Experiment 2: Synthesis of Aspirin (Acetylsalicylic Acid ) 1. How many moles of salicylic acid are...
Experiment 2: Synthesis of Aspirin (Acetylsalicylic Acid )
1. How many moles of salicylic acid are there in 1.0 grams of salicylic acid?
2. How many moles of acetic anhydride are there in 3 mL of acetic anhydride?
3. When 1.0g of salicylic acid and 3 mL of acetic anhydride react, DETERMINE which one is the limiting reactant (you can go to General Chemistry if you need help about limiting reagent)?
4. What is phosphoric acid used for in the reaction?
5. What is the heating source for the reaction?
6. How long will you heat the reaction mixture at 70 º C - 80 º C?
7. When water reacts with anhydride, what is the product?
8. Based on the description of the procedure, DO YOU THINK that pure acetylsalicylic acid is a solid or liquid compound?
9. How will you determine purify of the final product you made?
Homework Answers
The questions are based on mile concept.
Limiting reagent is the reactant which used up
completely in the reaction.
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Experiment 2: Synthesis of Aspirin (Acetylsalicylic Acid )
1. How many moles of salicylic acid are...
10) A student prepares aspirin (acetylsalicylic acid, C,H,0.) by reacting salicylic acid (C,H,O,) with acetic anhydride...
10) A student prepares aspirin (acetylsalicylic acid, C,H,0.) by reacting salicylic acid (C,H,O,) with acetic anhydride (C.H.O.). The balanced equation for the reaction is: 2 C,H,O, + C,H,O, + 2 C,H,O, + H,O The lab calls for 3.00 g of salicylic acid to be mixed with 6.40 g of acetic anhydride. What is the limiting reagent and what is the maximum amount of aspirin which can be prepared if the yield for the reaction is 91%?
3. 0.69g of salicylic acid was reacted with 0.6g acetic anhydride in the presence of concentrated phosphoric acid...
3. 0.69g of salicylic acid was reacted with 0.6g acetic anhydride in the presence of concentrated phosphoric acid to yield 0.80g of acetyl salicylic acid (see below). Determine the limiting reagent and percent yield. C-CH OH COOH CH, COOH CHC Salicylic acid MW 138.12. mp 159C Acetic anhydride Acetylsalicylic acid M W 102.09. bp 140CMW 180.15. mp 128-1370 4. How do you account for the smell of vinegar when an old bottle of aspirin opened?
1. Mass of salicylic acid (g) 2.0089 5.10ml & 2. Volume of acetic anhydride (mL) Limiting...
1. Mass of salicylic acid (g) 2.0089 5.10ml & 2. Volume of acetic anhydride (mL) Limiting reactant is (circle one): Salicylic Acid or Acetic Anhydride Calculation for Limiting Reactant: 3. Theoretical yield of aspirin (9) Calculation for Theoretical Yield of aspirin: 4. Mass of filter paper 0.3369 N 5. Mass of filter paper + aspirin 2.471g 6. Experimental Yield of aspirin (g) 7. Percent Yield Synthesis of Aspirin An early oral pain reliever, salicylic acid, was determined to cause stomach...
Aspirin can be made by reacting acetic anhydride (C4H6O3) with salicylic acid (C7H6O3) to form aspirin...
Aspirin can be made by reacting acetic anhydride (C4H6O3) with salicylic acid (C7H6O3) to form aspirin (C9H8O4). C4H6O3 + C7H6O3 --> C2H4O2 + C9H8O4 When synthesizing aspirin, a student began with 3.05 mL of acetic anhydride (density = 1.08 g/mL) and 1.85 g of salicylic acid. The reaction was allowed to run its course and 1.84 grams of aspirin was collected by the student. Determine the limiting reactant, theoretical yield of aspirin, and percent yield for the reaction.
PRELAB EXERCISE EXPERIMENT 21 Synthesis of Aspirin (Acetylsalicylic Acid) 1. What is the purpose of sulfuric...
PRELAB EXERCISE EXPERIMENT 21 Synthesis of Aspirin (Acetylsalicylic Acid) What is the purpose of sulfuric acid or phosphoric acid used in the acetylation reaction? Use equations to explain this purpose. The procedure calls for cautious addition of water to the reaction mixture while it is still hot. What purpose does the addition of water serve and why should the addition be done while the reaction mixture is hot? Provide an equation for the reaction involved.Using the quantities of salicylic acid and acetic anhydride...
please help Mustrates treat all types of ilnesses. Background Aspirin is a prodrug of salicylic acid,...
please help
Mustrates treat all types of ilnesses. Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the andient Greeks as a treatment for pain and fever. Salicylic acid (and many related phenols) are very hard on your Ho stomach, but when esterified, as aspirin is, they are much better tolerated. Simple esters are...
Instructions: Use the following reaction to answer the questions in part ad Tom aspirin acetic acid...
Instructions: Use the following reaction to answer the questions in part ad Tom aspirin acetic acid Salicylic P.M. - 138g/mol acetic anhydride P.M. -102.1g/mol PM180.2g/mol a. Calculate the theoretical yield if 6.0g of salicylic acid are reacted with 12mL of acetic anhydride (density 1.08g/ml) b. What is the limiting REAGENT and what is the excess REAGENT? c. How many moles of excess reagent did not react with the limiting reagent? d. f 6.9 g of aspirin are produced in an...
10. Calculate the theoretical yield of aspirin using 4.00 g of salicylic acid as the starting...
10. Calculate the theoretical yield of aspirin using 4.00 g of salicylic acid as the starting material. Assume acetic anhydride is in excess. (Hint: from the mass of salicylic acid acid use, how many moles of salycilic acid are present intitially? What is the salycilic acid : acetylsalicylic acid molar ratio? How many moles of acetylsalicylic acid are formed assuming 100% yield? Based on this abount of moles, how many grams of acetylsalicylic acid are formed? (this is the theoretical...
95 Experiment IX Synthesis of Aspirin Prelaboratory Assignment Name: frobect Bun, Bak Baniot Date...
95 Experiment IX Synthesis of Aspirin Prelaboratory Assignment Name: frobect Bun, Bak Baniot Date Sabaitecd Section #. . Using chemical structures, write the balanced equation for the synthesis of aspirin and label all reagents and products with their appropriate names. ooH он C14 14,03 2. What are the two functional groups on salicylic acid? 3. What are the two functional groups on aspirin? b. anhydride? b) How many moles of Apririn could be produced from 2 moles of salicylic acid?...
Show all steps for the synthesis of aspirin (acetylsalicylic acid) Hint: Esterification
Show all steps for the synthesis of aspirin (acetylsalicylic acid) Hint: Esterification он он acetic anhydride acetic acid salicylic acid C2H402) acetylsalicylic acid (C H3O) он он acetic anhydride acetic acid salicylic acid C2H402) acetylsalicylic acid (C H3O)
10) A student prepares aspirin (acetylsalicylic acid, C,H,0.) by reacting salicylic acid (C,H,O,) with acetic anhydride (C.H.O.). The balanced equation for the reaction is: 2 C,H,O, + C,H,O, + 2 C,H,O, + H,O The lab calls for 3.00 g of salicylic acid to be mixed with 6.40 g of acetic anhydride. What is the limiting reagent and what is the maximum amount of aspirin which can be prepared if the yield for the reaction is 91%?
3. 0.69g of salicylic acid was reacted with 0.6g acetic anhydride in the presence of concentrated phosphoric acid to yield 0.80g of acetyl salicylic acid (see below). Determine the limiting reagent and percent yield. C-CH OH COOH CH, COOH CHC Salicylic acid MW 138.12. mp 159C Acetic anhydride Acetylsalicylic acid M W 102.09. bp 140CMW 180.15. mp 128-1370 4. How do you account for the smell of vinegar when an old bottle of aspirin opened?
1. Mass of salicylic acid (g) 2.0089 5.10ml & 2. Volume of acetic anhydride (mL) Limiting reactant is (circle one): Salicylic Acid or Acetic Anhydride Calculation for Limiting Reactant: 3. Theoretical yield of aspirin (9) Calculation for Theoretical Yield of aspirin: 4. Mass of filter paper 0.3369 N 5. Mass of filter paper + aspirin 2.471g 6. Experimental Yield of aspirin (g) 7. Percent Yield Synthesis of Aspirin An early oral pain reliever, salicylic acid, was determined to cause stomach...
PRELAB EXERCISE EXPERIMENT 21 Synthesis of Aspirin (Acetylsalicylic Acid) What is the purpose of sulfuric acid or phosphoric acid used in the acetylation reaction? Use equations to explain this purpose. The procedure calls for cautious addition of water to the reaction mixture while it is still hot. What purpose does the addition of water serve and why should the addition be done while the reaction mixture is hot? Provide an equation for the reaction involved.Using the quantities of salicylic acid and acetic anhydride...
please help
Mustrates treat all types of ilnesses. Background Aspirin is a prodrug of salicylic acid, the actual active drug. A compound related to salicylic acid, salicin, was first isolated from willow bark in the mid 1700's, but willow-bark extract was used by the andient Greeks as a treatment for pain and fever. Salicylic acid (and many related phenols) are very hard on your Ho stomach, but when esterified, as aspirin is, they are much better tolerated. Simple esters are...
Instructions: Use the following reaction to answer the questions in part ad Tom aspirin acetic acid Salicylic P.M. - 138g/mol acetic anhydride P.M. -102.1g/mol PM180.2g/mol a. Calculate the theoretical yield if 6.0g of salicylic acid are reacted with 12mL of acetic anhydride (density 1.08g/ml) b. What is the limiting REAGENT and what is the excess REAGENT? c. How many moles of excess reagent did not react with the limiting reagent? d. f 6.9 g of aspirin are produced in an...
10. Calculate the theoretical yield of aspirin using 4.00 g of salicylic acid as the starting material. Assume acetic anhydride is in excess. (Hint: from the mass of salicylic acid acid use, how many moles of salycilic acid are present intitially? What is the salycilic acid : acetylsalicylic acid molar ratio? How many moles of acetylsalicylic acid are formed assuming 100% yield? Based on this abount of moles, how many grams of acetylsalicylic acid are formed? (this is the theoretical...
95 Experiment IX Synthesis of Aspirin Prelaboratory Assignment Name: frobect Bun, Bak Baniot Date Sabaitecd Section #. . Using chemical structures, write the balanced equation for the synthesis of aspirin and label all reagents and products with their appropriate names. ooH он C14 14,03 2. What are the two functional groups on salicylic acid? 3. What are the two functional groups on aspirin? b. anhydride? b) How many moles of Apririn could be produced from 2 moles of salicylic acid?...
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