K2CO3 C7HgO Mol. Wt.: 106.12 bp: 178°C C4H6O3 Mol. Wt.: 102.09 CgHgO2 Mol. Wt.: 148.16 bp: 140°C mp: 135°C
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Compound Benzaldehyde Amount moles equivalents MW (g/mol) Density (g/mL) 106.1 138.2 102.1 K2CO3 ...
Please help answer P1-P4 for this Perkin Reaction Lab Perkin Reaction Organic REActivity PERKIN REACTION (ALDOL...
Please help answer P1-P4 for this Perkin Reaction Lab
Perkin Reaction Organic REActivity PERKIN REACTION (ALDOL CONDENSATION) The Reaction Scheme: Formation of trans-cinnamic acid The following reaction is named the Perkin Reaction. It is a very specific type of Aldol condensation that forms a variety of cinnamic acid derivatives. In this lab, you will perform a Perkin reaction using benzaldehyde and potassium carbonate in acetic anhydride to form trans- cinnamic acid (1). Trans-cinnamic acid is a natural compound found in...
How many moles of benzaldehyde (density d = 1.04 g/ml), (molecular weight mw = 106.12 g/mol)...
How many moles of benzaldehyde (density d = 1.04 g/ml), (molecular weight mw = 106.12 g/mol) are required to react with 1.0 ml of acetone: (density d = 0.79 g/ml), (molecular weight mw = 58.08 g/mol)? 6. What is approximate theoretical yield for problem # 5 if you obtained 2.1 grams of dibenzylidene acetone (mw = 234.29 g/mol)?
find limiting reagent? acetone 3.63 mL benzaldehyde 10.5mL bp (°C) mol. wt. (g/mole) 58.08 density (g/mL)...
find limiting reagent?
acetone 3.63 mL
benzaldehyde 10.5mL
bp (°C) mol. wt. (g/mole) 58.08 density (g/mL) 0.791 56 106.23 178-179 1.044 Acetone Benzaldehyde NaOH Dibenzalacetone 40.00 234.30 mp 110-111 9. Calculations for synthesis-moles of reactants, limiting reagent, theoretical yield , % experimental yield, show all math
10. In the preparation of acetanilide, 4 mL of aniline (Density= 1.02 g/mL; MW=92.13g/mol) and 5...
10. In the preparation of acetanilide, 4 mL of aniline (Density= 1.02 g/mL; MW=92.13g/mol) and 5 mL of acetic anhydride (Density=1.08 g/mL; MW=102.09 g/mol) was used for synthesis of 3.2 grams of acetanilide (MW=135.17 g/mol). Please show your work. (12 pts) a) What is the limiting reagent during the reaction? b) What is the percent yield for acetanilide?
2 dibenzalacetone acetone benzaldehyde MW- 106.13 g/mol bp-1 78°C d 1.04 g/mL MW 234.30 g/mol mp #110-1110 MW-58.08 g/mol bp 56°C d 0.79 g/mL Its bs Reaction Setup (3 pts) S. OS Initial quant...
2 dibenzalacetone acetone benzaldehyde MW- 106.13 g/mol bp-1 78°C d 1.04 g/mL MW 234.30 g/mol mp #110-1110 MW-58.08 g/mol bp 56°C d 0.79 g/mL Its bs Reaction Setup (3 pts) S. OS Initial quantity of NaOH: S. I Initial quantity of benzaldehyde: mL Initial quantity of acetone: mL Theoretical yield of dibenzalacetone based on benzaldehyde: (show calculations) Theoretical yield of dibenzalacetone based on acetone 9 (show calculations) ce tone Limiting Reagent: Product Data (10 pts) fivAL Mass: 3.3g Percent Yield:...
How do I calculate theoretical yield? Crude data mass :.065g colorless liquid yield: 66.2% Purified data...
How do I calculate theoretical yield?
Crude data
mass :.065g colorless liquid
yield: 66.2%
Purified data
pure mass: not collected
pure yield: 65.0%
TEMPO O. CH2Cl2 KBr, NaOCI NaHCO3, H20 C7H30 Mol. Wt.: 108.14 bp: 205°C C7H60 Mol. Wt.: 106.12 bp: 178°C Compound Amount Moles Equivalents MW(g/mol) Benzyl Alcohol 0.100g 9.25 x 10-4 1 108.14 TEMPO(0.005M) 2mL 9.25 x 10-6 0.01 156.25 KBT 0.011g 9.25 x 10-5 0.1 119.00 NaOCI Soln (bleach) 2mL 1.3%soln.(N/A) 0.4 N/A NaHCO3 0.039g 4.625 x...
how do i calculate yield % and pure yield %?? I know i have to balance...
how do i calculate yield % and pure yield %??
I know i have to balance an equation first but C7H8O-> C7H6O
does not make sense to me...
I believe benzyl alcohol is the limiting reagent
>N TEMPO O. CH2Cl2 KBr, NaOCI NaHCO3, H20 CyH2O Mol. Wt.: 108.14 I wo bp: 205°C V CyH60 Mol. Wt.: 106.12 bp: 178°C Crude data Student Data: Purified data (Silica Gel Column - see protocol for conditions) Pure mass: Not collected Pure yield: %...
Complete the following table Compound MW (g/mol) Density (g/mL) BP (°C) MP (°C) Benzonitrile Sodium Hydroxide...
Complete the following table Compound MW (g/mol) Density (g/mL) BP (°C) MP (°C) Benzonitrile Sodium Hydroxide Hydrochloric Acid Concentration Concentration Concentration Dependent Dependent Dependent Benzoic Acid
K2CO3 1.5 H20 Br он heat 2,3-dibromocinnamic acid trans-1-bromo-2-phenylethene Compound MW mp (C)bp (C) density (g/ml)...
K2CO3 1.5 H20 Br он heat 2,3-dibromocinnamic acid trans-1-bromo-2-phenylethene Compound MW mp (C)bp (C) density (g/ml) mol) 2,3-dibromocinnamic acid 307.97 93-95 (threo) n'a n a 202-204 (erythro)E K CO.1.5H:O1 methylene chloride 138.21 84.93 56.11 891 na n a n'a 39.6 n a n a 1.33 n a 3 MKOH 2. a. What is the by-product formed in this reaction (not shown in given reaction equation)? b. What is the purpose of adding 3 M KOH at the beginning of the...
Please help answer P1-P4 for this Perkin Reaction Lab
Perkin Reaction Organic REActivity PERKIN REACTION (ALDOL CONDENSATION) The Reaction Scheme: Formation of trans-cinnamic acid The following reaction is named the Perkin Reaction. It is a very specific type of Aldol condensation that forms a variety of cinnamic acid derivatives. In this lab, you will perform a Perkin reaction using benzaldehyde and potassium carbonate in acetic anhydride to form trans- cinnamic acid (1). Trans-cinnamic acid is a natural compound found in...
find limiting reagent?
acetone 3.63 mL
benzaldehyde 10.5mL
bp (°C) mol. wt. (g/mole) 58.08 density (g/mL) 0.791 56 106.23 178-179 1.044 Acetone Benzaldehyde NaOH Dibenzalacetone 40.00 234.30 mp 110-111 9. Calculations for synthesis-moles of reactants, limiting reagent, theoretical yield , % experimental yield, show all math
10. In the preparation of acetanilide, 4 mL of aniline (Density= 1.02 g/mL; MW=92.13g/mol) and 5 mL of acetic anhydride (Density=1.08 g/mL; MW=102.09 g/mol) was used for synthesis of 3.2 grams of acetanilide (MW=135.17 g/mol). Please show your work. (12 pts) a) What is the limiting reagent during the reaction? b) What is the percent yield for acetanilide?
2 dibenzalacetone acetone benzaldehyde MW- 106.13 g/mol bp-1 78°C d 1.04 g/mL MW 234.30 g/mol mp #110-1110 MW-58.08 g/mol bp 56°C d 0.79 g/mL Its bs Reaction Setup (3 pts) S. OS Initial quantity of NaOH: S. I Initial quantity of benzaldehyde: mL Initial quantity of acetone: mL Theoretical yield of dibenzalacetone based on benzaldehyde: (show calculations) Theoretical yield of dibenzalacetone based on acetone 9 (show calculations) ce tone Limiting Reagent: Product Data (10 pts) fivAL Mass: 3.3g Percent Yield:...
How do I calculate theoretical yield?
Crude data
mass :.065g colorless liquid
yield: 66.2%
Purified data
pure mass: not collected
pure yield: 65.0%
TEMPO O. CH2Cl2 KBr, NaOCI NaHCO3, H20 C7H30 Mol. Wt.: 108.14 bp: 205°C C7H60 Mol. Wt.: 106.12 bp: 178°C Compound Amount Moles Equivalents MW(g/mol) Benzyl Alcohol 0.100g 9.25 x 10-4 1 108.14 TEMPO(0.005M) 2mL 9.25 x 10-6 0.01 156.25 KBT 0.011g 9.25 x 10-5 0.1 119.00 NaOCI Soln (bleach) 2mL 1.3%soln.(N/A) 0.4 N/A NaHCO3 0.039g 4.625 x...
how do i calculate yield % and pure yield %??
I know i have to balance an equation first but C7H8O-> C7H6O
does not make sense to me...
I believe benzyl alcohol is the limiting reagent
>N TEMPO O. CH2Cl2 KBr, NaOCI NaHCO3, H20 CyH2O Mol. Wt.: 108.14 I wo bp: 205°C V CyH60 Mol. Wt.: 106.12 bp: 178°C Crude data Student Data: Purified data (Silica Gel Column - see protocol for conditions) Pure mass: Not collected Pure yield: %...
Complete the following table Compound MW (g/mol) Density (g/mL) BP (°C) MP (°C) Benzonitrile Sodium Hydroxide Hydrochloric Acid Concentration Concentration Concentration Dependent Dependent Dependent Benzoic Acid
K2CO3 1.5 H20 Br он heat 2,3-dibromocinnamic acid trans-1-bromo-2-phenylethene Compound MW mp (C)bp (C) density (g/ml) mol) 2,3-dibromocinnamic acid 307.97 93-95 (threo) n'a n a 202-204 (erythro)E K CO.1.5H:O1 methylene chloride 138.21 84.93 56.11 891 na n a n'a 39.6 n a n a 1.33 n a 3 MKOH 2. a. What is the by-product formed in this reaction (not shown in given reaction equation)? b. What is the purpose of adding 3 M KOH at the beginning of the...
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