Homework Answers
Hydrides show a strong peak in the region 1000 - 1255 cm-1.
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What IR stretch would indicate you have a product that did not undergo a hydride shift? O A sharp peak in the range...
Which of the following IR stretches are telling of the formation of the alkene product? A broad peak in the range o...
Which of the following IR stretches are telling of the formation of the alkene product? A broad peak in the range of 3200 - 3525 cm A sharp peak in the range 3250 - 3325 cm-1 A medium to sharp peak in the range of 3000 - 3100 cm O A strong peak in the 1000 - 1255 cm-1
Functional Groups Alcohol O-H Wavelength range, cm-1 3000-3500 Signal strength Broad peak Carboxylic acid O-H 2500-3500...
Functional Groups Alcohol O-H Wavelength range, cm-1 3000-3500 Signal strength Broad peak Carboxylic acid O-H 2500-3500 Broad peak Amine N-H 3300-3500 Broad but half the size of OH Alkyl -C-H 2850-3000 Sharp, medium Alkene =C-H 3000-3100 Sharp, medium Sharp, strong 3200-3300 2100-2300 Alkyne CEC Sharp, weak Nitrile CEN 2100-2300 Sharp, strong Carbonyl C=0 1650-1750 Sharp, strong Alkene C=C 1600-1650 Sharp, strong Sharp, strong Aromatic CEC 1450-1600 IR of trans-cinnamic acid (10 points): 2.500-350 15 00 3067 3017 1686 OH: _...
Functional Groups Alcohol O-H Wavelength range, cm-1 3000-3500 Signal strength Broad peak Carboxylic acid O-H 2500-3500...
Functional Groups Alcohol O-H Wavelength range, cm-1 3000-3500 Signal strength Broad peak Carboxylic acid O-H 2500-3500 Broad peak Amine N-H 3300-3500 Broad but half the size of OH Alkyl -C-H 2850-3000 Sharp, medium Alkene =C-H 3000-3100 Sharp, medium 3200-3300 Sharp, strong Sharp, weak Alkyne CEC 2100-2300 Nitrile CEN 2100-2300 Sharp, strong Carbonyl C=0 1650-1750 Sharp, strong Alkene C=C 1600-1650 Sharp, strong Aromatic C=C 1450-1600 Sharp, strong on : The followings are IR spectra of benzocaine, trans-cinnamic acid and biphenyl. Identify...
HW4. A student ran a reaction and obtained the following data for an unknown by-product C that contains...
HW4. A student ran a reaction and obtained the following data for an unknown by-product C that contains an alcohol functionality. Alcohol C was purified by column chromatography. Fill in the data below Molecular Formula of C (derived by Mass Spec. analysis): C&H14O The degrees of unsaturation is: Given the degrees calculated, this means: (a) (b) The FT-IR for the unknown alcohol C 100 50- 0- 1000 2000 wavenumber (cm) 3000 1500 500 4000 Bond vibration (e.g. stretch or bend)...
1. Using the IR correlation table on the second image, indicate how you could distanguish between...
1. Using the IR correlation table on the second image,
indicate how you could distanguish between the following pairs of
compounds by using infrared spectroscopy. Give two specific
absence/appearance of wavrnumbers for each compound:
2. For this experiment, what is the purpose of adding acetone?
Predict what would happen if you omitted the acetone in the
experimental procedure.
3. Draw four different resonance structures of the
triphenylmethyl cation.
*IR correlation table
PRE-LAB QUESTIONS 1. Using the IR correlation table on...
Use the following correlation chart to help answer the IR spectrum questions: small range range of...
Use the following correlation chart to help answer the IR spectrum questions: small range range of values N-H -O-H-CEN usually broad peak C-o strong 1600-1660 EC-H 3250-3300 2200 1680 gco sco 2710- 2820 2 peaks 3000- 3100 CECH (N-H C-H 1730 2200 broad with spikes --3300 O-H 1600 2850- 2960 1710 broad-3300-3400 -CO-H broad-3000 1650 4000 3500 3000 2000 1500 2500 wavenumber, cm 1000 1. (2 pts.) Shown below are IR spectra of cyclohexanecarbaldehyde (I) and cyclohexene (II). Which of...
What peak in the IR spectrum most clearly demonstrates the presence of alcohol product? If the...
What peak in the IR spectrum most clearly demonstrates the
presence of alcohol product? If the product had unreacted aldehyde
remaining, what IR peak would indicate the presence of this
contaminant?
% Transmittance 4000 100 grignard 3500 3445.90 alcohol 0-H stretching 3000 2955.99 C-H alkane stretching 2869.74 2835.23 2500 Wavenumbers (cm-1) 2000 C-H stretching 1610.54 1585.02 1500 1509.80 1464.30 1442.09 1381.94 1301.38 1242.79 1171.03 1107.61 1000 1033.47 958 30 935.19 834.42 798.16 766.54 638.11 551.44 500
Need help answering questions 5 (a, b, & c), 6, & 7. Thank you. erimental data:...
Need help answering questions 5 (a, b, & c), 6, & 7.
Thank you.
erimental data: a. Calculate the theoretical yield of product from today's experiment. Show your work (1 point) o.sgol = 0.00179 mol 278.775 g/mol lol = 0.0ol 79 mol x 260.33 ghnol = 0.466 g g b. Report the mass of synthesized product (0.25 point): 260.33 c. Report the melting range of synthesized product (0.5 point): 160-163°C d. Calculate the percent yield of today's experiment. Show your...
1. Predict whether the frequency of the IR absorption peak for the C=N stretch of the imine product is greater or less than the frequency for C=O stretch. 2. The amine was not isolated in this reacti...
1. Predict whether the frequency of the IR absorption peak for
the C=N stretch of the imine product is greater or less than the
frequency for C=O stretch.
2. The amine was not isolated in this reaction sequence. Predict
how the IR spectrum of the amine would differ from the IR of the
amide.
CH3 NaBH4 но но ÓCH3 оснз vanilin mp 81-83 °C it is Soli (E-2-methoxy-4-(p-tolylimino)methyl)phenol mp 116-117 °C C1sH15NO2 p-toluidine molar mass: 152.15 molar mass: 107.15 mp...
NMR, please help. 16) Chemical Formula: C,H,O, IR: strong peak 1720cm-1 PPM mple A4 thouis Yoo...
NMR, please help.
16) Chemical Formula: C,H,O, IR: strong peak 1720cm-1 PPM mple A4 thouis Yoo 05 quadret 1:2:2:1 Triplet 1:3:1 244 PPM USER: -- DATE: 04/12/10 08:27 PTS1d: 4096 Nuts - A4 OF1: 372.1 010 AlglobalVZGH.ppg SWI: 1000 PW: 19.6 us PD: 3.0 sec NA LB: 0.0 (ethylacetate) H3C CH₂ - CH3 C4H8O₂ 2. PROTON MAGNETIC RESONANCE SPECTRAL DATA Complete the table below by listing the chemical shiits of all of the signal patterns in the nmr spectrum of...
Which of the following IR stretches are telling of the formation of the alkene product? A broad peak in the range of 3200 - 3525 cm A sharp peak in the range 3250 - 3325 cm-1 A medium to sharp peak in the range of 3000 - 3100 cm O A strong peak in the 1000 - 1255 cm-1
Functional Groups Alcohol O-H Wavelength range, cm-1 3000-3500 Signal strength Broad peak Carboxylic acid O-H 2500-3500 Broad peak Amine N-H 3300-3500 Broad but half the size of OH Alkyl -C-H 2850-3000 Sharp, medium Alkene =C-H 3000-3100 Sharp, medium Sharp, strong 3200-3300 2100-2300 Alkyne CEC Sharp, weak Nitrile CEN 2100-2300 Sharp, strong Carbonyl C=0 1650-1750 Sharp, strong Alkene C=C 1600-1650 Sharp, strong Sharp, strong Aromatic CEC 1450-1600 IR of trans-cinnamic acid (10 points): 2.500-350 15 00 3067 3017 1686 OH: _...
Functional Groups Alcohol O-H Wavelength range, cm-1 3000-3500 Signal strength Broad peak Carboxylic acid O-H 2500-3500 Broad peak Amine N-H 3300-3500 Broad but half the size of OH Alkyl -C-H 2850-3000 Sharp, medium Alkene =C-H 3000-3100 Sharp, medium 3200-3300 Sharp, strong Sharp, weak Alkyne CEC 2100-2300 Nitrile CEN 2100-2300 Sharp, strong Carbonyl C=0 1650-1750 Sharp, strong Alkene C=C 1600-1650 Sharp, strong Aromatic C=C 1450-1600 Sharp, strong on : The followings are IR spectra of benzocaine, trans-cinnamic acid and biphenyl. Identify...
HW4. A student ran a reaction and obtained the following data for an unknown by-product C that contains an alcohol functionality. Alcohol C was purified by column chromatography. Fill in the data below Molecular Formula of C (derived by Mass Spec. analysis): C&H14O The degrees of unsaturation is: Given the degrees calculated, this means: (a) (b) The FT-IR for the unknown alcohol C 100 50- 0- 1000 2000 wavenumber (cm) 3000 1500 500 4000 Bond vibration (e.g. stretch or bend)...
1. Using the IR correlation table on the second image,
indicate how you could distanguish between the following pairs of
compounds by using infrared spectroscopy. Give two specific
absence/appearance of wavrnumbers for each compound:
2. For this experiment, what is the purpose of adding acetone?
Predict what would happen if you omitted the acetone in the
experimental procedure.
3. Draw four different resonance structures of the
triphenylmethyl cation.
*IR correlation table
PRE-LAB QUESTIONS 1. Using the IR correlation table on...
Use the following correlation chart to help answer the IR spectrum questions: small range range of values N-H -O-H-CEN usually broad peak C-o strong 1600-1660 EC-H 3250-3300 2200 1680 gco sco 2710- 2820 2 peaks 3000- 3100 CECH (N-H C-H 1730 2200 broad with spikes --3300 O-H 1600 2850- 2960 1710 broad-3300-3400 -CO-H broad-3000 1650 4000 3500 3000 2000 1500 2500 wavenumber, cm 1000 1. (2 pts.) Shown below are IR spectra of cyclohexanecarbaldehyde (I) and cyclohexene (II). Which of...
What peak in the IR spectrum most clearly demonstrates the
presence of alcohol product? If the product had unreacted aldehyde
remaining, what IR peak would indicate the presence of this
contaminant?
% Transmittance 4000 100 grignard 3500 3445.90 alcohol 0-H stretching 3000 2955.99 C-H alkane stretching 2869.74 2835.23 2500 Wavenumbers (cm-1) 2000 C-H stretching 1610.54 1585.02 1500 1509.80 1464.30 1442.09 1381.94 1301.38 1242.79 1171.03 1107.61 1000 1033.47 958 30 935.19 834.42 798.16 766.54 638.11 551.44 500
Need help answering questions 5 (a, b, & c), 6, & 7.
Thank you.
erimental data: a. Calculate the theoretical yield of product from today's experiment. Show your work (1 point) o.sgol = 0.00179 mol 278.775 g/mol lol = 0.0ol 79 mol x 260.33 ghnol = 0.466 g g b. Report the mass of synthesized product (0.25 point): 260.33 c. Report the melting range of synthesized product (0.5 point): 160-163°C d. Calculate the percent yield of today's experiment. Show your...
1. Predict whether the frequency of the IR absorption peak for
the C=N stretch of the imine product is greater or less than the
frequency for C=O stretch.
2. The amine was not isolated in this reaction sequence. Predict
how the IR spectrum of the amine would differ from the IR of the
amide.
CH3 NaBH4 но но ÓCH3 оснз vanilin mp 81-83 °C it is Soli (E-2-methoxy-4-(p-tolylimino)methyl)phenol mp 116-117 °C C1sH15NO2 p-toluidine molar mass: 152.15 molar mass: 107.15 mp...
NMR, please help.
16) Chemical Formula: C,H,O, IR: strong peak 1720cm-1 PPM mple A4 thouis Yoo 05 quadret 1:2:2:1 Triplet 1:3:1 244 PPM USER: -- DATE: 04/12/10 08:27 PTS1d: 4096 Nuts - A4 OF1: 372.1 010 AlglobalVZGH.ppg SWI: 1000 PW: 19.6 us PD: 3.0 sec NA LB: 0.0 (ethylacetate) H3C CH₂ - CH3 C4H8O₂ 2. PROTON MAGNETIC RESONANCE SPECTRAL DATA Complete the table below by listing the chemical shiits of all of the signal patterns in the nmr spectrum of...
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