Q27. 6 marks Amitriptyline is a basic drug with a pKa of 9.4 and a Pire...
Would the methylene chloride layer be above or below the experiment? Justify your answer. 1. aqueous layer in today's ium carbonate used in the isolation of caffeine? Be specific as to the 2. Why is potass chemical species the carbonate may act on. Why was sodium sulfate used? 3. 4. After introducing 1.0 g of potassium carbonate into the centri hot water extract, it was capped, shaken, and then cooled to room temperature. Following this, roug minute. Why wasn't the...
Exercise 2 Separation of a Mixture Based on Acid-Base Properties One purpose of this exercise is to learn how to use a separatory funnel to extract a single component away from other compounds in solution. To do so, we will apply the principles of solubility and acid-base behavior you’re seeing in class. One of the compounds is neutral in the acid-base sense. It has no ability to either donate or accept a proton from an aqueous solution, and will remain...
QUESTION: Show the mechanism of the reduction of 3-dimethylaminopropiophenone hydrochloride to form the alcohol? PROCEDURE: Add 2.00 g of 3-dimethylaminopropiophenone hydrochloride, 10 mL of distilled water and a magnetic stir bar to a 100 mL beaker, and stir to dissolve. This is the reaction beaker. Add (with stirring) sufficient 10% NaOH (about 5–6 mL) to bring the solution to pH >10. The free base will form and come out of solution as a milky oil. With continued stirring, add enough...
Heroin (Mw = 369.42 g/mol) is weakly basic compound due to its tertiary amine group. The pKa of its conjugate acid form is 7.95. Six grams of a street drug containing heroin and calcium phosphate as the only components was shaken with 60 mL of chloroform. The chloroform was carefully decanted and evaporated to yield 738.84 mg of white solid, which was then dissolved in 300 mL of 6 mM HCl in water. This aqueous solution was divided into three...
3) The hydrogen atom in HCl is electrophilic whereas the hydrogen atoms in sodium borohydride are nucleophilic. Offer a plausible rationale for this difference in reactivity. PROCEDURES 1. Add 2.00 g of 3-dimethylaminopropiophenone hydrochloride, 10 mL of distilled water and a magnetic stir bar to a 100 ml beaker, and stir to dissolve. This is the reaction beaker. 2. Add (with stirring) sufficient 10% NaOH (about 5-6 mL) to bring the solution to pH > 10. The free base will...
please answer all these questions, thank you. CHEM 242L Exp. 4 Report/ Synthesis of Oil of Wintergreen Name Score: 20 1) Assess the effectiveness of the experiment and your technique by A) reporting the yield of each step in grams and percent as well as the overall percent yield (What is "overall percent yield?). SHOW ALL CALCULATIONS! B) Give a complete analysis of the identity and purity of your final product and any isolated intermediates 2 What was the purpose...
10. Write a one-page summary of the attached paper? INTRODUCTION Many problems can develop in activated sludge operation that adversely affect effluent quality with origins in the engineering, hydraulic and microbiological components of the process. The real "heart" of the activated sludge system is the development and maintenance of a mixed microbial culture (activated sludge) that treats wastewater and which can be managed. One definition of a wastewater treatment plant operator is a "bug farmer", one who controls the aeration...