what about the capillary tube doesn't affect the melting point?
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* A student cools a sample in a capillary tube after melting it. Upon attempting to determine the melting point on the same sample, the stjudent does not obtain the same melting point. Why? . A student places his TLC plate in a chamber where the solvent level is higher than the starting line on the TLC. How does that affect the experiment? . A student leaves off the top of her TLC chamber. How will that affect her Rf...
A student performs two melting-point determinations on a crystalline product. In one determination, the capillary tube contains a sample about 1−2 mm in height and the melting range is found to be 141−142°C. In the other determination, the sample height is 4−5 mm and the melting range is found to be 141−145°C. Explain the broader melting-point range observed for the second sample. The reported melting point for the compound is 143°C. Explain what may have caused the broader melting range...
In melting point experiment, (we use benzoic acid (solid),acetanilide (solid) and we put them in capillary tube and let them heat with thiele tube.) why Raoult's law is related to melting point? I think Raoult's law is only in liquid. please make me understand.. How solids are interact with each other as liquid?
Post lab questions for chromatography and melting point lab. i have a few ideas of what the answers to these questions should be, but I would like to double check. if anyone can help me, that would be so awesome. Thank you! A student cools a sample in a capillary tube after melting it. Upon attempting to determine the melting point on the same sample, the student does not obtain the same melting point. Why? A student places his TLC...
Question 1 5 pts - What is the purpose of melting point? All the answers To check the purity of solids To check identity of unkown solids To publish for new solids for future characterization Question 2 5 pts How does impurity change melting point value and range? increase-narrowing decrease-narrowing decrease-broadening O increase-broadening Question 3 5 pts What is the reason of an impurity affecting melting point of a solid? Watch Mel. Point Theory video. Not known Obc it weakens...
Question 1 5 pts - What is the purpose of melting point? All the answers To check the purity of solids To check identity of unkown solids To publish for new solids for future characterization Question 2 5 pts How does impurity change melting point value and range? increase-narrowing decrease-narrowing decrease-broadening O increase-broadening Question 3 5 pts What is the reason of an impurity affecting melting point of a solid? Watch Mel. Point Theory video. Not known Obc it weakens...
- A student is trying to identify an unknown solid based on its melting point. She noted that the compound began to melt at 182°C and finished melting at 187°C. Knowing it is possible for there to be impurities in the sample, is this compound more likely to be camphor or hydroquinone. Explain your reasoning. A young chemist has synthesized what he believed to be acetaminophen. He measured the melting point of this newly formed compound to be 163-178°C. If...
2. Some compounds sublime in the capillary and some decompose before melting. How do you determine melting point of these compounds
When performing a melting point on a solid compound, 2 melting point determinations were made. One sample, which was 1 mm in height in the capillary, possessed a melting point of 150-151°C. The other sample was 25 mm in height. What would you expect the approximate melting point to be for this 25 mm sample, if the heating rate for both samples was 2 degrees per minute? (Hint: use algebra to solve the mp range) 4.
True/False When determining a melting point, it is desirable to use as much material as possible, thus ensuring that you can observe a true equilibrium between solid and liquid phases. True/False Although a preliminary melting point can be done quickly to get an estimate of the approximate melting range, a sharp and accurate melting point value requires heating no faster than 1o – 2o per minute. True/False If you wish to repeat a melting point experiment, it is desirable to...