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d. Suppose you mistakenly acidify the filtrate with HCl instead of with HNO3. What would you...
3. a. What happens in Part Fl if conc NaOH is substituted for conc NH4OH? b....
3. a. What happens in Part Fl if conc NaOH is substituted for conc NH4OH? b. What happens to the precipitate in Part F1 if conc HCl is added? 3. Dissolve the Cu2+ and Bil Sulfides. Add 15 drops of 6 M HNO3 to the precipitate from Part E.2 and carefully heat with a direct flame until the precipitates dissolve. (Caution: make sure the test tube is pointed away from all other students while heating). Cool and centrifuge. Save the...
Oxalate ion will interfere with the Group D tests after we make the solution acidic. Also,...
Oxalate ion will interfere with the Group D tests after we make the solution acidic. Also, ammonium ion may prevent the precipitation of Group Dcations as hydroxides in sodium hydroxide solution. Thus, must treat the supernatant liquid left after we have precipitated calcium oxalate, in order to destroy any remaining Oxalate or ammonium ions prior to further analysis. To accomplish this, we transfer the solution to a crucible, add concentrated nitric acid and heat the mixture to dryness in a...
Question: Procedure Separation and Identification of Pb2 (aq), Fe (aq), Al(a), and Cu Note: Tests should...
Question:
Procedure Separation and Identification of Pb2 (aq), Fe (aq), Al(a), and Cu Note: Tests should be performed concurrently on the known and the unknown solutions. Volumes are approximate. All work excepting the centrifugation should be done in the fume hood 1. To about 2. mL of your sample in a test tube, add 5 drops (-0.2 mL) of 6 M HCl(a). Mix well and centrifuge. Decant the clear liquid into a clean test tube and save it for Step...
Observations seemed to be off, how would the structural formula influence my observations and what would...
Observations seemed to be off, how would the structural
formula influence my observations and what would the balanced
equations be for the different solutions?
IIIB. Oxidation reaction with Fehling's solution-(Cu2 /Cu Aldehydes can be further oxidized to carboxylic acids by mild oxidizing agents such as Cu ions. Ketones do not undergo this reaction. One such mild oxidizing reagent is Fehling's solution, a solution of copper sulfate (CuSO4) mixed with an alkaline solution of sodium-potassium tartrate. In the process Cu?+ is...
help!! need tk balance the metals nickel(II), iron(III), manganese(II), and aluminum!! due in 20 minutes 4....
help!! need tk balance the metals nickel(II), iron(III),
manganese(II), and aluminum!! due in 20 minutes
4. Add 12 drops of water and 2 drops of 12 M hydrochloric acid and stir thoroughly for about a minute. Centrifuge and decant the solution immediately. Save the solution for Step 6. 5. Wash the precipitate from Step 4 with water and discard the washing. Add 5 drops of 6 M hydrochloric acid and 1 drop of 6M nitric acid. Heat in a water...
3. Suppose after adding HCl to ppt 16, you do not have any black solid. What,...
3. Suppose after adding HCl to ppt 16, you do not have any black solid. What, if anything, should you do to test for Co2 and Ni*? Qual Scheme: Group III: Co?(pink), N1" (green), Fet+ (yellow), Cr" (blue-grey), Mn(pink), AP (colorless), Zn? (colorless). Unknown B Solution: Use 10 dps of unknown sample and 10 dps of H20 and go to Procedure for Group III. Procedure for Group II: Add 2 dps NHCl soln, add 6M NHOH until just basic to...
I need to write a conclusion for this lab. Based off these results what kinds of...
I need to write a conclusion for this lab. Based off these
results what kinds of conclusions can be drawn?
S OY Orre tes. A, B. Color, pH, Specific Gravity, and Electrolytes "Normal Urine Specimen" Test A. Color I clear "Abnormal Urine Specimen" slightly cloudy PH 2 1.10 gime! Specific gravity 0.70 glume - B. Electrolytes (Indicate absent - present +, strongly present ++) nornal Nat CI SO,2- PO,- 219 C-F. Glucose, Ketone Bodies, Protein, and Urobilinogen "Normal Urine Specimen"...
what is the theoretical yield of anisalacetophenone and dibenzalacetone formed? thank you. The Aldol Condensation Precautions:...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
Attached is the lab experiment. Here are the questions I need help with: 1. What is...
Attached is the lab experiment. Here are the questions I need
help with:
1. What is the purpose of each of the following steps in this
experiment?
a. Adding solid NaCl to the reaction mixture
b. Repeated washings with water, sat'd NAHCO3, and brine
c. the pipet column chromatography
2. Which compound, cyclohexanol or cyclohexanone will have a
higher Rf on a TLC plate?
3. What is the advantage of using sodium hypochlorite as an
oxidant over CrO3 or Na2Cr2O7...
What would be my percent yield if i retrieved 3.1020 grams of soap? thank you, please show all work.
what would be my percent yield if i retrieved 3.1020 grams of
soap? thank you, please show all work.
SAPONIFICATION (HYDROLYSIS OF A FAD Fats and edible oils consitute a special class of esters called riglycerides in which alcohol part of the molecule, the trihydroxy compound glycerol, forms with three molecules of various long-chain carboxylic acids (called fatty acids). Ty reactions of simple esters can also be carried out on fats and oils,i acid-or-base-catalyzed hydrolysis. three ester linkages carboxylic acids...
3. a. What happens in Part Fl if conc NaOH is substituted for conc NH4OH? b. What happens to the precipitate in Part F1 if conc HCl is added? 3. Dissolve the Cu2+ and Bil Sulfides. Add 15 drops of 6 M HNO3 to the precipitate from Part E.2 and carefully heat with a direct flame until the precipitates dissolve. (Caution: make sure the test tube is pointed away from all other students while heating). Cool and centrifuge. Save the...
Oxalate ion will interfere with the Group D tests after we make the solution acidic. Also, ammonium ion may prevent the precipitation of Group Dcations as hydroxides in sodium hydroxide solution. Thus, must treat the supernatant liquid left after we have precipitated calcium oxalate, in order to destroy any remaining Oxalate or ammonium ions prior to further analysis. To accomplish this, we transfer the solution to a crucible, add concentrated nitric acid and heat the mixture to dryness in a...
Question:
Procedure Separation and Identification of Pb2 (aq), Fe (aq), Al(a), and Cu Note: Tests should be performed concurrently on the known and the unknown solutions. Volumes are approximate. All work excepting the centrifugation should be done in the fume hood 1. To about 2. mL of your sample in a test tube, add 5 drops (-0.2 mL) of 6 M HCl(a). Mix well and centrifuge. Decant the clear liquid into a clean test tube and save it for Step...
Observations seemed to be off, how would the structural
formula influence my observations and what would the balanced
equations be for the different solutions?
IIIB. Oxidation reaction with Fehling's solution-(Cu2 /Cu Aldehydes can be further oxidized to carboxylic acids by mild oxidizing agents such as Cu ions. Ketones do not undergo this reaction. One such mild oxidizing reagent is Fehling's solution, a solution of copper sulfate (CuSO4) mixed with an alkaline solution of sodium-potassium tartrate. In the process Cu?+ is...
help!! need tk balance the metals nickel(II), iron(III),
manganese(II), and aluminum!! due in 20 minutes
4. Add 12 drops of water and 2 drops of 12 M hydrochloric acid and stir thoroughly for about a minute. Centrifuge and decant the solution immediately. Save the solution for Step 6. 5. Wash the precipitate from Step 4 with water and discard the washing. Add 5 drops of 6 M hydrochloric acid and 1 drop of 6M nitric acid. Heat in a water...
3. Suppose after adding HCl to ppt 16, you do not have any black solid. What, if anything, should you do to test for Co2 and Ni*? Qual Scheme: Group III: Co?(pink), N1" (green), Fet+ (yellow), Cr" (blue-grey), Mn(pink), AP (colorless), Zn? (colorless). Unknown B Solution: Use 10 dps of unknown sample and 10 dps of H20 and go to Procedure for Group III. Procedure for Group II: Add 2 dps NHCl soln, add 6M NHOH until just basic to...
I need to write a conclusion for this lab. Based off these
results what kinds of conclusions can be drawn?
S OY Orre tes. A, B. Color, pH, Specific Gravity, and Electrolytes "Normal Urine Specimen" Test A. Color I clear "Abnormal Urine Specimen" slightly cloudy PH 2 1.10 gime! Specific gravity 0.70 glume - B. Electrolytes (Indicate absent - present +, strongly present ++) nornal Nat CI SO,2- PO,- 219 C-F. Glucose, Ketone Bodies, Protein, and Urobilinogen "Normal Urine Specimen"...
what is the theoretical yield of anisalacetophenone and
dibenzalacetone formed? thank you.
The Aldol Condensation Precautions: Acetone, ethanol and acetophenone are flammable; work in a fume hood. Sodium hydroxide is a strong base and can cause severe skin burns and eye damage. Safety goggles are required. Gloves are recommended. Purpose To carry out two Aldol condensation reactions in which no heat is needed to obtain the condensation product. The two reactions differ in the number of enolizable protons at the...
Attached is the lab experiment. Here are the questions I need
help with:
1. What is the purpose of each of the following steps in this
experiment?
a. Adding solid NaCl to the reaction mixture
b. Repeated washings with water, sat'd NAHCO3, and brine
c. the pipet column chromatography
2. Which compound, cyclohexanol or cyclohexanone will have a
higher Rf on a TLC plate?
3. What is the advantage of using sodium hypochlorite as an
oxidant over CrO3 or Na2Cr2O7...
what would be my percent yield if i retrieved 3.1020 grams of
soap? thank you, please show all work.
SAPONIFICATION (HYDROLYSIS OF A FAD Fats and edible oils consitute a special class of esters called riglycerides in which alcohol part of the molecule, the trihydroxy compound glycerol, forms with three molecules of various long-chain carboxylic acids (called fatty acids). Ty reactions of simple esters can also be carried out on fats and oils,i acid-or-base-catalyzed hydrolysis. three ester linkages carboxylic acids...
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