In the Isolation of Caffeine form Excedrin, a) what is the purpose of treating the dichloromethane...
In the Isolation of Caffeine form Excedrin,
a) what is the purpose of treating the dichloromethane extract with aqueous NaHCO3 solution? Write a suitable chemical equation to describe the process.
b) Which component(s) of Excedrin do you expect to find in the organic layer? Draw the structure(s) in the correct ionization states.
c) Which component(s) of Excedrin do you expect to find in the aqueous layer? Draw the structure(s) in the correct ionization states.
Homework Answers
Add Answer to:
In the Isolation of Caffeine form Excedrin,
a) what is the purpose of treating the dichloromethane...
in the isolation of caffeine from excedrin, what is the purpose of treating the dichloromethane extract...
in the isolation of caffeine from excedrin, what is the purpose of treating the dichloromethane extract with aqueous NaHCO3? Also, Write a chemical equation to describe the process.
Solutions??? Lab Partner(s): Isolation of Active Ingredients of Excedrin-Week 1 Task A: Separate the mixture of...
Solutions???
Lab Partner(s): Isolation of Active Ingredients of Excedrin-Week 1 Task A: Separate the mixture of active ingredients of Excedrin from the exciplents in the toblet. 01. Complete the following flowchart. Based on step 1 you performed in the lab. Moture of aspirin, caffeine and acetaminophen along with insoluble excipients Solvent a itrate residue Q3. Based on step 2 you performed, complete the following flowchart to depict the scheme of separation of acetaminophen from insoluble excipients. Mixture of acetaminophen and...
Question 7 (1 point) To extract the reaction product from the aqueous reaction mixture, dichloromethane will...
Question 7 (1 point) To extract the reaction product from the aqueous reaction mixture, dichloromethane will be added and liquid-liquid extraction will be carried out. Which layer will be the organic (dichloromethane) layer? The density of dichloromethane is 1.33 g/mL. bottom layer depends on the day the middle layer top layer Question 1 (1 point) What class of compound do you always get if you reduce an aldehyde? O 2º alcohol O carboxylic acid ketone 1° alcohol
Options for each question: 6 M HCL, 5% HCL solution, Dichloromethane, 6 M NaOH, 5% NaOH...
Options for each question: 6 M
HCL, 5% HCL solution, Dichloromethane, 6 M NaOH, 5% NaOH
solution
Question 8 Status: Not yet answered Points possible: 1.00 When separating benzoic acid, naphthalene, and aniline, identify the solution used for each described purpose. Reconstitute benzoic acid from aqueous layer Choose... Extract benzoic acid into the aqueous layer Choose... Reconstitute aniline from aqueous layer Choose.. Extract aniline into the aqueous layer Choose... Extract reconstituted benzoic acid out of the aqueous layer Choose... Extract...
Based on solubility, density, and polarity information what will happen if a caffeine extraction and sublimation...
Based on solubility, density, and polarity information what will happen if a caffeine extraction and sublimation experiment is carried out at 100°C? (Note: show the outline, the experiment might not work perfectly in the actual lab, but a hypothetical outline is needed). Procedure below: Boil 20mL DI water. Place 1st tea bag in beaker taken off heat and cool to handling temperature. Squeeze tea from bag without breaking it. Boil the mixture. Repeat steps with 2nd teabag. Cool to room...
Answer the following before coming to lab: 1.) Based on what you saw last week, which...
Answer the following before coming to lab: 1.) Based on what you saw last week, which enantiomer of tartaric acid would you expect to co- crystallize with (SS)-1,2-diammoniumcyclohexane? 2.) If you had a neutral aqueous solution of triethylamine, would you add acid or base in order to extract it with an organic solvent? 3.) Now, consider a dichloromethane solution of triethylamine. Would you extract with acidic aqueous or basic aqueous solution in order to get the triethylamine out of the...
1.) What percent recovery could be expected if 1.000 g of caffeine was initially dissolved in...
1.) What percent recovery could be expected if 1.000 g of
caffeine was initially dissolved in 120 mL of water and then
extracted with a single 80 mL portion of ethyl acetate?
2.) What percent recovery could be expected if 1.000 g of
caffeine was initially dissolved in 120 mL of water and then
extracted as per the protocol given in the lab manual?
3.) Percent recovery and percent yield are occasionally used as
if they are interchangeable terms. They...
Post lab question 1. What can you do if you do not know which layer is...
Post lab question 1. What can you do if you do not know which layer is which in an extraction procedure? 2. Consider the densities of the following pairs of liquids. Which liquid would you expect (which is the organic layer and which is the aqueous layer? to be on top and which will be on the bottom? Do all the liquids form two layers? a. Hexane and water b. Ethanol and water c. Dichloromethane and water d. Ethyl acetate...
Introduction: The technique used to separate an organic compound from a mixture of compounds is called...
Introduction: The technique used to separate an organic compound from a mixture of compounds is called Extraction. Extraction process selectively dissolves one or more of the mixture compounds into a suitable solvent. The solution of these dissolved compounds is referred to as the Extract. Here the organic solvent dichloromethane is used to extract caffeine from an aqueous extract of tea leaves because caffeine is more soluble in dichloromethane (140 mg/ml) than it is in water (22 mg/ml). However, there are...
Extraction of solids: Experiment outlined below Draw a “roadmap” of the experiment, containing chemical structures and...
Extraction of solids: Experiment outlined below
Draw a “roadmap” of the experiment, containing chemical
structures and “layers” (organic and aqueous). This should contain
the individual reactions occurring in each step, and show which
layer the various components are present. Make sure you think about
whether the acetaminophen, caffeine and aspirin are neutral,
protonated or deprotonated.
Preliminary separation obtain a sample (1.0g) of the mixture. weigh the sample and record it. this sample should consist of a 2:1:1 mixture (by mass)...
Solutions???
Lab Partner(s): Isolation of Active Ingredients of Excedrin-Week 1 Task A: Separate the mixture of active ingredients of Excedrin from the exciplents in the toblet. 01. Complete the following flowchart. Based on step 1 you performed in the lab. Moture of aspirin, caffeine and acetaminophen along with insoluble excipients Solvent a itrate residue Q3. Based on step 2 you performed, complete the following flowchart to depict the scheme of separation of acetaminophen from insoluble excipients. Mixture of acetaminophen and...
Question 7 (1 point) To extract the reaction product from the aqueous reaction mixture, dichloromethane will be added and liquid-liquid extraction will be carried out. Which layer will be the organic (dichloromethane) layer? The density of dichloromethane is 1.33 g/mL. bottom layer depends on the day the middle layer top layer Question 1 (1 point) What class of compound do you always get if you reduce an aldehyde? O 2º alcohol O carboxylic acid ketone 1° alcohol
Options for each question: 6 M
HCL, 5% HCL solution, Dichloromethane, 6 M NaOH, 5% NaOH
solution
Question 8 Status: Not yet answered Points possible: 1.00 When separating benzoic acid, naphthalene, and aniline, identify the solution used for each described purpose. Reconstitute benzoic acid from aqueous layer Choose... Extract benzoic acid into the aqueous layer Choose... Reconstitute aniline from aqueous layer Choose.. Extract aniline into the aqueous layer Choose... Extract reconstituted benzoic acid out of the aqueous layer Choose... Extract...
Answer the following before coming to lab: 1.) Based on what you saw last week, which enantiomer of tartaric acid would you expect to co- crystallize with (SS)-1,2-diammoniumcyclohexane? 2.) If you had a neutral aqueous solution of triethylamine, would you add acid or base in order to extract it with an organic solvent? 3.) Now, consider a dichloromethane solution of triethylamine. Would you extract with acidic aqueous or basic aqueous solution in order to get the triethylamine out of the...
1.) What percent recovery could be expected if 1.000 g of
caffeine was initially dissolved in 120 mL of water and then
extracted with a single 80 mL portion of ethyl acetate?
2.) What percent recovery could be expected if 1.000 g of
caffeine was initially dissolved in 120 mL of water and then
extracted as per the protocol given in the lab manual?
3.) Percent recovery and percent yield are occasionally used as
if they are interchangeable terms. They...
Post lab question 1. What can you do if you do not know which layer is which in an extraction procedure? 2. Consider the densities of the following pairs of liquids. Which liquid would you expect (which is the organic layer and which is the aqueous layer? to be on top and which will be on the bottom? Do all the liquids form two layers? a. Hexane and water b. Ethanol and water c. Dichloromethane and water d. Ethyl acetate...
Extraction of solids: Experiment outlined below
Draw a “roadmap” of the experiment, containing chemical
structures and “layers” (organic and aqueous). This should contain
the individual reactions occurring in each step, and show which
layer the various components are present. Make sure you think about
whether the acetaminophen, caffeine and aspirin are neutral,
protonated or deprotonated.
Preliminary separation obtain a sample (1.0g) of the mixture. weigh the sample and record it. this sample should consist of a 2:1:1 mixture (by mass)...
Most questions answered within 3 hours.
-
10. Complete the table below
only using hexadecimal numbers:
AL CODE
EBX
EAX
[EAX]
mov eax,...
asked 14 minutes ago -
trust is best established through the combination of ------and
------- .
1. magnanimity and justice
2....
asked 29 minutes ago -
Blood pressure is normally taken on the upper arm at the level
of the heart. Suppose,...
asked 28 minutes ago -
Suppose that the satellite around the earth has an orbit that is
24 KM larger in...
asked 31 minutes ago -
Calculate the [OH (aq)] in limes which have a [H3O*(aq)] of 1.3 x
10 mol/L
asked 29 minutes ago -
A nozzle with a radius of 0.250 cm is attached to a garden hose
with a...
asked 40 minutes ago -
PLEASE do not use any loops for the program; only recursion is
allowed
4. Write a...
asked 49 minutes ago -
Please help me with me. I did the first part to write the operations but in...
asked 46 minutes ago -
Use Cryptool to find the Cryptographic SHA-1 hash value of the
string "abc". The calculator is...
asked 51 minutes ago -
You are attempting to calculate a firm’s free cash flow to
equity. You know the following...
asked 1 hour ago -
the following reaction occurs in a balloon containing
N2O2 gas
N2O4(g)=2NO2(g)
will the volume of the...
asked 2 hours ago -
answer the questions throughout this program
public class Day implements Comparable {
Private Boolean atWork;...
asked 2 hours ago