Spectroscopy problem. I've given it a go but not sure whether it's correct or not
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Spectroscopy problem. I've given it a go but not sure
whether it's correct or not
Problem...
Deduce the structure based on the information below: Concepts: organic spectroscopy, organic chemistry - Problem 53...
Deduce the structure based on the information below:
Concepts: organic spectroscopy, organic chemistry
- Problem 53 IR Spectrum (liquid film) 4000 3000 1600 1200 . 800 2000 V (cm Mass Spectrum % of baso peak No significant UV absorption above 220 nm 115 M+ 146 40 80 200 240 120 160 m/e 280 13C NMR Spectrum (50.0 MHz, CDC, solution) solvent proton decoupled 200 160 120 80 40 0 8 (ppm) TH NMR Spectrum (200 MHZ, CDCI, solution) TMS LIIIIIIIIIIIIIIIII...
For problems 11-12 answer the questions on the Mass Spectroscopy problem set worksheet. Problem 11 Problem...
For problems 11-12 answer the questions on the Mass Spectroscopy
problem set worksheet.
Problem 11 Problem (z m that IR Spectrum liquid film IR Spectrum oldim 4000 3000 2000 1600 1200 800 4000 3000 2000 V (cm 1800 ) 1200 800 Vom) 0.0 100F Mass Spectrum Mass Spectrum of base peak No significant UV absorption above 220 mm of base 107/109 1015486162 UV spectrum 530 mg/10mis path length: 100 cm solvencyclohexane 120 40 80 120 160 m/e 200 240 280...
Deduce the following structure of the compound given their IR, H1 NMR, 13C NMR spectra, and...
Deduce the following structure of the compound given their IR, H1
NMR, 13C NMR spectra, and assign IR functional group absorptions
and assign the structure's protons and carbons to their respective
spectral resonances.
Compound 6 1756 IR Spectrum uid Sm) 15820 4000 3000 2000 1600 1200 800 V (cm) 100 55 Mass Spectrum 71 80 70 60 No significant UV M158 (1%) absorption above 220 nm C&H140s 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50.0 MHz,...
Attached are four spectra for isomer with the MF= c12h14o4. Determine the structure for each molecule...
Attached are four spectra for isomer with the MF=
c12h14o4. Determine the structure for each molecule and draw them
below.
problem 63 IR Spectrum (CCI, solution) 1765 4000 3000 1200 800 2000 V (cm ) Mass Spectrum UV Spectrum & 8 8 g 8 of base 2 mar 269 nm (10910€ 2.7) humax 263 nm (10910 2.7) M -222 (< 1) 169 sahent: methanol 8 C12H1404 240 280 40 80 120 160 200 13C NMR Spectrum (50.0 MHz, COCI, solution)...
Find the compounds using NMR and IR: Problem 85 IR Spectrum (liquid fiim) 1720 1600 2000...
Find the compounds using NMR and IR:
Problem 85 IR Spectrum (liquid fiim) 1720 1600 2000 v (cm) 800 3000 1200 4000 100 Mass Spectrum 73 140 138 80 No significant UV 60 115 absorption above 220 nm 40 M 194/196 (1% ) 20 CeH1102Br 120 160 200 240 280 40 80 m/e 13C NMR Spectrum (50.0 MHz, CDCI, solution) DEPT CH, Cн, сн! solvent proton decoupled 8 (ppm) 160 120 40 200 80 H NMR Spectrum (200 MHz, CDCI,...
Fall 2019 Problem 5 IR Spectrum (iquid fim) 1715 4000 3000 2000 V (cm) 1600 1200...
Fall 2019 Problem 5 IR Spectrum (iquid fim) 1715 4000 3000 2000 V (cm) 1600 1200 800 100 44 Mass Spectrum 80 60 58 20 M. 86 C5H100 280 40 240 80 200 120 160 13C NMR Spectrum (20.0 MHz, CDCI, solution) -CH3 C-H proton decoupled TMS CH solvent ul 5 (ppm) 40 80 120 160 200 H NMR Spectrum (100 MHz, CDC, solution) expansion of 400 MHz spectrum 20 Hz TMS 0.99 ppm 2.21 2.31 9.75 2 3 6...
Problem 112: treat the peaks at 2.3 ppm as two singlets, as the 1BC NMR confirms. Problem 112 I...
Problem 112: treat the peaks at 2.3 ppm as two singlets, as the 1BC NMR confirms. Problem 112 IR Spectrum 4000 3000 2000 1600 1200 V (cm) Mass Spectrum uv Spectrum 100 A,s. 265 nm (log10ε 2.6) λ max 271 nm 0og10ε 2.6 ) M* 150 solvent: methanol 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100.0 MHz, CDC, solution) 24 20 ppm 24 proton decoupled 200 160 120 80 40 δ (ppm) H NMR Spectrum 400...
Find the compounds using IR and NMR: Problem 25 2251 IR Spectrum (liquid film) 800 1600...
Find the compounds using IR and NMR:
Problem 25 2251 IR Spectrum (liquid film) 800 1600 1200 4000 3000 2000 v (cm) 100 Mass Spectrum M 117 80 77 60 91 40 20 CgH7N 200 80 120 160 240 280 40 m/e expansion 13C NMR Spectrum (100.0 MHz, CDCI, solution) 130 129 ppm DEPT CH Cн,! сн! expansion 130 129 ppm solvent proton decoupled (ppm) 40 200 160 120 80 H NMR Spectrum (400 MHz. CDCI, solution) TMS 10 7...
Can someone please walk through the steps on getting the final structure (boxed towards top)? 7...
Can someone please walk through the steps on getting the final
structure (boxed towards top)?
7 IR Spectrum (liquid film) groups: -- 1712 12771254 c=0 4000 3000 1200 800 2000 1600 V (cm) ;C=0 1001 121 Mass Spectrum 80 601 149 % of base peak 12-7=5 M+ 194 40 20 Label C1, H₂ 40₃ 40 80 200 240 280 120 160 m/e 13C NMR Spectrum (50.0 MHz, CDCI, solution) CH CM (Из CH3 Resolves into two signals at higher field...
need help elucidating this please IR Spectrum KB ) 800 0.0 1200 4000 3000 2000 1600...
need help elucidating this please
IR Spectrum KB ) 800 0.0 1200 4000 3000 2000 1600 V emi) Mass Spectrum Sofbose pak UN spectrum 15 mg/100 ml path length: 02 om solvent: ethanol 1 1.56 200 350 40 80 240 200 120 m 200 160 /e 250 300 2. (nm) 13C NMR Spectrum (50.0 MHz, CDCI, solution) Resolves into two signals at higher field DEPT Chat Chat Cht - Resolves into two signals at higher field solvent proton decoupled 0...
Deduce the structure based on the information below:
Concepts: organic spectroscopy, organic chemistry
- Problem 53 IR Spectrum (liquid film) 4000 3000 1600 1200 . 800 2000 V (cm Mass Spectrum % of baso peak No significant UV absorption above 220 nm 115 M+ 146 40 80 200 240 120 160 m/e 280 13C NMR Spectrum (50.0 MHz, CDC, solution) solvent proton decoupled 200 160 120 80 40 0 8 (ppm) TH NMR Spectrum (200 MHZ, CDCI, solution) TMS LIIIIIIIIIIIIIIIII...
For problems 11-12 answer the questions on the Mass Spectroscopy
problem set worksheet.
Problem 11 Problem (z m that IR Spectrum liquid film IR Spectrum oldim 4000 3000 2000 1600 1200 800 4000 3000 2000 V (cm 1800 ) 1200 800 Vom) 0.0 100F Mass Spectrum Mass Spectrum of base peak No significant UV absorption above 220 mm of base 107/109 1015486162 UV spectrum 530 mg/10mis path length: 100 cm solvencyclohexane 120 40 80 120 160 m/e 200 240 280...
Deduce the following structure of the compound given their IR, H1
NMR, 13C NMR spectra, and assign IR functional group absorptions
and assign the structure's protons and carbons to their respective
spectral resonances.
Compound 6 1756 IR Spectrum uid Sm) 15820 4000 3000 2000 1600 1200 800 V (cm) 100 55 Mass Spectrum 71 80 70 60 No significant UV M158 (1%) absorption above 220 nm C&H140s 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (50.0 MHz,...
Attached are four spectra for isomer with the MF=
c12h14o4. Determine the structure for each molecule and draw them
below.
problem 63 IR Spectrum (CCI, solution) 1765 4000 3000 1200 800 2000 V (cm ) Mass Spectrum UV Spectrum & 8 8 g 8 of base 2 mar 269 nm (10910€ 2.7) humax 263 nm (10910 2.7) M -222 (< 1) 169 sahent: methanol 8 C12H1404 240 280 40 80 120 160 200 13C NMR Spectrum (50.0 MHz, COCI, solution)...
Find the compounds using NMR and IR:
Problem 85 IR Spectrum (liquid fiim) 1720 1600 2000 v (cm) 800 3000 1200 4000 100 Mass Spectrum 73 140 138 80 No significant UV 60 115 absorption above 220 nm 40 M 194/196 (1% ) 20 CeH1102Br 120 160 200 240 280 40 80 m/e 13C NMR Spectrum (50.0 MHz, CDCI, solution) DEPT CH, Cн, сн! solvent proton decoupled 8 (ppm) 160 120 40 200 80 H NMR Spectrum (200 MHz, CDCI,...
Fall 2019 Problem 5 IR Spectrum (iquid fim) 1715 4000 3000 2000 V (cm) 1600 1200 800 100 44 Mass Spectrum 80 60 58 20 M. 86 C5H100 280 40 240 80 200 120 160 13C NMR Spectrum (20.0 MHz, CDCI, solution) -CH3 C-H proton decoupled TMS CH solvent ul 5 (ppm) 40 80 120 160 200 H NMR Spectrum (100 MHz, CDC, solution) expansion of 400 MHz spectrum 20 Hz TMS 0.99 ppm 2.21 2.31 9.75 2 3 6...
Problem 112: treat the peaks at 2.3 ppm as two singlets, as the 1BC NMR confirms. Problem 112 IR Spectrum 4000 3000 2000 1600 1200 V (cm) Mass Spectrum uv Spectrum 100 A,s. 265 nm (log10ε 2.6) λ max 271 nm 0og10ε 2.6 ) M* 150 solvent: methanol 40 80 120 160 200 240 280 m/e 13C NMR Spectrum (100.0 MHz, CDC, solution) 24 20 ppm 24 proton decoupled 200 160 120 80 40 δ (ppm) H NMR Spectrum 400...
Find the compounds using IR and NMR:
Problem 25 2251 IR Spectrum (liquid film) 800 1600 1200 4000 3000 2000 v (cm) 100 Mass Spectrum M 117 80 77 60 91 40 20 CgH7N 200 80 120 160 240 280 40 m/e expansion 13C NMR Spectrum (100.0 MHz, CDCI, solution) 130 129 ppm DEPT CH Cн,! сн! expansion 130 129 ppm solvent proton decoupled (ppm) 40 200 160 120 80 H NMR Spectrum (400 MHz. CDCI, solution) TMS 10 7...
Can someone please walk through the steps on getting the final
structure (boxed towards top)?
7 IR Spectrum (liquid film) groups: -- 1712 12771254 c=0 4000 3000 1200 800 2000 1600 V (cm) ;C=0 1001 121 Mass Spectrum 80 601 149 % of base peak 12-7=5 M+ 194 40 20 Label C1, H₂ 40₃ 40 80 200 240 280 120 160 m/e 13C NMR Spectrum (50.0 MHz, CDCI, solution) CH CM (Из CH3 Resolves into two signals at higher field...
need help elucidating this please
IR Spectrum KB ) 800 0.0 1200 4000 3000 2000 1600 V emi) Mass Spectrum Sofbose pak UN spectrum 15 mg/100 ml path length: 02 om solvent: ethanol 1 1.56 200 350 40 80 240 200 120 m 200 160 /e 250 300 2. (nm) 13C NMR Spectrum (50.0 MHz, CDCI, solution) Resolves into two signals at higher field DEPT Chat Chat Cht - Resolves into two signals at higher field solvent proton decoupled 0...
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