Hi can someone help me with question 2? It deals with Rf values and the collected data is given below!
Homework Answers
The correct order in terms of Rf values is given below.
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Hi can someone help me with question 2? It deals with Rf values
and the collected...
Hi can someone please help with question #1. It deals with Rf values and the data...
Hi can someone please help with question #1. It deals with Rf
values and the data collected is given below!
Results: Rf Values Of Compounds In Solvents Solvents 100% 50% hexanes 75% hexanes 25% ethyl 100% ethyl Hexane 25% hexanes 75% ethyl acetate 50% ethyl Compounds acetate acetate acetate trans-Stilbene 0.125 0.419 0.781 0.594 0.906 9-Fluorenone 0.156 0.677 0.906 0.375 0.843 Benzoic Acid 0.094 0.742 0.813 0.656 0.937 # 1. A solvent that gives a high Rf value is said...
Hi can someone help me with my pre lab theory questions (1,2,3) on rate of elution...
Hi can someone help me with my pre lab theory questions (1,2,3)
on rate of elution or Rf? Here is some background below. Please
help explain as many as possible (1-3)! I dont really get the
relation ships in this lab, thank you!
1. What factors affect the rate of elution in organic compounds? 2. Explain what is the relationship between polarities of compounds (polar/non- polar compound) and rate of elution (Rf). 3. Explain what is the relationship between solvent...
Can someone please help me out with the Rf value PLEASE!! Thin Layer Chromatography Procedures 1)...
Can someone please help me out with the Rf value
PLEASE!!
Thin Layer Chromatography Procedures 1) Prepare a solvent solution in a 150 mL beaker by using 5 mL of Hexane and 3 mL of ethyl acetate Take one plate and spot (small spots) it with the three different standard solutions given. The standard solutions are 2-nitroaniline, 3-nitroaniline, and 4-nitroaniline. The fourth spot will be the unknown sample obtained. 2) 3) Align these spots at 1 cm from the bottom...
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC...
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC and GC. Use the structures and properties of the compounds to aid in answering the following questions. A. In the TLC experiment, the mixture is spotted on a silica TLC plate and eluted with a 1:1 mixture of hexanes and ethyl acetate. Three spots are observed on the plate, with Re values of 0.25, 0.58, and 0.74. Indicate which spot corresponds to which compound....
Please can someone help me to interpret this. This was from Orgo II Williamson ether Lab. These a...
Please can someone help me to interpret this. This was
from Orgo II Williamson ether Lab. These are the results and I need
help interpreting what this is showing. More especially for the
discussion and conclusion section. Thank You!
(if needed here are the procedures)
Add a magnetic stir bar to a 25ml round or pear-shaped
flask.
Add guaiacol (0.55ml,5mmoles) to the flask along with 3ml of
95% ethanol. Make sure the guaiacol dissolves in the ethanol before
proceeding.
Add...
Can someone help me figure out this unknown compound? It should be an alcohol C-H Analysis...
Can someone help me figure out this unknown compound? It
should be an alcohol
C-H Analysis %C=84.75 %H=6.57 Melting Point (°C) 66 Boiling Point (°C) 298 TLC (R) n/a Carbon NMR of unknown #68 Common Name: 13C NMR WPCName Zoom Out CAS No: Solvent: BP: MP: 1.00 0.90 0.80 0.70 0.60 0.50 0.40 0.30 0.20 0.10 0.00 40 130 110 100 IR Spectrum for unknown #68 BP: FTIR Common Name: IUPAC Name: MP MICRONS 22 23 24 25 26 272.12.07...
Unknown 315-S20-2 Can someone help me fill out the table on the right side please IR...
Unknown 315-S20-2
Can someone help me fill out the table on the right side
please
IR Spectrum:
Unknown # 315-S20-2 Mol. Wt. = 181.0 g/mol C-33.17% H=5.01% 0 = 17.68% Molecular Formula Degree of Unsaturation = Mass Spectrum IR spectrum (liquid film) 100- Relative Intensity 150 175 25 50 75 100 125 m/z Based on the M.W., circle & label the molecular ion peak (M). Spectrum Region Frequency (cm ) Peak Shape (sharp, broad) MAVUTO Peak Intensity (strong, med., weak)...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
Exercise 2 Separation of a Mixture Based on Acid-Base Properties One purpose of this exercise is...
Exercise 2 Separation of a Mixture Based on Acid-Base Properties One purpose of this exercise is to learn how to use a separatory funnel to extract a single component away from other compounds in solution. To do so, we will apply the principles of solubility and acid-base behavior you’re seeing in class. One of the compounds is neutral in the acid-base sense. It has no ability to either donate or accept a proton from an aqueous solution, and will remain...
Hi can someone please help with question #1. It deals with Rf
values and the data collected is given below!
Results: Rf Values Of Compounds In Solvents Solvents 100% 50% hexanes 75% hexanes 25% ethyl 100% ethyl Hexane 25% hexanes 75% ethyl acetate 50% ethyl Compounds acetate acetate acetate trans-Stilbene 0.125 0.419 0.781 0.594 0.906 9-Fluorenone 0.156 0.677 0.906 0.375 0.843 Benzoic Acid 0.094 0.742 0.813 0.656 0.937 # 1. A solvent that gives a high Rf value is said...
Hi can someone help me with my pre lab theory questions (1,2,3)
on rate of elution or Rf? Here is some background below. Please
help explain as many as possible (1-3)! I dont really get the
relation ships in this lab, thank you!
1. What factors affect the rate of elution in organic compounds? 2. Explain what is the relationship between polarities of compounds (polar/non- polar compound) and rate of elution (Rf). 3. Explain what is the relationship between solvent...
Can someone please help me out with the Rf value
PLEASE!!
Thin Layer Chromatography Procedures 1) Prepare a solvent solution in a 150 mL beaker by using 5 mL of Hexane and 3 mL of ethyl acetate Take one plate and spot (small spots) it with the three different standard solutions given. The standard solutions are 2-nitroaniline, 3-nitroaniline, and 4-nitroaniline. The fourth spot will be the unknown sample obtained. 2) 3) Align these spots at 1 cm from the bottom...
2. A solution containing a mixture of naphthalene, benzoic acid, and benzaldehyde is analyzed via TLC and GC. Use the structures and properties of the compounds to aid in answering the following questions. A. In the TLC experiment, the mixture is spotted on a silica TLC plate and eluted with a 1:1 mixture of hexanes and ethyl acetate. Three spots are observed on the plate, with Re values of 0.25, 0.58, and 0.74. Indicate which spot corresponds to which compound....
Please can someone help me to interpret this. This was
from Orgo II Williamson ether Lab. These are the results and I need
help interpreting what this is showing. More especially for the
discussion and conclusion section. Thank You!
(if needed here are the procedures)
Add a magnetic stir bar to a 25ml round or pear-shaped
flask.
Add guaiacol (0.55ml,5mmoles) to the flask along with 3ml of
95% ethanol. Make sure the guaiacol dissolves in the ethanol before
proceeding.
Add...
Can someone help me figure out this unknown compound? It
should be an alcohol
C-H Analysis %C=84.75 %H=6.57 Melting Point (°C) 66 Boiling Point (°C) 298 TLC (R) n/a Carbon NMR of unknown #68 Common Name: 13C NMR WPCName Zoom Out CAS No: Solvent: BP: MP: 1.00 0.90 0.80 0.70 0.60 0.50 0.40 0.30 0.20 0.10 0.00 40 130 110 100 IR Spectrum for unknown #68 BP: FTIR Common Name: IUPAC Name: MP MICRONS 22 23 24 25 26 272.12.07...
Unknown 315-S20-2
Can someone help me fill out the table on the right side
please
IR Spectrum:
Unknown # 315-S20-2 Mol. Wt. = 181.0 g/mol C-33.17% H=5.01% 0 = 17.68% Molecular Formula Degree of Unsaturation = Mass Spectrum IR spectrum (liquid film) 100- Relative Intensity 150 175 25 50 75 100 125 m/z Based on the M.W., circle & label the molecular ion peak (M). Spectrum Region Frequency (cm ) Peak Shape (sharp, broad) MAVUTO Peak Intensity (strong, med., weak)...
Experiment Write Up Proposal You will write up a synthesis procedure for one reaction that could be potentially run in a face- to-face Chem 2321 lab session. Your proposal will include an introduction and procedure. The procedure will include step-by-step instructions for running the reaction (including reaction monitoring), work-up. (product isolation and purification), and analysis (characterization). You will need to include sample calculations for percent yield and provide sample spectra analysis. You must upload your proposal as a single document...
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