In our TLC system, which compound is more likely to be at the solvent front: 1 or 2. CH3CH2CH2CH=O CH3CH2CH2...
In our TLC system, which compound is more likely to be at the solvent front: 1 or 2.
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CH3CH2CH2CH=O |
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CH3CH2CH2CH3 |
Homework Answers
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In our TLC system, which compound is more likely to be at the solvent front: 1 or 2. CH3CH2CH2CH=O CH3CH2CH2...
1. When 2-propanol was used as the developing solvent, two substances moved with the solvent front...
1. When 2-propanol was used as the developing solvent, two substances moved with the solvent front (Rf= 1) during TLC analysis on a silica gel plate. Can you conclude that they are identical? If not, what additional experiment(s) would you perform? 2. The Rf value of compound A is 0.34 when a TLC plate is developed in hexane and 0.44 when the plate is developed in diethyl ether. Compound B has an Rf value of 0.42 in hexane and 0.60...
Question 9 1 pts Considering the silica gel TLC plate shown, which compound is the most...
Question 9 1 pts Considering the silica gel TLC plate shown, which compound is the most polar (the solvent front is at 4.0 cm)? Spot Distance traveled (cm) A 0.50 В 2.0 IC 3.0 D 1.0 O Compound B (spot B) Compound A (spot A) O Compound D (spot D) O Compound C (spot C)
3. If the TLC plate development had stopped before the solvent front reached the top of...
3. If the TLC plate development had stopped before the solvent front reached the top of the TLC plate (i.e. maybe it reached the middle of the TLC plate when it was stopped, instead): a) Would the Rf values have been affected? If so, how? If not, why not? Give a numerical example to support your answer. b) Would the size of the spots have been affected? If so, how? If not, why not? (Hint: think about the diffusion of...
Please help 2. Consider the TLC plate shown below that was done on silica gel using...
Please help
2. Consider the TLC plate shown below that was done on silica gel using a solvent mixture of 4:1 hexane/EtoAc as the eluent. 4:1 Hexane:EtOAC marked solvent front Spot B Spot A A origin (a) Which of the two organic compounds labeled A and B is less polar? (b) Calculate the Rf value of compound B. (c) How would the following changes affect the Rf values of A and B? i. Change to a more polar solvent mixture...
1. A mixture containing Compound X and Compound Y is analyzed using silica gel TLC. a....
1. A mixture containing Compound X and Compound Y is analyzed using silica gel TLC. a. If Compound X has an Rf value of 0.7 and Compound Y has an Rvalue of 0.3, which compound is more polar? Explain. b. The solvent traveled 50 mm. How far did Compound Y travel? 2. Why isn't it reasonable for an R. value to be greater than 1? 3. How many spots would you expect to see if you conducted a TLC separation...
1) Calculate the Rf value of a spot that travels 5.7 cm, with a solvent front...
1) Calculate the Rf value of a spot that travels 5.7 cm, with a solvent front that travels 13 cm. 2) A student spots an unknown sample on a TLC plate and develops it in pentane solvent. Only one spot, for which the Rf value is 0.05, is observed. Is the unknown material a pure compound? What can be done to verify the purity of the sample using thin-layer chromatography? 3) You try to synthesize n-hexyl bromide as a product...
4. TLC Data: Provide a drawing of your TLC plate with proper labels, and specify which solvent system was used to d...
4. TLC Data: Provide a drawing of your TLC plate with proper labels, and specify which solvent system was used to develop the TLC. Comment on the purity of your product according to TLC. Explain why the newly produced phenacetin would run higher on the TLC plate compared to the starting material acetaminophen.
When 2-propanol was used as the developing solvent, two substances moved with the solvent front (Rf...
When 2-propanol was used as the developing solvent, two substances moved with the solvent front (Rf = 1) during TLC analysis on a silica gel plate. Can you conclude that they are identical? If not, what additional experiments(s) would you perform?
Predicting Solubilities Decide which compound will be more likely to dissolve in the given liquid. Think...
Predicting Solubilities Decide which compound will be more likely to dissolve in the given liquid. Think about the IMF between the solvent and each solute. 1. Solvent: methanol (CH3OH) Solutes: carbon diselenide and oxygen dichloride - 2. Solvent: carbon disulfide Solutes: methanol (CH3OH) and lithium chloride 3. Solvent: water Solutes: carbon tetrachloride and ammonia
can you please answer all 1. When you run a TLC of the reaction in ethyl...
can
you please answer all
1. When you run a TLC of the reaction in ethyl acetate : hexanes :: 1:1, the plate below is produced. Give a solvent system that would be expected to produce greater separation and a BRIEF (8 words) justification about your choice. (5 points) 9 10 8 7 LLLLLLL 6 5 4 001 2 3 b. Calculate the R for the bottom spot. (5 points) c. Which compound on the TLC plate is the most...
1. When 2-propanol was used as the developing solvent, two substances moved with the solvent front (Rf= 1) during TLC analysis on a silica gel plate. Can you conclude that they are identical? If not, what additional experiment(s) would you perform? 2. The Rf value of compound A is 0.34 when a TLC plate is developed in hexane and 0.44 when the plate is developed in diethyl ether. Compound B has an Rf value of 0.42 in hexane and 0.60...
Question 9 1 pts Considering the silica gel TLC plate shown, which compound is the most polar (the solvent front is at 4.0 cm)? Spot Distance traveled (cm) A 0.50 В 2.0 IC 3.0 D 1.0 O Compound B (spot B) Compound A (spot A) O Compound D (spot D) O Compound C (spot C)
Please help
2. Consider the TLC plate shown below that was done on silica gel using a solvent mixture of 4:1 hexane/EtoAc as the eluent. 4:1 Hexane:EtOAC marked solvent front Spot B Spot A A origin (a) Which of the two organic compounds labeled A and B is less polar? (b) Calculate the Rf value of compound B. (c) How would the following changes affect the Rf values of A and B? i. Change to a more polar solvent mixture...
1. A mixture containing Compound X and Compound Y is analyzed using silica gel TLC. a. If Compound X has an Rf value of 0.7 and Compound Y has an Rvalue of 0.3, which compound is more polar? Explain. b. The solvent traveled 50 mm. How far did Compound Y travel? 2. Why isn't it reasonable for an R. value to be greater than 1? 3. How many spots would you expect to see if you conducted a TLC separation...
1) Calculate the Rf value of a spot that travels 5.7 cm, with a solvent front that travels 13 cm. 2) A student spots an unknown sample on a TLC plate and develops it in pentane solvent. Only one spot, for which the Rf value is 0.05, is observed. Is the unknown material a pure compound? What can be done to verify the purity of the sample using thin-layer chromatography? 3) You try to synthesize n-hexyl bromide as a product...
4. TLC Data: Provide a drawing of your TLC plate with proper labels, and specify which solvent system was used to develop the TLC. Comment on the purity of your product according to TLC. Explain why the newly produced phenacetin would run higher on the TLC plate compared to the starting material acetaminophen.
Predicting Solubilities Decide which compound will be more likely to dissolve in the given liquid. Think about the IMF between the solvent and each solute. 1. Solvent: methanol (CH3OH) Solutes: carbon diselenide and oxygen dichloride - 2. Solvent: carbon disulfide Solutes: methanol (CH3OH) and lithium chloride 3. Solvent: water Solutes: carbon tetrachloride and ammonia
can
you please answer all
1. When you run a TLC of the reaction in ethyl acetate : hexanes :: 1:1, the plate below is produced. Give a solvent system that would be expected to produce greater separation and a BRIEF (8 words) justification about your choice. (5 points) 9 10 8 7 LLLLLLL 6 5 4 001 2 3 b. Calculate the R for the bottom spot. (5 points) c. Which compound on the TLC plate is the most...
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