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List two experimental techniques that can provide evidence of the ordered arrangement of pores in templated...

List two experimental techniques that can provide evidence of the ordered arrangement of pores in templated mesoporous silicas. Briefly explain how the evidence is provided in the two cases.

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Microwave assisted technique for the synthesis of mesoporous silica nanoparticles (MSNs). could be another low-cost approach for the synthesis of MSNs. Various reports show that MSNs with ordered pore size and arrangement could be rapidly synthesized by this method

As per IUPAC, mesoporous materials are defined as the one having a pore size in the range of 2–50 nm and an ordered arrangement of pores giving an ordered structure to it .
The pore size of these could be varied and tuned through the choice of surfactants used. Generally, MCM-41 is hexagonal with a pore diameter of 2.5 to 6 nm wherein cationic surfactants were used as templates.
These may vary in their structural arrangement or the pore size.

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