what kind of information about a compound do you get from melting point? Thin layer chromatography? How could these be useful in assessing the product of a chemical reaction?
MELTING POINT melting point is the temperature at which the chemical compound start melting. Every compound has specific melting point. So melting point is used to determine the product and purity of the product in the chemical reaction . while assessing the product of the chemical reaction we determine the melting point first if it suits the melting point of the product required, we will primarily confirm that reaction is going in correct process and we are getting the correct product.
if there is a decrease in melting point we can confirm that there is impurity in the product obtained.
THIN LAYER CHROMATOGRAPHY In TLC the stationary phase is solid and the mobile phase is liquid. Different compounds have different absorption properties and move with different speed when applied on the TLC plate.
As different chemical compounds have different mobility on TLC they have different Rf values [ Rf valule is defined as the mobility of the compound to that of mobile phase] that means each compound have a specific Rf values.
while assessing the product of the chemical reaction if the Rf value of the obtained product matches the predetermined Rf value of the product we will confirm the reaction is going in the correct process and we are getting the correct product
what kind of information about a compound do you get from melting point? Thin layer chromatography?...
Wanting to monitor the reaction progress you decide to use normal phase thin-layer chromatography, but do not know what the best conditions are to use. If you had the standards for all potential products and your starting materials, outline how would you go about determining the best TLC conditions for monitoring the reaction progress. Provide drawings of an ideal TLC plate with the number of theoretical products you would expect and their relative positions. How do you know when the...
11. Why should you use pencil instead of pen when marking on a thin layer chromatography plate? a. Pencil lead isn't as dark. b. The components of pen ink will separate along with your sample, while pencil lead will not. c. Pen ink will not mark on a TLC plate. d. Pen ink will undergo a chemical reaction with the solvent. 12. Which of the following is not a reason to use thin-layer chromatography? a. To determine the number of...
Thin layer chromatography is used for (select all that apply) 1. following the course of a reaction. 2. determining the number of compounds in a mixture. , helping to establish if two compounds have identical retention times under the same TLC conditions. 4. determining the melting point of a solid sample. determining the number and types of bonds present in a compound.
6. How was thin-layer chromatography utilized in the aspartame experiment? (In other words, what type of information could be revealed by this technique in the experiment?)
Thin Layer Chromatography: One spot with an RF of .62 is observed after you develop the TLC of a reaction mixture. Does this prove that you have only one product present? Explain.
Why is thin layer chromatography used to determine the purity of a sample when you could use an IR spectrum? How does TLC confirm the purity?
Laboratory Instructor STUDENT REPORT A. Data Sheet EXPERIMENT 28 Aspartame 1. Thin-layer chromatography Distance traveled by solvent (1) Substance Distance teweled DR value Calculations: 2. KMnO, test Observations 10 min. 15 min. Reaction? 5 min. Substance 1092 330 Exploring Chemistry 3. Cari nitrate test B. Reflective Exercises and phenylalanine columns on the 1. How many spots should be seen for each of the aspartic acid and price chromatogram? Why? 2. Referring to the chromatogram, what did you here and what...
2. An unknown compound was analyzed using thin layer chromatography, its constituted of two components (A and B) as shown in the TLC (Silica coated stationary phase; Chloroform and Ethyl acetate as mobile phase). The mixture was then loaded onto column with silica as the stationary phase and the same solvent system was used. (2 points) Column Chromatography TLC time A В Predict the order of elution of the compounds (A and B). which one would be eluted first/last and...
Page 1 of 2 Exp. 3 Isolation of Caffeine from Instant Coffee: Extraction and Thin Layer Chromatography Please provide each question you answer. Pre-Lab 1. Explain what a "partition or distribution" coefficient is. Use a dra coefficient of 3. 2. Explain how centrifugation works and critical safety consideration 3. Explain what anhydrous calcium chloride is and what it does in thi 4. Explain how thin layer chromatography works, what an Rt signifie 5. If the above squares are the display...
Decide what kind of crystalline solid each element or compound in the table forms, and what kind of force holds the solid together. Then, rank the solids in order of decreasing melting point. That Is, select "1" next to the solid with the highest melting point, "2" next to the solid w highest melting point, and so on. CYou may need to use the scrollbar to see all the choices.) type of solid force holding the solid melting point o...