The questions in the first picture are related to the Synthesis of Vanillyl Alcohol from Vanillin...
0.015mol vanillin in ethanol Normally vanillyl alcohol is recovered using filtration. Is it possible for the vanillyl alcohol product from borohydride reduction of vanillin to be captured through extraction and how would it be done?
provide the reaction mechanism for this reaction scheme
OH NaBH4 HO o 5% NaOH, 0 °C Vanillin Vanillyl Alcohol
Organic synthesis fragrance Lab chosen alcohol is benzyl which reacts with acetic anhydride draw the reaction mechanism for the reaction between the anhydride and your alcohol (Benzyl) that resulted in the formation of the ester you synthesized.
Why should trans-2-octene be the most abundant product for the dehydrohalogenation reaction? (From "Synthesis and Dehydrohalogenation of 2-Bromooctane" Organic Chem. 1 Lab)
These questions are about a lab on Grignard Reactions 10. (3) If you had done this reaction in the lab, you would have added the Grignard reagent to a carbonyl containing molecules such as the ones from question 3. After addition the reaction is usually opaque and forms white precipitate, what is the precipitate made of? In other words, what are the salts that form? 11. (3) After these salts have formed, the reaction is quenched with acid, 5 N...
acetic acid is 25 ml and alcohol is 20 ml
The synthesis of an ester by the reaction of a carboxylic with an alcohol is an equilibrium reaction. H - R-OH HO ROH R OR, Recall from general chemistry that, according to Le Caiclista principle, an equilibrium can be shifted toward greater product formation by using an excess of reactant or by removal of a reaction product as it forms. 1. Are any products removed during the reaction period (the...
Ester Synthesis In today's lab, you will perform small scale Fischer esterifications to make a variety of esters. H2SO4 R OH + R'OH = ROR' Combinatorial chemistry is a term used to describe small scale reactions, where in a large number of different molecules can be made using the same reaction conditions, by varying the reactants. In the case of Fischer esterifications, one can vary the carboxylic acid and keep the alcohol constant or keep the carboxylic acid constant and...
Combinatorial Chemistry: Ester Synthesis In today's lab, you will perform small scale Fischer esterifications to make a variety of esters. H2SO4 R OH + R'OH = ROR Combinatorial chemistry is a term used to describe small scale reactions, where in a large number of different molecules can be made using the same reaction conditions, by varying the reactants. In the case of Fischer esterifications, one can vary the carboxylic acid and keep the alcohol constant or keep the carboxylic acid...
Design a scheme and draw the mechanism for the synthesis of the
following compound from benzene and an alkyl halide.
Application Questions 1. Design a scheme and draw the mechanism for the synthesis of the following compound from benzene and an alkyl halide. For the compound in application question one, design a scheme and draw the mechanism for the synthesis from benzene and an alcohol. 2. Explain why you cannot directly form the following compound from a Friedel-Crafts alkylation of...
OCH3 OH from One route to the synthesis of HO and CH,CH2MgBr is to 1) protect the ketone as an acetal, 2) reduce the ester to an alcohol, 3) hydrolyze the acetal back to the ketone, 4) protect the alcohol as a TMS ether, 5) react the ketone with the Grignard reagent followed by acidic workup to give the desired product. A second route to the desired product would start with the selective reduction of only the ketone to an...