol. IR spectrum: possible compounds (pink list): (this was all the info given!) 103 100 3710 7Bon-1. 95 45%T 368062cm-1. 95.00%T 90- 85- 1, 88.30%T 261A)cm-1, 88.52%T 179.98cm 1.85 83 71%T 11 22.39am 114282cm. 5%T T 810.17 6.88%T 104.02cm-1, 84,p%T 2922 79on-1, 82.48%T 323ST 80%T 1 1. 8052%T 3363 20cm-1, 78.85%T 38...
help with identifiying each unknown in extraction and washing experiment. the ir spectra are given below, along with data, and the lab sheet is attached. Neutral Solid Primary amine (Aniline) 3403cm - NE presence Transmittance 60 3258cm 1 streren NOUD Streich 50 Ctretcher strator NH2 aromatto 11 NO2 aring 2-nitroaniline K LILI 3600 3200 2800 2400 2000 1800 1600 Wavenumber cm-1 1400 1200 1000 800 600 Basic Solid primary amine Transmittance I NH2 Stretch p-acetvianiline 70 60 CS HG NO...