How can you tell that a compound has decomposed on melting and how do impurities affect the melting point of a pure compound?
When a compound decomposed it give some product. So, if during melting the color of the compound was changed or evolution of gas takes place then it means compound get decomposed.
Presence of impurities in a sample always lowered the melting point.
How can you tell that a compound has decomposed on melting and how do impurities affect the melting point of a pure comp...
help pls Why do soluble impurities affect the melting point while insoluble impurities are expected not to affect the melting point? (3 points) Student ID: Section: Mention at least one technique that you have learned during 3210 Ta separating a mixture containing anthracene and toluic acid in 1:1 ratio. Assume luble in ether. Sketch an outline of the separation procedure you will perform in the lab (4 points)
Recrystallization: Percent error of melting point and how impurities affect melting point: Please explain both questions below: (Part A) During a recrystallization experiment, the literature melting point of a compound is 105-107 °C. The melting point temperature you obtain from your recrystallized compound is 103-105 °C. Which of the following would be the proper way to set up the percent error of your mp? (a) (104/106)*100 (b) [(106-104)/106] *100 (c) (107/105)*100 (d) [(107-105)/107] *100 (Part B) For a recrystallization experiment...
1. Why do soluble impurities affect the melting point while insoluble impurities are expected not to affect the melting point? (3 points) 2. Why cold solvents are preferred during recrystallization and when is recrystallization selected vs other purification techniques you have learned during 3210 labs. (3 points) 3. The solid compound "X" has two components (A and B). After heating the solid powder (X), one component (A) is left and the other component (B) evaporated directly. Comment on the nature...
What are soluble impurities. (b) Do soluble impurities in solids effect the melting point of the sample? if so, what are the effects?(c) What are insoluble impurities? (d) Do insoluble impurities in solids effect the melting point of the sample? if so , what are the effects?
Question 14 The melting point of a pure compound is known to be 110-111°. Describe the melting behavior expected if this compound is contaminated with 5% of an impurity. 90-96 111-113 90-91 110-111 5 pts Question 15 You and your lab partner take melting points of the same sample. You observe a melting point of 101-107°C, while your partner observes a value of 110-112°C. Explain how you can get two different values with exactly the same sample. One of the...
Question 14 The melting point of a pure compound is known to be 110-111º. Describe the melting behavior expected if this compound is contaminated with 5% of an impurity. 90-96 111-113 90-91 110-111 5 pts Question 15 You and your lab partner take melting points of the same sample. You observe a melting point of 101-107°C, while your partner observes a value of 110-112°C. Explain how you can get two different values with exactly the same sample. One of the...
Why do impurities reduce the melting point measurement value and increase the measurement range?
If you have a compound whose literature melting point you don’t know, how can the experimentally determined melting point provide evidence of purity?
If your sample has impurities, would the melting point range be large or small. Explain why.
can you help with part b why isn't the product pure based on the melting point??? for part c the experiment was Separation of acid/base/neutral compounds using liquid- liquid extraction of benzocaine-trans-cinnamic acid and biphenyl what was the purpose of using Na2SO4 estion 6: 100mg of each Acid, Base and Neutral compounds were used. Assuming 70mg mzocaine, 66mg trans-cinnamic acid and 50mg of biphenyl were isolated. a. Calculate % recovery of benzocaine, trans-cinnamic acid and biphenyl respectively. (show your calculation,...