Record your conclusions for the presence of salicylic acid in each solution - How would I determine the presence when looking at the tube?
5. How did exposing the aspirin powder to air for 8 to 12 hours affect its composition?
Generally, salicylic acid with Fe(iii) give purple color. so, you can confirmed the presence of salicylic acid by adding Fe into the given tube of solution and get purple color complex.
Exposing the aspirin powder to air for 8 to 12 hour change it's smell of vinegar. The acetylsalicylic acid is being de-acetylated.
Record your conclusions for the presence of salicylic acid in each solution - How would I...
3. 0.69g of salicylic acid was reacted with 0.6g acetic anhydride in the presence of concentrated phosphoric acid to yield 0.80g of acetyl salicylic acid (see below). Determine the limiting reagent and percent yield. C-CH OH COOH CH, COOH CHC Salicylic acid MW 138.12. mp 159C Acetic anhydride Acetylsalicylic acid M W 102.09. bp 140CMW 180.15. mp 128-1370 4. How do you account for the smell of vinegar when an old bottle of aspirin opened?
use condensed structural formulas to write the balance
equation for the reaction of salicylic acid with acetic
anhydride.
Use the models to demonstrate the reaction
use condensed structural formulas to write the balance
equation for the reaction of salicylic acid with methanol.
Use the models to demonstrate the reaction
Describe the appearance of aspirin product
REPORT SHEET: ASPIRIN Name Partner(s) Date Section Instructor A. Molecular models Use condensed Ne condensed structural formulas to write the balanced equation for the reaction...
Experiment 2: Synthesis of Aspirin (Acetylsalicylic Acid ) 1. How many moles of salicylic acid are there in 1.0 grams of salicylic acid? 2. How many moles of acetic anhydride are there in 3 mL of acetic anhydride? 3. When 1.0g of salicylic acid and 3 mL of acetic anhydride react, DETERMINE which one is the limiting reactant (you can go to General Chemistry if you need help about limiting reagent)? 4. What is phosphoric acid used for in the...
i did the synthesis of aspirin experiment and got the data
below. how do you do the theoretical yield? percent yield of the
pure aspirin?
DATA: Mass of Salicylic Acid: 2.034g Volume of Acetic Anhydride used in synthesis: 4.00ml Mass of filter paper: 0.196g Mass of filter paper plus Aspirin: 1.868g Mass of Aspirin: 1.672g Percent Yield of Pure Aspirin: I Experimental Procedure HAZARD: Sulfuric acid, acetic anhydride and glacial acetic acid are corrosive to the skin. They are also...
14.0 g of acetylsalicylic acid were obtained from 23.9 g of salicylic acid. Determine the percentage yield of acetylsalicylic acid. What I did: 23.9 g ÷ 138 g = 0.1732 mol Known Information: Reactant mass: 23.9 g Product mass: 14.0 g Reactant moles: 0.1732 moles *Please help: How would I solve for the Theoretical maximum moles of acetylsalicylic acid? acetylsalicylic acid C₉H₈O₄ (12•9) + (1•8) + (4•16) = 180 g/mol Would it be 14.0 g ÷ 180 g? Please explain.
1) Which reactant, salicylic acid or acetic anhydride, is in
excess? Show your work.
2) If you were to use 3.17 g of starting material, how much
product would you expect? Again, show your work.
3) Why is phosphoric acid added to the reaction?
4) A small amount of water is added at the end of the reaction
to react with the excess acetic anhydride. Show a balanced equation
for that reaction.
5) Explain the purpose of the FeCl3 test...
Please help me answer questions #1 through #12. Lab information
and results are listed to the right side. Thank you!
Paragraph . 1マーに 1 HTTL 2 | x' x, | so ea l E 1ヨ回ドもデ. | 2m 규亨ー过1K % Yield g aspirin obtained/ g aspirin calculated x 100 1. Mass of empty Erlenmeyer Flask,EF 2. Mass of EFsalicylic acid 3. Mass of EF+sslicylic acid + acetic anhydride 4. Mass of E 5. Calculate mass of salicylic acid used 8. Calculate...
Pre-lab Questions:
Importance A one-step preparation of aspirin from its precursor, salicylic acid, via an ester formation illustrates one of synthetic organic chemistry's most important uses, making the drugs that treat all types of illnesses. OH HOOH Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the ancient Greeks as a treatment for pain...
someone help me with these 7 questions
add a drop of iodine solution. If starch is present, I Wl iodine. The starch-iodine complex is deep blue-violet. Repeat this test with a com- mercial aspirin tablet and with the acetylsalicylic acid prepared in this experiment O N S at is the purpose of the concentrated phosphoric acid used in the first step? What would happen if the phosphoric acid were left out? 2. 1. Wh 3. If you used 250 mg...
Suplementary Questions Carbon Dioxide Conclusions 1. Can a candle burn in carbon dioxide? Does carbon dioxide burn? 2. What happened to the burning candle? Could carbon dioxide be used as a fire extinguisher? 3. Why should you release the carbon dioxide into the bottom of the cup? Hydrogen Conclusions 1. What difference did you notice between Parts 1 and 2 in the hydrogen experiment? Explain. 2. What is the purpose of the soap solution? 3. Why should extreme care be...