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Complete the reaction table above, including the quantities you used in the reaction, prior to th...
fill in the blanks please! Pre-Lab for Lidocaine Analog Synthesis - Step 2 Complete the reaction...
fill in the blanks please!
Pre-Lab for Lidocaine Analog Synthesis - Step 2 Complete the reaction table above, including the quantities you used in the reaction, prior to the addition of extra diethylamine. HN Toluene HAN 1 + 2 HN Reflux a-chloro-2,6- dimethylacetanilide piperidine Toluene N-(2,6-dimethylphenyl)-2- (piperidin-1-yl)acetamide FW g/mol g/mol g/mol g/mL Amount mg mL g (Theory) (Theory) mmol Equivs.
Pre-Lab for Lidocaine Analog Synthesis Step 1 1) Complete the reaction table below with the expected quantities use...
Pre-Lab for Lidocaine Analog Synthesis Step 1 1) Complete the reaction table below with the expected quantities used and obtained in this reaction NH2 HN 1) ACOH 2) Na Chloroacetyl chloride 2,6- Sodium a-chloro-2,6- Acetic acid dimethylace tanilide dimethylaniline acetate 0.4 M (aq) FW g/mol g/mol g/mol g/mL g/mL Amount g (Theory) mL mL mL mL (Theory) mmol Equivs 1.0 1.1 2) Draw the mechan is m of this amide formation (you can look up nucleophilic acyl substitution reactio ns...
1) Complete the table below in your notebooks and as a pre-lab. Look up the density...
1) Complete the table below in your notebooks and as a pre-lab. Look up the density of acetyl chloride and m.p. of biphenyl on the web (10 pts). CH Cb reflux AICI: C4H20 Biphenyl C12H10 Acetyl Chloride CH3CIO Methylene chloride CH2Cl2 MW (g/mol) 154.2 78.5 133.3 196.2 mg 0.1 mL mg 6 mL Qty. measured Amount (mmol) Stoich. Equivs. mg (theory) (theory) 1.5 3.75 m.p. (°C) (6.p.) Dens. (g/mL)
using the procedure above complete the stoichiometry table Procedure In an oven-dried, 100 ml round bottom...
using the procedure above complete the stoichiometry
table
Procedure In an oven-dried, 100 ml round bottom flask containing magnetic stirring bar was added hydrobenzoin (1.0 8.4.7 mmol), anhydrous iron(III) chloride (0.3 g, 1.8 mmol), and anhydrous acetone (30 ml). The mixture was heated to reflux and stirred for 30 min. The reaction mixture was cooled tort and transferred to a separatory funnel containing 10% aq potassium carbonate (10 mL). Water (50 mL) was added and the aqueous solution was extracted...
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepa...
i need help with the postlab questions please
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
fill in the blanks please!
Pre-Lab for Lidocaine Analog Synthesis - Step 2 Complete the reaction table above, including the quantities you used in the reaction, prior to the addition of extra diethylamine. HN Toluene HAN 1 + 2 HN Reflux a-chloro-2,6- dimethylacetanilide piperidine Toluene N-(2,6-dimethylphenyl)-2- (piperidin-1-yl)acetamide FW g/mol g/mol g/mol g/mL Amount mg mL g (Theory) (Theory) mmol Equivs.
Pre-Lab for Lidocaine Analog Synthesis Step 1 1) Complete the reaction table below with the expected quantities used and obtained in this reaction NH2 HN 1) ACOH 2) Na Chloroacetyl chloride 2,6- Sodium a-chloro-2,6- Acetic acid dimethylace tanilide dimethylaniline acetate 0.4 M (aq) FW g/mol g/mol g/mol g/mL g/mL Amount g (Theory) mL mL mL mL (Theory) mmol Equivs 1.0 1.1 2) Draw the mechan is m of this amide formation (you can look up nucleophilic acyl substitution reactio ns...
1) Complete the table below in your notebooks and as a pre-lab. Look up the density of acetyl chloride and m.p. of biphenyl on the web (10 pts). CH Cb reflux AICI: C4H20 Biphenyl C12H10 Acetyl Chloride CH3CIO Methylene chloride CH2Cl2 MW (g/mol) 154.2 78.5 133.3 196.2 mg 0.1 mL mg 6 mL Qty. measured Amount (mmol) Stoich. Equivs. mg (theory) (theory) 1.5 3.75 m.p. (°C) (6.p.) Dens. (g/mL)
using the procedure above complete the stoichiometry
table
Procedure In an oven-dried, 100 ml round bottom flask containing magnetic stirring bar was added hydrobenzoin (1.0 8.4.7 mmol), anhydrous iron(III) chloride (0.3 g, 1.8 mmol), and anhydrous acetone (30 ml). The mixture was heated to reflux and stirred for 30 min. The reaction mixture was cooled tort and transferred to a separatory funnel containing 10% aq potassium carbonate (10 mL). Water (50 mL) was added and the aqueous solution was extracted...
i need help with the postlab questions please
Grignard reagent THE GRIGNARD REAGENT-PREPARATION AND REACTION In this experiment, you will prepare a Grignard reagent, phenyl magnesium bromide, from bromobenzene and magnesium metal. The Grignard reagent will then react with methyl benzoate to form triphenylmethanol. Introduction Grignard reagents, such as organomagnesium halides, were discovered in 1910 by French chemist Victor Grignard. The Grignard reaction is one of the most general methods for carbon- carbon bond formation in all of organic chemistry....
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