What would happen if you had used a 1:1 mixture of ethyl acetate instead of hexane to elute your column? Would the product (DEET) have come out faster or slower? Would this have improved your separation, or made it worse?
What would happen if you had used a 1:1 mixture of ethyl acetate instead of hexane...
Common solvents used in TLC analysis are hexane and ethyl acetate, the latter being more polar. A TLC has been performed on a mixture of two compounds. The solvent ran for 3 cm(plate length is 6cm) with 5% ethyl acetate in hexane. The two spots were not resolved, meaning they showed up too close to each other. What can you suggest to possible improve the results of the separation?
4. (6 points) What is the condensation product if diethyl malonate is used instead of ethyl acetoacetate? но. но н* heat resorcinol diethyl malonate 1) Is this reaction faster or slower than the reaction with ethyl acetoacetate? 2) Explain why.
Question 10 1 pts What hazard classification would you expect a 90% ethyl acetate/10% hexane mixture to have? Flammable liquid Corrosive Toxic Flammable solid Question 16 1 pts The TLC diagram shown represents the analysis of three different compounds. Which of the three columns is/are likely to represent a pure compound, and why? 0 0 2 * 3 Columns 1 and 3, because there is only one spot in each. Column 2 only, because there are two spots present Columns...
A simple distillation was performed to separate a mixture containing both hexane and heptane. Explain why the observed starting vapor temperature in the simple distillation should be above the boiling point of hexane. Then, explain why if a fractional distillation was performed instead you would have a better separation (be sure to include how the fractionating column works in your explanation).
If you had stearic acid in a hexane solution and some of the hexane evaporated, what would happen to the Avogadro’s number and why? Thank you.
1) When you measured out one mL of the trans-1,2-dibenzoylethylene in ethyl acetate solution it had a mass of 0.890 grams. (0.050 g of yellow solid and rest of it is Ethyl acetate). The forerun of ethyl acetate had a mass of 0.075g and the rest of the ethyl acetate collected had a mass of 0.253 g. The trans-1,2-dibenzoylethylene had a mass of 0.046 g. What is the percent recovery of each of the materials?
can you please answer all 1. When you run a TLC of the reaction in ethyl acetate : hexanes 1:1, the plate below is produced. Give a solvent system that would be expected to produce greater separation and a BRIEF (8 words) justification about your choice. (5 points) 7 6 5 4 3 b. Calculate the R for the bottom spot. (5 points) c. Which compound on the TLC plate is the most polar? (5 points) 2. Why is it...
2. Aliquid mixture contains two substances whose boiling points are only 10°C apart. Which method of distillation should be utilized to obtain a clean separation of the two substances. Explain. 3. Which of the following pairs of liquids could be separated by simple distillation? Why? a. Ethyl acetate (b.p. 77°C) & Phenol (b.p. 181.7°C) b. Cyclohexane (b.p. 80.7°C) & Toluene (b.p. 111C) C. Hexane (b.p. 69.10C) & Ethylbenzene (b.p. 136°C) 4. What effect would (a) an increase or (b) a...
1. What is the purpose of column chromatography 2. What is the stationary phase? Mobile phase? 3. What is the purpose of the cotton (glass wool) in column chromatography? 4. What is the purpose of the sand? 5. Why is it important to prevent the column from drying? 6. What can happen if you disrupt your even layer of silica gel? 7. Which compounds come off the column first, polar or nonpolar? 8. Keyon synthesized acetylferrocene (orange) in organic chemistry...
These questions are from an experiment where we had a mixture of Ferrocene, acetylferrocene and diacetyl ferrocene and we separated each by using column chromatography. Before doing the column chromatography we did TLC analysis to ensure that we did, in fact, have a mixture of these 3 compounds. During the column chromatography we first eluted the ferrocene using pure hexane. Then we eluted the acetylferrocene using a 1:1 mixture of hexane and methylene chloride. Then we eluted the diacetylferrocene using...