After I made extraction I put dry agent ( sodium magniusm) and the lab time is up and I left it for two days insteaf of 10 mins and all my product is gone
Can you pease think if reasons why nothing left ?
May be the solvent which has been used to collect the amine is evaporated slowly in two days. You may recover it by using the same solvent you have used before (provided the amine has not been decomposed)
( This is common thing which happens in synthesis lab. If the product has been left in the solvent kept with drying agent overnight, the solvent evaporates leaving behind only the drying agent and the compund. If the compound is stable enough it can be recovered using the same solvent)
After I made extraction I put dry agent ( sodium magniusm) and the lab time is...
i need to calculate the theortetical yield by finding the limiting reactant of the experiment by converting reactants to product, then calculate the percent yield using the limiting reactant -in my experiment the amout of crystals i obtained was 1.232 g (watch glass + filter paper = 31.228 g and watch glass, filter paper, + crystals = 32.460 g) REACTION SCHEME H сно, ОН- ОСH, CH panisaldehyde acetophenone Molar Mass: 120.15g/mol Molar Mass: 136.15g/mol Molar Mass: 239.30g/mol Density: 1.119g/mL Density:...
I only need help with the PRE-LAB section. I included the recorded information. Calculate the mass in gram of Sodium hydroxide (NaOH), 2-naphthol, and 1-bromobutane (n-BuBr). EXPERIMENT 9 SYNTHESIS OF 2-BUTOXYNAPHTHALENE OH 1. NaOH, ETOH .LT 2. n-BuBr DISCUSSION: Nucleophilic substitution reaction is a frequently used method to convert one functional group into another. A nucleophile is mixed with an electrophile and the nucleophile replaces the leaving group to produce a new compound. In this experiment, a weak nucleophile (2-naphthol)...
Organic Chemistry Help! Questions and Exercises 1. In the course of reflux of the triglyceride in a sodium hydroxide solution you will notice a lot of foaming. Explain. What is left behind in the aqueous layer after filtration of the saponification product? The starting material and the product of the saponification reaction have similar melting points. How do you know you actually isolated a new product rather than just recovered the starting material? Give at least two different methods to...
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